Microstructural characteristics of Nd：YAG powders leading to transparent ceramics
We reported on the successful synthesis of the Nd：YAG （Nd：Y3Al5O12） nano-powders by using urea as the precipitant with the microwave assisted homogeneous precipitation （MAHP） method. The different microstructural characteristics of the Nd：YAG nano-powders were affected by the concentrations of （Y3＋＋...
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| Published in: | Journal of rare earths Vol. 29; no. 6; pp. 585 - 591 |
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| Format: | Journal Article |
| Language: | English |
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Elsevier B.V
01-06-2011
State Key Laboratory of Crystal Materials. Shandong University, Jinan 250100, China |
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| Abstract | We reported on the successful synthesis of the Nd：YAG （Nd：Y3Al5O12） nano-powders by using urea as the precipitant with the microwave assisted homogeneous precipitation （MAHP） method. The different microstructural characteristics of the Nd：YAG nano-powders were affected by the concentrations of （Y3＋＋Nd3＋） and Al3＋ （[Y3＋＋Nd3＋]=0.06 mol/L, [Al3＋]=0.1 mol/L）, aging time （6 d） and aging condition （in vessel）. The optimum microstructural characteristics of the high quality Nd：YAG nano-powders leading to transparent Nd：YAG ceramics including the pure YAG phase, the smallest crystallite size, a uniform crystallite size distribution, less density defects, uniform micro-components and the proper molar ratio of （Y3＋＋Nd3＋） and Al3＋ （0.6148） were discussed. |
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| AbstractList | We reported on the successful synthesis of the Nd：YAG （Nd：Y3Al5O12） nano-powders by using urea as the precipitant with the microwave assisted homogeneous precipitation （MAHP） method. The different microstructural characteristics of the Nd：YAG nano-powders were affected by the concentrations of （Y3＋＋Nd3＋） and Al3＋ （[Y3＋＋Nd3＋]=0.06 mol/L, [Al3＋]=0.1 mol/L）, aging time （6 d） and aging condition （in vessel）. The optimum microstructural characteristics of the high quality Nd：YAG nano-powders leading to transparent Nd：YAG ceramics including the pure YAG phase, the smallest crystallite size, a uniform crystallite size distribution, less density defects, uniform micro-components and the proper molar ratio of （Y3＋＋Nd3＋） and Al3＋ （0.6148） were discussed. We reported on the successful synthesis of the Nd:YAG (Nd:Y sub(3Al) sub(5)O sub(12) nano-powders by using urea as the precipitant with the microwave assisted homogeneous precipitation (MAHP) method. The different microstructural characteristics of the Nd:YAG nano-powders were affected by the concentrations of (Y[super]3++Nd[super]3+) and Al[super]3+ ([Y[super]3++Nd[super]3+]=0.06 mol/L, [Al[super]3+]=0.1 mol/L), aging time (6 d) and aging condition (in vessel). The optimum microstructural characteristics of the high quality Nd:YAG nano-powders leading to transparent Nd:YAG ceramics including the pure YAG phase, the smallest crystallite size, a uniform crystallite size distribution, less density defects, uniform micro-components and the proper molar ratio of (Y[super]3++Nd[super]3+) and Al[super]3+ (0.6148) were discussed.) We reported on the successful synthesis of the Nd:YAG (Nd:Y 3Al 5O 12) nano-powders by using urea as the precipitant with the microwave assisted homogeneous precipitation (MAHP) method. The different microstructural characteristics of the Nd:YAG nano-powders were affected by the concentrations of (Y 3++Nd 3+) and Al 3+ ([Y 3++Nd 3+]=0.06 mol/L, [Al 3+]=0.1 mol/L), aging time (6 d) and aging condition (in vessel). The optimum microstructural characteristics of the high quality Nd:YAG nano-powders leading to transparent Nd:YAG ceramics including the pure YAG phase, the smallest crystallite size, a uniform crystallite size distribution, less density defects, uniform micro-components and the proper molar ratio of (Y 3++Nd 3+) and Al 3+ (0.6148) were discussed. TQ174.758; We reported on the successful synthesis of the Nd:YAG (Nd:Y3Al5O12) nano-powders by using urea as the precipitant with the microwave assisted homogeneous precipitation (MAHP) method. The different microstructural characteristics of the Nd:YAG nano-powders were affected by the concentrations of (Y3++Nd3+) and Al3+ ([Y3++Nd3+]=0.06 mol/L, [Al3+]=0.1 mol/L), aging time (6 d) and aging condition (in vessel). The optimum microstructural characteristics of the high quality Nd:YAG nano-powders leading to transparent Nd:YAG ceramics including the pure YAG phase, the smallest crystallite size, a uniform crystallite size distribution, less density defects, uniform micro-components and the proper molar ratio of (Y3++Nd3+) and Al3+ (0.6148) were discussed. |
| Author | 张晓琳 刘铎 刘宏 王继扬 秦海明 桑元华 |
| AuthorAffiliation | State Key Laboratory of Crystal Materials, Shandong University, Jinan 250100, China |
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| CitedBy_id | crossref_primary_10_1155_2014_408910 crossref_primary_10_1016_j_ceramint_2017_06_131 crossref_primary_10_1007_s12034_013_0598_1 crossref_primary_10_7498_aps_63_197801 crossref_primary_10_1016_S1002_0721_14_60087_9 crossref_primary_10_1364_OME_2_000235 crossref_primary_10_1016_S1002_0721_12_60106_9 crossref_primary_10_1016_S1002_0721_12_60310_X crossref_primary_10_1016_S1002_0721_12_60250_6 |
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| Copyright | 2011 The Chinese Society of Rare Earths Copyright © Wanfang Data Co. Ltd. All Rights Reserved. |
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| Keywords | chemical synthesis X-ray diffraction ceramics defects rare earths |
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| Notes | 11-2788/TF We reported on the successful synthesis of the Nd：YAG （Nd：Y3Al5O12） nano-powders by using urea as the precipitant with the microwave assisted homogeneous precipitation （MAHP） method. The different microstructural characteristics of the Nd：YAG nano-powders were affected by the concentrations of （Y3＋＋Nd3＋） and Al3＋ （[Y3＋＋Nd3＋]=0.06 mol/L, [Al3＋]=0.1 mol/L）, aging time （6 d） and aging condition （in vessel）. The optimum microstructural characteristics of the high quality Nd：YAG nano-powders leading to transparent Nd：YAG ceramics including the pure YAG phase, the smallest crystallite size, a uniform crystallite size distribution, less density defects, uniform micro-components and the proper molar ratio of （Y3＋＋Nd3＋） and Al3＋ （0.6148） were discussed. ZHANG Xiaolin , LIU Duo , LIU Hong , WANG Jiyang , QIN Haiming , SANG Yuanhua （State Key Laboratory of Crystal Materials, Shandong University, Jinan 250100, China） ceramics; chemical synthesis; X-ray diffraction; defects; rare earths ObjectType-Article-2 SourceType-Scholarly Journals-1 ObjectType-Feature-1 content type line 23 |
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| PublicationYear | 2011 |
| Publisher | Elsevier B.V State Key Laboratory of Crystal Materials. Shandong University, Jinan 250100, China |
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| Snippet | We reported on the successful synthesis of the Nd：YAG （Nd：Y3Al5O12） nano-powders by using urea as the precipitant with the microwave assisted homogeneous... We reported on the successful synthesis of the Nd:YAG (Nd:Y 3Al 5O 12) nano-powders by using urea as the precipitant with the microwave assisted homogeneous... We reported on the successful synthesis of the Nd:YAG (Nd:Y sub(3Al) sub(5)O sub(12) nano-powders by using urea as the precipitant with the microwave assisted... TQ174.758; We reported on the successful synthesis of the Nd:YAG (Nd:Y3Al5O12) nano-powders by using urea as the precipitant with the microwave assisted... |
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| SubjectTerms | Ceramics chemical synthesis Crystallites defects Density Microstructure Nanocomposites Nanomaterials Nanostructure Nd：YAG激光 Rare earth metals rare earths X-ray diffraction Y3Al5O12 均相沉淀 微观结构特征 纳米粉体 组织 老化时间 陶瓷粉末 |
| Title | Microstructural characteristics of Nd：YAG powders leading to transparent ceramics |
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