Cyclooligosiloxanolate cluster complexes of transition metals and lanthanides

Cyclooligosiloxanolate complexes of higher valent transition metals and lanthanides were synthesized and characterized by single-crystal X-ray diffraction experiments, spectra, cyclic voltammetry, conductivity and magnetic behaviour. These complexes are sandwich-type clusters containing assemblies o...

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Published in:	Journal of molecular catalysis. A, Chemical Vol. 107; no. 1; pp. 313 - 321
Main Authors:	Zucchi, C., Shchegolikhina, O.I., Borsari, M., Cornia, A., Gavioli, G., Fabretti, A.C., Rentschler, E., Gatteschi, D., Ugo, R., Psaro, R., Pozdniakova, Yu.A., Lindeman, S.V., Zhdanov, A.A., Pályi, G.
Format:	Journal Article Conference Proceeding
Language:	English
Published:	Amsterdam Elsevier B.V 01-05-1996 Elsevier
Subjects:	Chemistry Cluster complexes Condensed matter: structure, mechanical and thermal properties Coordination compounds Cyclooligosiloxanolate clusters Exact sciences and technology Inorganic chemistry and origins of life Inorganic compounds Lanthanides Metal complexes Physics Preparations and properties Siloxanolate Structure of solids and liquids; crystallography Structure of specific crystalline solids Transition metals Siloxanolate Transition metals Cluster complexes Lanthanides Cyclooligosiloxanolate clusters Molecular structure Organic ligand Organic siloxane Complex cluster Anionic complex Tetranuclear complex Gadolinium Complexes Experimental study X ray diffraction Oxo complex Sodium Compounds Cyclic voltammetry Mu complex Lanthanide Complexes Electrochemical reaction Crystalline structure
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Abstract	Cyclooligosiloxanolate complexes of higher valent transition metals and lanthanides were synthesized and characterized by single-crystal X-ray diffraction experiments, spectra, cyclic voltammetry, conductivity and magnetic behaviour. These complexes are sandwich-type clusters containing assemblies of 4 to 8 metals between siloxanolate ligand ‘layers’. A high degree of electron delocalization in the metal containing fragment of these complexes is detected by electrochemical and magnetic measurements. The synthesis, crystal and molecular structure determined by X-ray diffraction of Na 6{[C 6H 5SiO 2) 8] 2Gd 4( μ 4-O)} is reported.
AbstractList	Cyclooligosiloxanolate complexes of higher valent transition metals and lanthanides were synthesized and characterized by single-crystal X-ray diffraction experiments, spectra, cyclic voltammetry, conductivity and magnetic behaviour. These complexes are sandwich-type clusters containing assemblies of 4 to 8 metals between siloxanolate ligand ‘layers’. A high degree of electron delocalization in the metal containing fragment of these complexes is detected by electrochemical and magnetic measurements. The synthesis, crystal and molecular structure determined by X-ray diffraction of Na 6{[C 6H 5SiO 2) 8] 2Gd 4( μ 4-O)} is reported.
Author	Rentschler, E. Pályi, G. Gatteschi, D. Ugo, R. Shchegolikhina, O.I. Borsari, M. Cornia, A. Zucchi, C. Psaro, R. Lindeman, S.V. Fabretti, A.C. Gavioli, G. Pozdniakova, Yu.A. Zhdanov, A.A.
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Copyright	1996 1996 INIST-CNRS
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Keywords	Siloxanolate Transition metals Cluster complexes Lanthanides Cyclooligosiloxanolate clusters Molecular structure Organic ligand Organic siloxane Complex cluster Anionic complex Tetranuclear complex Gadolinium Complexes Experimental study X ray diffraction Oxo complex Sodium Compounds Cyclic voltammetry Mu complex Lanthanide Complexes Electrochemical reaction Crystalline structure
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Snippet	Cyclooligosiloxanolate complexes of higher valent transition metals and lanthanides were synthesized and characterized by single-crystal X-ray diffraction...
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SubjectTerms	Chemistry Cluster complexes Condensed matter: structure, mechanical and thermal properties Coordination compounds Cyclooligosiloxanolate clusters Exact sciences and technology Inorganic chemistry and origins of life Inorganic compounds Lanthanides Metal complexes Physics Preparations and properties Siloxanolate Structure of solids and liquids; crystallography Structure of specific crystalline solids Transition metals
Title	Cyclooligosiloxanolate cluster complexes of transition metals and lanthanides
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