Novel thiophene symmetrical Schiff base compounds as corrosion inhibitor for mild steel in acidic media

► The aim of the present investigation is to examine the inhibitory action of two Schiff bases. ► Compounds are mixed type (cathodic/anodic) inhibitors. ► Inhibition efficiency (% IE) increases with increasing concentration of compounds. ► Adsorption of compounds on mild steel surface obeys Langmuir...

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Published in:	Corrosion science Vol. 53; no. 4; pp. 1484 - 1488
Main Authors:	Issaadi, S., Douadi, T., Zouaoui, A., Chafaa, S., Khan, M.A., Bouet, G.
Format:	Journal Article
Language:	English
Published:	Kidlington Elsevier Ltd 01-04-2011 Elsevier
Subjects:	A. Hydrochloric acid A. Mild steel Anodic Applied sciences C. Corrosion C. Inhibitor C. Schiff base Carbon steels Corrosion Corrosion environments Corrosion inhibitors Corrosion prevention Electrochemical impedance spectroscopy Exact sciences and technology Inhibition Isotherms Life Sciences Metals. Metallurgy Schiff bases Surface chemistry Thiophenes C. Schiff base C. Inhibitor A. Mild steel C. Corrosion A. Hydrochloric acid Hydrochloric acid Schiff base Corrosion Carbon steel Corrosion protection C Schiff base Acid medium Corrosion inhibitor Inhibitor Mild steel
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Abstract	► The aim of the present investigation is to examine the inhibitory action of two Schiff bases. ► Compounds are mixed type (cathodic/anodic) inhibitors. ► Inhibition efficiency (% IE) increases with increasing concentration of compounds. ► Adsorption of compounds on mild steel surface obeys Langmuir’s isotherm. The inhibiting effect of two Schiff bases on the corrosion of the mild steel (MS) in 1 M HCl has been studied by electrochemical impedance spectroscopy (EIS) and Tafel polarisation measurements. The Schiff bases, 4,4′-bis(3-carboxaldehyde thiophene) diphenyl diimino ether ( L 1) and 4,4′-bis(3-carboxaldehyde thiophene) diphenyl diimino ethane ( L 2), were synthesized using 3-carboxaldehydethiophene and its corresponding amine. Polarisation curves reveal that both compounds are mixed type (cathodic/anodic) inhibitors and inhibition efficiency (% IE) increases with increasing concentration of compounds. It is suggested that their effects depend on their concentrations and the molecular structures. Adsorption of compounds on mild steel surface is spontaneous and obeys Langmuir’s isotherm.
AbstractList	► The aim of the present investigation is to examine the inhibitory action of two Schiff bases. ► Compounds are mixed type (cathodic/anodic) inhibitors. ► Inhibition efficiency (% IE) increases with increasing concentration of compounds. ► Adsorption of compounds on mild steel surface obeys Langmuir’s isotherm. The inhibiting effect of two Schiff bases on the corrosion of the mild steel (MS) in 1 M HCl has been studied by electrochemical impedance spectroscopy (EIS) and Tafel polarisation measurements. The Schiff bases, 4,4′-bis(3-carboxaldehyde thiophene) diphenyl diimino ether ( L 1) and 4,4′-bis(3-carboxaldehyde thiophene) diphenyl diimino ethane ( L 2), were synthesized using 3-carboxaldehydethiophene and its corresponding amine. Polarisation curves reveal that both compounds are mixed type (cathodic/anodic) inhibitors and inhibition efficiency (% IE) increases with increasing concentration of compounds. It is suggested that their effects depend on their concentrations and the molecular structures. Adsorption of compounds on mild steel surface is spontaneous and obeys Langmuir’s isotherm. The inhibiting effect of two Schiff bases on the corrosion of the mild steel (MS) in 1M HCl has been studied by electrochemical impedance spectroscopy (EIS) and Tafel polarisation measurements. The Schiff bases, 4,4'-bis(3-carboxaldehyde thiophene) diphenyl diimino ether (L 1) and 4,4'-bis(3-carboxaldehyde thiophene) diphenyl diimino ethane (L 2), were synthesized using 3-carboxaldehydethiophene and its corresponding amine. Polarisation curves reveal that both compounds are mixed type (cathodic/anodic) inhibitors and inhibition efficiency (% IE) increases with increasing concentration of compounds. It is suggested that their effects depend on their concentrations and the molecular structures. Adsorption of compounds on mild steel surface is spontaneous and obeys Langmuir's isotherm. The inhibiting effect of two Schiff bases on the corrosion of the mild steel (MS) in 1 M HCl has been studied by electrochemical impedance spectroscopy (EIS) and Tafel polarisation measurements. The Schiff bases, 4,4′-bis(3-carboxaldehyde thiophene) diphenyl diimino ether (L1) and 4,4′-bis(3-carboxaldehyde thiophene) diphenyl diimino ethane (L2), were synthesized using 3-carboxaldehydethiophene and its corresponding amine. Polarisation curves reveal that both compounds are mixed type (cathodic/anodic) inhibitors and inhibition efficiency (% IE) increases with increasing concentration of compounds. It is suggested that their effects depend on their concentrations and the molecular structures. Adsorption of compounds on mild steel surface is spontaneous and obeys Langmuir’s isotherm.
Author	Khan, M.A. Bouet, G. Issaadi, S. Zouaoui, A. Chafaa, S. Douadi, T.
Author_xml	– sequence: 1 givenname: S. surname: Issaadi fullname: Issaadi, S. email: issaadi-s@univ-setif.dz organization: Laboratoire d’Électrochimie des Matériaux Moléculaires et Complexes, Faculté des Sciences de l’Ingénieur, Université Ferhat Abbas, DZ-19000 Sétif, Algeria – sequence: 2 givenname: T. surname: Douadi fullname: Douadi, T. organization: Laboratoire d’Électrochimie des Matériaux Moléculaires et Complexes, Faculté des Sciences de l’Ingénieur, Université Ferhat Abbas, DZ-19000 Sétif, Algeria – sequence: 3 givenname: A. surname: Zouaoui fullname: Zouaoui, A. organization: Laboratoire d’Électrochimie des Matériaux Moléculaires et Complexes, Faculté des Sciences de l’Ingénieur, Université Ferhat Abbas, DZ-19000 Sétif, Algeria – sequence: 4 givenname: S. surname: Chafaa fullname: Chafaa, S. organization: Laboratoire d’Électrochimie des Matériaux Moléculaires et Complexes, Faculté des Sciences de l’Ingénieur, Université Ferhat Abbas, DZ-19000 Sétif, Algeria – sequence: 5 givenname: M.A. surname: Khan fullname: Khan, M.A. organization: Université d’Angers, Chimie de coordination, SONAS, EA 921, France – sequence: 6 givenname: G. surname: Bouet fullname: Bouet, G. organization: Université d’Angers, Chimie de coordination, SONAS, EA 921, France
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Keywords	C. Schiff base C. Inhibitor A. Mild steel C. Corrosion A. Hydrochloric acid Hydrochloric acid Schiff base Corrosion Carbon steel Corrosion protection C Schiff base Acid medium Corrosion inhibitor Inhibitor Mild steel
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Snippet	► The aim of the present investigation is to examine the inhibitory action of two Schiff bases. ► Compounds are mixed type (cathodic/anodic) inhibitors. ►... The inhibiting effect of two Schiff bases on the corrosion of the mild steel (MS) in 1M HCl has been studied by electrochemical impedance spectroscopy (EIS)... The inhibiting effect of two Schiff bases on the corrosion of the mild steel (MS) in 1 M HCl has been studied by electrochemical impedance spectroscopy (EIS)...
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SubjectTerms	A. Hydrochloric acid A. Mild steel Anodic Applied sciences C. Corrosion C. Inhibitor C. Schiff base Carbon steels Corrosion Corrosion environments Corrosion inhibitors Corrosion prevention Electrochemical impedance spectroscopy Exact sciences and technology Inhibition Isotherms Life Sciences Metals. Metallurgy Schiff bases Surface chemistry Thiophenes
Title	Novel thiophene symmetrical Schiff base compounds as corrosion inhibitor for mild steel in acidic media
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