Effect of the eutectic Al-(Ce,La) phase morphology on microstructure, mechanical properties, electrical conductivity and heat resistance of Al-4.5(Ce,La) alloy after SPD and subsequent annealing
This paper reports on a crucial role of the morphology of intermetallic Al11RE3 phase and Al/Al11RE3 interphase (where RE – Rare Earth) surface area, before plastic deformation, on the electrical and mechanical properties and the thermostability of aluminium alloys. Cast Al-4.5 (Ce + La) alloy sampl...
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| Published in: | Journal of alloys and compounds Vol. 796; pp. 321 - 330 |
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| Main Authors: | , , , , , , |
| Format: | Journal Article |
| Language: | English |
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Elsevier B.V
05-08-2019
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| Abstract | This paper reports on a crucial role of the morphology of intermetallic Al11RE3 phase and Al/Al11RE3 interphase (where RE – Rare Earth) surface area, before plastic deformation, on the electrical and mechanical properties and the thermostability of aluminium alloys. Cast Al-4.5 (Ce + La) alloy samples, processed with and without spheroidization treatment (ST), were subjected to high pressure torsion (HPT) at room temperature (RT) followed by annealing at 230 °C, 280 °C and 400 °C for 1 h. It is demonstrated, that the changes of initial alloy structure (particles shape/size) and the decrease of interphase surface area affect the distribution of intermetallic particles after HPT, the distribution of ultrafine grains and the dislocation density, as well as the formation of a supersaturated solid solution of Ce and La in aluminium. The optimal combination of strength (ultimate tensile stress (σUTS) 430 MPa) and conductivity (55.9% International Annealed Copper Standard, IACS) was obtained after ST, HPT and an annealing temperature of 230 °C.
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•Influence intermetallic morphology on structure and properties of Al alloys is studied.•The alloys were subjected to severe plastic deformation in different initial state.•HPT of Al-4.5(Ce,La) alloy results in supersaturated solid solution formation.•Application of pre-HPT heat treatment prevents the solid solution formation during HPT.•The diffusion of Ce and La in Al is provided by extra vacancy concentration. |
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| AbstractList | This paper reports on a crucial role of the morphology of intermetallic Al11RE3 phase and Al/Al11RE3 interphase (where RE – Rare Earth) surface area, before plastic deformation, on the electrical and mechanical properties and the thermostability of aluminium alloys. Cast Al-4.5 (Ce + La) alloy samples, processed with and without spheroidization treatment (ST), were subjected to high pressure torsion (HPT) at room temperature (RT) followed by annealing at 230 °C, 280 °C and 400 °C for 1 h. It is demonstrated, that the changes of initial alloy structure (particles shape/size) and the decrease of interphase surface area affect the distribution of intermetallic particles after HPT, the distribution of ultrafine grains and the dislocation density, as well as the formation of a supersaturated solid solution of Ce and La in aluminium. The optimal combination of strength (ultimate tensile stress (σUTS) 430 MPa) and conductivity (55.9% International Annealed Copper Standard, IACS) was obtained after ST, HPT and an annealing temperature of 230 °C. This paper reports on a crucial role of the morphology of intermetallic Al11RE3 phase and Al/Al11RE3 interphase (where RE – Rare Earth) surface area, before plastic deformation, on the electrical and mechanical properties and the thermostability of aluminium alloys. Cast Al-4.5 (Ce + La) alloy samples, processed with and without spheroidization treatment (ST), were subjected to high pressure torsion (HPT) at room temperature (RT) followed by annealing at 230 °C, 280 °C and 400 °C for 1 h. It is demonstrated, that the changes of initial alloy structure (particles shape/size) and the decrease of interphase surface area affect the distribution of intermetallic particles after HPT, the distribution of ultrafine grains and the dislocation density, as well as the formation of a supersaturated solid solution of Ce and La in aluminium. The optimal combination of strength (ultimate tensile stress (σUTS) 430 MPa) and conductivity (55.9% International Annealed Copper Standard, IACS) was obtained after ST, HPT and an annealing temperature of 230 °C. [Display omitted] •Influence intermetallic morphology on structure and properties of Al alloys is studied.•The alloys were subjected to severe plastic deformation in different initial state.•HPT of Al-4.5(Ce,La) alloy results in supersaturated solid solution formation.•Application of pre-HPT heat treatment prevents the solid solution formation during HPT.•The diffusion of Ce and La in Al is provided by extra vacancy concentration. |
| Author | Bikmukhametov, Ilyas Medvedev, Andrey E. Valiev, Ruslan Z. Murashkin, Maxim Y. Enikeev, Nariman A. Lapovok, Rimma Hodgson, Peter D. |
| Author_xml | – sequence: 1 givenname: Andrey E. orcidid: 0000-0002-8616-0042 surname: Medvedev fullname: Medvedev, Andrey E. email: medvedevandreyrf@gmail.com organization: Institute for Frontier Materials, Deakin University, Waurn Ponds, Victoria 3216, Australia – sequence: 2 givenname: Maxim Y. surname: Murashkin fullname: Murashkin, Maxim Y. organization: Institute of Physics of Advanced Materials, Ufa State Aviation Technical University, Ufa 450000, Russia – sequence: 3 givenname: Nariman A. orcidid: 0000-0002-7503-8949 surname: Enikeev fullname: Enikeev, Nariman A. organization: Institute of Physics of Advanced Materials, Ufa State Aviation Technical University, Ufa 450000, Russia – sequence: 4 givenname: Ilyas orcidid: 0000-0002-7763-5579 surname: Bikmukhametov fullname: Bikmukhametov, Ilyas organization: Institute for Frontier Materials, Deakin University, Waurn Ponds, Victoria 3216, Australia – sequence: 5 givenname: Ruslan Z. surname: Valiev fullname: Valiev, Ruslan Z. organization: Institute of Physics of Advanced Materials, Ufa State Aviation Technical University, Ufa 450000, Russia – sequence: 6 givenname: Peter D. surname: Hodgson fullname: Hodgson, Peter D. organization: Institute for Frontier Materials, Deakin University, Waurn Ponds, Victoria 3216, Australia – sequence: 7 givenname: Rimma surname: Lapovok fullname: Lapovok, Rimma organization: Institute for Frontier Materials, Deakin University, Waurn Ponds, Victoria 3216, Australia |
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| Keywords | Electrical conductivity Rare earth Mechanical strength Intermetallic particles Atom probe tomography High-pressure torsion |
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| SubjectTerms | Alloys Aluminum base alloys Annealing Atom probe tomography Cerium Dislocation density Earth surface Electrical conductivity Electrical resistivity Heat resistance High-pressure torsion Intermetallic particles Lanthanum Mechanical properties Mechanical strength Morphology Plastic deformation Rare earth Solid solutions Spheroidizing Surface area Tensile stress Thermal resistance Thermal stability Ultrafines |
| Title | Effect of the eutectic Al-(Ce,La) phase morphology on microstructure, mechanical properties, electrical conductivity and heat resistance of Al-4.5(Ce,La) alloy after SPD and subsequent annealing |
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