Synthesis, characterization and development of high performance siloxane-modified epoxy paints
Diglycidyl ether of bisphenol A (DGEBA) epoxy was modified with hydroxyl-terminated poly dimethyl siloxane (HPDMS), through ring opening addition polymerization reaction. The structural elucidation of the siloxane-modified epoxy resin (ESR) was carried out by FT-IR, 1H-NMR and 13C-NMR spectroscopic...
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| Published in: | Progress in organic coatings Vol. 54; no. 3; pp. 248 - 255 |
|---|---|
| Main Authors: | , , , , |
| Format: | Journal Article |
| Language: | English |
| Published: |
Lausanne
Elsevier B.V
01-11-2005
Elsevier Sequoia |
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| Online Access: | Get full text |
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| Abstract | Diglycidyl ether of bisphenol A (DGEBA) epoxy was modified with hydroxyl-terminated poly dimethyl siloxane (HPDMS), through ring opening addition polymerization reaction. The structural elucidation of the siloxane-modified epoxy resin (ESR) was carried out by FT-IR,
1H-NMR and
13C-NMR spectroscopic techniques. The physico-chemical characterization of the synthesized resin (ESR) was done by standard methods. DGEBA and ESR, were subjected to paint formulation with the help of TiO
2, Fe
2O
3 and lemon chrome pigments. The formulated paint systems were cured at room temperature with polyamide (PA) used as curing agent. The DGEBA–PA and siloxane-modified epoxy–polyamide (ESR–PA) paints were applied on mild steel strips. The physico-mechanical and anticorrosive performance of the coated panels was evaluated by standard methods. Thermal analysis of DGEBA–PA, epoxy siloxane/PA systems was carried out by thermogravimetric analysis (TGA). The effect of siloxane incorporation and the role of PA as a curing agent on the coating properties of these paint systems was also investigated. The ESR–PA system was found to exhibit good thermal and corrosion resistance performance. |
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| AbstractList | Diglycidyl ether of bisphenol A (DGEBA) epoxy was modified with hydroxyl-terminated poly dimethyl siloxane (HPDMS), through ring opening addition polymerization reaction. The structural elucidation of the siloxane-modified epoxy resin (ESR) was carried out by FT-IR,
1H-NMR and
13C-NMR spectroscopic techniques. The physico-chemical characterization of the synthesized resin (ESR) was done by standard methods. DGEBA and ESR, were subjected to paint formulation with the help of TiO
2, Fe
2O
3 and lemon chrome pigments. The formulated paint systems were cured at room temperature with polyamide (PA) used as curing agent. The DGEBA–PA and siloxane-modified epoxy–polyamide (ESR–PA) paints were applied on mild steel strips. The physico-mechanical and anticorrosive performance of the coated panels was evaluated by standard methods. Thermal analysis of DGEBA–PA, epoxy siloxane/PA systems was carried out by thermogravimetric analysis (TGA). The effect of siloxane incorporation and the role of PA as a curing agent on the coating properties of these paint systems was also investigated. The ESR–PA system was found to exhibit good thermal and corrosion resistance performance. Diglycidyl ether of bisphenol A (DGEBA) epoxy was modified with hydroxyl-terminated poly dimethyl siloxane (HPDMS), through ring opening addition polymerization reaction. The structural elucidation of the siloxane-modified epoxy resin (ESR) was carried out by FT-IR, 1H-NMR and13C-NMR spectroscopic techniques. The physico-chemical characterization of the synthesized resin (ESR) was done by standard methods. DGEBA and ESR, were subjected to paint formulation with the help of TiO2, Fe2O3 and lemon chrome pigments. The formulated paint systems were cured at room temperature with polyamide (PA) used as curing agent. The DGEBA-PA and siloxane-modified epoxy-polyamide (ESR-PA) paints were applied on mild steel strips. The physico-mechanical and anticorrosive performance of the coated panels was evaluated by standard methods. Thermal analysis of DGEBA-PA, epoxy siloxane/PA systems was carried out by thermogravimetric analysis (TGA). The effect of siloxane incorporation and the role of PA as a curing agent on the coating properties of these paint systems was also investigated. The ESR-PA system was found to exhibit good thermal and corrosion resistance performance. |
| Author | Alam, Manawwer Pandey, S.K. Ahmad, Sharif Gupta, A.P. Sharmin, Eram |
| Author_xml | – sequence: 1 givenname: Sharif surname: Ahmad fullname: Ahmad, Sharif email: sharifahmad_jmi@yahoo.co.in organization: Materials Research Laboratory, Department of Chemistry, Jamia Millia Islamia, New Delhi 110025, India – sequence: 2 givenname: A.P. surname: Gupta fullname: Gupta, A.P. organization: Department of Applied Chemistry & Polymer Technology, Delhi College of Engineering, New Delhi 110042, India – sequence: 3 givenname: Eram surname: Sharmin fullname: Sharmin, Eram organization: Materials Research Laboratory, Department of Chemistry, Jamia Millia Islamia, New Delhi 110025, India – sequence: 4 givenname: Manawwer surname: Alam fullname: Alam, Manawwer organization: Materials Research Laboratory, Department of Chemistry, Jamia Millia Islamia, New Delhi 110025, India – sequence: 5 givenname: S.K. surname: Pandey fullname: Pandey, S.K. organization: Department of Applied Chemistry & Polymer Technology, Delhi College of Engineering, New Delhi 110042, India |
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| Keywords | Epoxy resin Polyamide Anticorrosive Paint Polydimethylsiloxane Ring opening polymerization Coatings Retention Formulation Optical properties Pigments Epoxy resin: Polydimethylsiloxane Manufacturing Nuclear magnetic resonance Infrared spectrum Siloxane polymer Scanning electron microscopy Chemical resistance Color Thermogravimetry Experimental study Corrosion resistance Bisphenol A Gloss Epoxide Fourier transform spectra Performance |
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| SubjectTerms | Anticorrosive Applied sciences Coatings. Paints, varnishes and inks Corrosion Corrosion mechanisms Epoxy resin Exact sciences and technology Manufacturing Metals. Metallurgy Paint Polyamide Polydimethylsiloxane Polymer industry, paints, wood |
| Title | Synthesis, characterization and development of high performance siloxane-modified epoxy paints |
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