Flexible all-fiber electrospun supercapacitor
We present an all-fiber flexible supercapacitor with composite nanofiber electrodes made via electrospinning and an electrospun separator. With the addition of manganese acetylacetonate (MnACAC) to polyacrylonitrile (PAN) as a precursor for the electrospinning process and subsequent heat treatment,...
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| Published in: | Journal of power sources Vol. 384; pp. 264 - 269 |
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| Main Authors: | , , , , , , |
| Format: | Journal Article |
| Language: | English |
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Elsevier B.V
30-04-2018
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| Abstract | We present an all-fiber flexible supercapacitor with composite nanofiber electrodes made via electrospinning and an electrospun separator. With the addition of manganese acetylacetonate (MnACAC) to polyacrylonitrile (PAN) as a precursor for the electrospinning process and subsequent heat treatment, the performance of pure PAN supercapacitors was improved from 90 F g−1 to 200 F g−1 (2.5 mV s−1) with possible mass loadings of MnACAC demonstrated as high as 40 wt%. X-ray diffraction measurements showed that after thermal treatment, the MnACAC was converted to MnO, meanwile, the thermal decomposition of MnACAC increased the graphitic degree of the carbonised PAN. Scanning electron microscopy and image processing showed that static electrospinning of pure PAN and PAN-Mn resulted in fiber diameters of 460 nm and 480 nm respectively after carbonisation. Further analysis showed that the fiber orientation exhibited a slight bias which was amplified with the addition of MnACAC. Use of focused ion beam scanning electron microscopy tomography also showed that MnO particles were evenly distributed through the fiber at low MnACAC concentrations, while at a 40 wt% loading the MnO particles were also visible on the surface. Comparison of the electrospun separators showed improved performance relative to a commercial Celgard separator (200 F g−1 vs 141 F g−1).
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•Electrospun all-fiber flexible supercapacitor with nanofiber electrodes/separator.•Increased graphitic degree with the addition of MnACAC and thermal decomposition.•Enhanced capacitive performance with the addition of MnO.•Quantified nanofiber alignment and increased bias with MnO over undoped fibers.•FIBSEM tomography of nanofibers showing MnO disitribution in carbon nanofibers. |
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| AbstractList | We present an all-fiber flexible supercapacitor with composite nanofiber electrodes made via electrospinning and an electrospun separator. With the addition of manganese acetylacetonate (MnACAC) to polyacrylonitrile (PAN) as a precursor for the electrospinning process and subsequent heat treatment, the performance of pure PAN supercapacitors was improved from 90 F g−1 to 200 F g−1 (2.5 mV s−1) with possible mass loadings of MnACAC demonstrated as high as 40 wt%. X-ray diffraction measurements showed that after thermal treatment, the MnACAC was converted to MnO, meanwile, the thermal decomposition of MnACAC increased the graphitic degree of the carbonised PAN. Scanning electron microscopy and image processing showed that static electrospinning of pure PAN and PAN-Mn resulted in fiber diameters of 460 nm and 480 nm respectively after carbonisation. Further analysis showed that the fiber orientation exhibited a slight bias which was amplified with the addition of MnACAC. Use of focused ion beam scanning electron microscopy tomography also showed that MnO particles were evenly distributed through the fiber at low MnACAC concentrations, while at a 40 wt% loading the MnO particles were also visible on the surface. Comparison of the electrospun separators showed improved performance relative to a commercial Celgard separator (200 F g−1 vs 141 F g−1).
[Display omitted]
•Electrospun all-fiber flexible supercapacitor with nanofiber electrodes/separator.•Increased graphitic degree with the addition of MnACAC and thermal decomposition.•Enhanced capacitive performance with the addition of MnO.•Quantified nanofiber alignment and increased bias with MnO over undoped fibers.•FIBSEM tomography of nanofibers showing MnO disitribution in carbon nanofibers. |
| Author | Brandon, Nigel P. Naylor Marlow, Max Cooper, Samuel J. Chen, Xiaolong Song, Bowen Wu, Billy Liu, Xinhua |
| Author_xml | – sequence: 1 givenname: Xinhua orcidid: 0000-0002-4111-7235 surname: Liu fullname: Liu, Xinhua organization: Dyson School of Design Engineering, Imperial College London, United Kingdom – sequence: 2 givenname: Max surname: Naylor Marlow fullname: Naylor Marlow, Max organization: Dyson School of Design Engineering, Imperial College London, United Kingdom – sequence: 3 givenname: Samuel J. surname: Cooper fullname: Cooper, Samuel J. organization: Dyson School of Design Engineering, Imperial College London, United Kingdom – sequence: 4 givenname: Bowen surname: Song fullname: Song, Bowen organization: Earth Science and Engineering, Imperial College London, United Kingdom – sequence: 5 givenname: Xiaolong surname: Chen fullname: Chen, Xiaolong organization: Dyson School of Design Engineering, Imperial College London, United Kingdom – sequence: 6 givenname: Nigel P. surname: Brandon fullname: Brandon, Nigel P. organization: Earth Science and Engineering, Imperial College London, United Kingdom – sequence: 7 givenname: Billy orcidid: 0000-0003-3963-4900 surname: Wu fullname: Wu, Billy email: billy.wu@imperial.ac.uk organization: Dyson School of Design Engineering, Imperial College London, United Kingdom |
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| Keywords | Electrospinning Supercapacitor Nanofiber Manganese oxide Separator |
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