Kinetic analysis of nonisothermal degradation of acrylonitrile-butadiene/ethylene-propylene-diene rubber blends reinforced with carbon black filler
The nonisothermal degradation process of acrylonitrile–butadiene/ethylene–propylene–diene rubber blends reinforced with carbon black filler was investigated with thermogravimetric analysis (TGA) and derivative thermogravimetry (DTG), using the different calculation procedures. Using different isocon...
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| Published in: | Polymer composites Vol. 33; no. 7; pp. 1233 - 1243 |
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| Main Authors: | , , , , |
| Format: | Journal Article |
| Language: | English |
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| Abstract | The nonisothermal degradation process of acrylonitrile–butadiene/ethylene–propylene–diene rubber blends reinforced with carbon black filler was investigated with thermogravimetric analysis (TGA) and derivative thermogravimetry (DTG), using the different calculation procedures. Using different isoconversional methods, it was found that the degradation of the 50 phr loaded carbon black in NBR/EPDM (80/20) blend represents the complex process, where exists the conversion region with a constant value of the apparent activation energy (Ea). It was found that the degradation process of the carbon black‐loaded polymer blend under nitrogen atmosphere, can be described by the three‐(D3) dimensional diffusion mechanism. Good agreement was observed between the experimental and calculated differential (rate) conversion curves, for the investigated degradation process. It was established that the considered polymer blend which have high contents of the carbon black (50 phr carbon black), shows very strong self‐protective behavior (i.e., in the formation of a protective barrier). POLYM. COMPOS., 2012. © 2012 Society of Plastics Engineers |
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| AbstractList | The nonisothermal degradation process of acrylonitrile–butadiene/ethylene–propylene–diene rubber blends reinforced with carbon black filler was investigated with thermogravimetric analysis (TGA) and derivative thermogravimetry (DTG), using the different calculation procedures. Using different isoconversional methods, it was found that the degradation of the 50 phr loaded carbon black in NBR/EPDM (80/20) blend represents the complex process, where exists the conversion region with a constant value of the apparent activation energy (
E
a
). It was found that the degradation process of the carbon black‐loaded polymer blend under nitrogen atmosphere, can be described by the three‐(D3) dimensional diffusion mechanism. Good agreement was observed between the experimental and calculated differential (rate) conversion curves, for the investigated degradation process. It was established that the considered polymer blend which have high contents of the carbon black (50 phr carbon black), shows very strong self‐protective behavior (i.e., in the formation of a protective barrier). POLYM. COMPOS., 2012. © 2012 Society of Plastics Engineers The nonisothermal degradation process of acrylonitrile–butadiene/ethylene–propylene–diene rubber blends reinforced with carbon black filler was investigated with thermogravimetric analysis (TGA) and derivative thermogravimetry (DTG), using the different calculation procedures. Using different isoconversional methods, it was found that the degradation of the 50 phr loaded carbon black in NBR/EPDM (80/20) blend represents the complex process, where exists the conversion region with a constant value of the apparent activation energy (Ea). It was found that the degradation process of the carbon black‐loaded polymer blend under nitrogen atmosphere, can be described by the three‐(D3) dimensional diffusion mechanism. Good agreement was observed between the experimental and calculated differential (rate) conversion curves, for the investigated degradation process. It was established that the considered polymer blend which have high contents of the carbon black (50 phr carbon black), shows very strong self‐protective behavior (i.e., in the formation of a protective barrier). POLYM. COMPOS., 2012. © 2012 Society of Plastics Engineers The nonisothermal degradation process of acrylonitrile-butadiene/ethylene-propylene-diene rubber blends reinforced with carbon black filler was investigated with thermogravimetric analysis (TGA) and derivative thermogravimetry (DTG), using the different calculation procedures. Using different isoconversional methods, it was found that the degradation of the 50 phr loaded carbon black in NBR/EPDM (80/20) blend represents the complex process, where exists the conversion region with a constant value of the apparent activation energy (Ea). It was found that the degradation process of the carbon black-loaded polymer blend under nitrogen atmosphere, can be described by the three-(D3) dimensional diffusion mechanism. Good agreement was observed between the experimental and calculated differential (rate) conversion curves, for the investigated degradation process. It was established that the considered polymer blend which have high contents of the carbon black (50 phr carbon black), shows very strong self-protective behavior (i.e., in the formation of a protective barrier). POLYM. COMPOS., 2012. © 2012 Society of Plastics Engineers [PUBLICATION ABSTRACT] |
| Author | Marinović-Cincović, Milena Jovanović, Vojislav Janković, Bojan Samaržija-Jovanović, Suzana Marković, Gordana |
| Author_xml | – sequence: 1 givenname: Bojan surname: JANKOVIC fullname: JANKOVIC, Bojan organization: Faculty of Physical Chemistry, Department for Dynamics and Matter Structure, University of Belgrade, Studentski trg 12-16, P.O. Box 137, 11001 Belgrade, Serbia – sequence: 2 givenname: Milena surname: MARINOVIC-CINCOVIC fullname: MARINOVIC-CINCOVIC, Milena organization: Institute of Nuclear Science Vinča, University of Belgrade, Laboratory for Radiation Chemistry and Physics Gamma, Mike Petrovića Alasa 12-14, P.O. Box 552, 11001 Belgrade, Serbia – sequence: 3 givenname: Vojislav surname: JOVANOVIC fullname: JOVANOVIC, Vojislav organization: Faculty of Natural Science and Mathematics, Department of Chemistry, University of Priština, Lole Ribara 29, 38220 Kosovska Mitrovica, Serbia – sequence: 4 givenname: Suzana surname: SAMARZIJA-JOVANOVIC fullname: SAMARZIJA-JOVANOVIC, Suzana organization: Faculty of Natural Science and Mathematics, Department of Chemistry, University of Priština, Lole Ribara 29, 38220 Kosovska Mitrovica, Serbia – sequence: 5 givenname: Gordana surname: MARKOVIC fullname: MARKOVIC, Gordana organization: Tigar, Quality Department, Technical rubber goods, Nikole Pašića 213, 18300 Pirot, Serbia |
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| Cites_doi | 10.1016/j.polymer.2006.04.024 10.1007/s10973-009-0131-3 10.1002/polc.5070060121 10.1016/j.polymdegradstab.2006.03.001 10.1080/014423598230108 10.1016/j.progsolidstchem.2005.11.022 10.1016/0141-3910(86)90028-5 10.1016/S0040-6031(97)00482-6 10.1016/j.polymdegradstab.2004.01.017 10.1016/j.eurpolymj.2009.10.002 10.1016/0040-6031(92)85118-F 10.1038/201068a0 10.1007/s00289-006-0706-0 10.1016/j.polymer.2005.06.067 10.1016/S1573-4374(08)80016-7 10.1016/S0141-3910(97)00066-9 10.1007/BF01903696 10.1016/0165-2370(94)00791-8 10.1016/0301-0104(94)00402-V 10.1016/j.polymdegradstab.2004.09.013 10.1039/a606395k 10.1002/pen.20396 10.1016/0032-3861(95)91441-9 10.5254/1.3534979 10.1016/S0040-6031(97)00046-4 10.1021/jp0022205 10.5254/1.3547616 10.1002/app.21111 10.1177/0307174X0202900310 10.3144/expresspolymlett.2008.18 10.1002/pc.20328 10.1016/j.polymer.2005.11.037 10.1002/app.23773 10.1021/ac60131a045 10.1016/S0141-3910(00)00115-4 10.1016/0040-6031(93)80506-6 |
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| Issue | 7 |
| Keywords | EPDM rubber Polymer blends Carbon black Ethylene propylene rubber Polymer Kinetics Nitrile rubber Activation energy Mechanism |
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| Snippet | The nonisothermal degradation process of acrylonitrile–butadiene/ethylene–propylene–diene rubber blends reinforced with carbon black filler was investigated... The nonisothermal degradation process of acrylonitrile-butadiene/ethylene-propylene-diene rubber blends reinforced with carbon black filler was investigated... |
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| SubjectTerms | Applied sciences Composites Exact sciences and technology Forms of application and semi-finished materials Laminates Physicochemistry of polymers Polymer industry, paints, wood Technology of polymers |
| Title | Kinetic analysis of nonisothermal degradation of acrylonitrile-butadiene/ethylene-propylene-diene rubber blends reinforced with carbon black filler |
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