Simultaneous determination of iron, copper and zinc concentrations in skin phantoms using XRF spectrometry
X‐ray fluorescence analysis was used to determine the concentrations of iron, copper and zinc in skin phantoms. The system used consisted of a high‐output tungsten target x‐ray tube and a germanium secondary target, the fluorescence from which was used to excite the elements in the sample. Calibrati...
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| Published in: | X-ray spectrometry Vol. 31; no. 1; pp. 47 - 52 |
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01-01-2002
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| Abstract | X‐ray fluorescence analysis was used to determine the concentrations of iron, copper and zinc in skin phantoms. The system used consisted of a high‐output tungsten target x‐ray tube and a germanium secondary target, the fluorescence from which was used to excite the elements in the sample. Calibration models were constructed in order to allow quantitative predictions of metal concentrations, with spectral analysis performed using the Marquardt method of non‐linear least‐squares fitting. For an acquisition time of 2000 s, minimum detectable concentrations of <10 µg g−1 for iron and <5 µg g−1 for copper and zinc were measured. These values are comparable to the levels encountered in healthy human skin. Copyright © 2002 John Wiley & Sons, Ltd. |
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| AbstractList | X‐ray fluorescence analysis was used to determine the concentrations of iron, copper and zinc in skin phantoms. The system used consisted of a high‐output tungsten target x‐ray tube and a germanium secondary target, the fluorescence from which was used to excite the elements in the sample. Calibration models were constructed in order to allow quantitative predictions of metal concentrations, with spectral analysis performed using the Marquardt method of non‐linear least‐squares fitting. For an acquisition time of 2000 s, minimum detectable concentrations of <10 µg g
−1
for iron and <5 µg g
−1
for copper and zinc were measured. These values are comparable to the levels encountered in healthy human skin. Copyright © 2002 John Wiley & Sons, Ltd. X‐ray fluorescence analysis was used to determine the concentrations of iron, copper and zinc in skin phantoms. The system used consisted of a high‐output tungsten target x‐ray tube and a germanium secondary target, the fluorescence from which was used to excite the elements in the sample. Calibration models were constructed in order to allow quantitative predictions of metal concentrations, with spectral analysis performed using the Marquardt method of non‐linear least‐squares fitting. For an acquisition time of 2000 s, minimum detectable concentrations of <10 µg g−1 for iron and <5 µg g−1 for copper and zinc were measured. These values are comparable to the levels encountered in healthy human skin. Copyright © 2002 John Wiley & Sons, Ltd. |
| Author | Farquharson, Michael J. Bagshaw, Andrew P. |
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| Cites_doi | 10.1002/(SICI)1097-4539(199805/06)27:3<198::AID-XRS265>3.0.CO;2-B 10.1002/(SICI)1097-0215(19981209)78:6<720::AID-IJC9>3.0.CO;2-F 10.1002/jso.2930460311 10.1023/A:1006757424682 10.1002/(SICI)1097-4539(199907/08)28:4<270::AID-XRS350>3.0.CO;2-U 10.1007/BF00205193 10.2340/0001555560295299 10.1046/j.1523-1755.1999.055Suppl.69022.x 10.1088/0031-9155/45/5/320 10.1097/00004836-199907000-00007 10.1007/BF02916818 10.1016/S0969-8043(97)00264-9 10.1137/0111030 10.1111/j.1365-4362.1986.tb03449.x 10.1088/0031-9155/42/6/008 10.1111/j.1572-0241.1999.851_w.x 10.2340/0001555553473476 10.1088/0031-9155/30/9/005 10.1088/0031-9155/44/4/011 10.1007/BF02789296 10.2340/0001555553477480 10.1088/0031-9155/40/3/006 10.1016/S0168-583X(98)01057-X 10.1039/an9810601168 10.1088/0031-9155/44/5/012 10.1111/j.1749-6632.1990.tb24369.x 10.1118/1.1637303 10.1007/BF02783340 10.1159/000250254 |
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Exp. Clin. Cancer Res. contributor: fullname: Jayadeep A |
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| Title | Simultaneous determination of iron, copper and zinc concentrations in skin phantoms using XRF spectrometry |
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