Green Synthesis of Copper Nanoparticles Using Cotton

Copper nanoparticles (CuNP) were obtained by a green synthesis method using cotton textile fibers and water as solvent, avoiding the use of toxic reducing agents. The new synthesis method is environmentally friendly, inexpensive, and can be implemented on a larger scale. This method showed the cellu...

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Published in:	Polymers Vol. 13; no. 12; p. 1906
Main Authors:	Pérez-Alvarez, Marissa, Cadenas-Pliego, Gregorio, Pérez-Camacho, Odilia, Comparán-Padilla, Víctor E., Cabello-Alvarado, Christian J., Saucedo-Salazar, Esmeralda
Format:	Journal Article
Language:	English
Published:	Basel MDPI AG 08-06-2021 MDPI
Subjects:	Antimicrobial agents Cellulose Chemical vapor deposition Copper Cotton COVID-19 Fourier transforms Functional groups Methods Nanocomposites Nanoparticles Oxidation Reducing agents Severe acute respiratory syndrome coronavirus 2 Spectrum analysis Stabilizers (agents) Stainless steel Textile fibers United States > US
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Abstract	Copper nanoparticles (CuNP) were obtained by a green synthesis method using cotton textile fibers and water as solvent, avoiding the use of toxic reducing agents. The new synthesis method is environmentally friendly, inexpensive, and can be implemented on a larger scale. This method showed the cellulose capacity as a reducing and stabilizing agent for synthetizing Cellulose–Copper nanoparticles (CCuNP). Nanocomposites based on CCuNP were characterized by XRD, TGA, FTIR and DSC. Functional groups present in the CCuNP were identified by FTIR analysis, and XRD patterns disclosed that nanoparticles correspond to pure metallic Cu°, and their sizes are at a range of 13–35 nm. Results demonstrated that CuNPs produced by the new method were homogeneously distributed on the entire surface of the textile fiber, obtaining CCuNP nanocomposites with different copper wt%. Thus, CuNPs obtained by this method are very stable to oxidation and can be stored for months. Characterization studies disclose that the cellulose crystallinity index (CI) is modified in relation to the reaction conditions, and its chemical structure is destroyed when nanocomposites with high copper contents are synthesized. The formation of CuO nanoparticles was confirmed as a by-product, through UV spectroscopy, in the absorbance range of 300–350 nm.
AbstractList	Copper nanoparticles (CuNP) were obtained by a green synthesis method using cotton textile fibers and water as solvent, avoiding the use of toxic reducing agents. The new synthesis method is environmentally friendly, inexpensive, and can be implemented on a larger scale. This method showed the cellulose capacity as a reducing and stabilizing agent for synthetizing Cellulose–Copper nanoparticles (CCuNP). Nanocomposites based on CCuNP were characterized by XRD, TGA, FTIR and DSC. Functional groups present in the CCuNP were identified by FTIR analysis, and XRD patterns disclosed that nanoparticles correspond to pure metallic Cu°, and their sizes are at a range of 13–35 nm. Results demonstrated that CuNPs produced by the new method were homogeneously distributed on the entire surface of the textile fiber, obtaining CCuNP nanocomposites with different copper wt%. Thus, CuNPs obtained by this method are very stable to oxidation and can be stored for months. Characterization studies disclose that the cellulose crystallinity index (CI) is modified in relation to the reaction conditions, and its chemical structure is destroyed when nanocomposites with high copper contents are synthesized. The formation of CuO nanoparticles was confirmed as a by-product, through UV spectroscopy, in the absorbance range of 300–350 nm.
Author	Pérez-Camacho, Odilia Cabello-Alvarado, Christian J Comparán-Padilla, Víctor E Pérez-Alvarez, Marissa Saucedo-Salazar, Esmeralda Cadenas-Pliego, Gregorio
AuthorAffiliation	2 CONACYT-Centro de Investigación y de Innovación del Estado de Tlaxcala, Tlaxcala 90000, Mexico 1 Centro de Investigación en Química Aplicada, Departamento de Síntesis de Polímeros, Saltillo 25294, Coahuila, Mexico; odilia.perez@ciqa.edu.mx (O.P.-C.); victor.comparan@ciqa.edu.mx (V.E.C.-P.); christian.cabello@ciqa.edu.mx (C.J.C.-A.); esmeralda.saucedo@ciqa.edu.mx (E.S.-S.)
AuthorAffiliation_xml	– name: 2 CONACYT-Centro de Investigación y de Innovación del Estado de Tlaxcala, Tlaxcala 90000, Mexico – name: 1 Centro de Investigación en Química Aplicada, Departamento de Síntesis de Polímeros, Saltillo 25294, Coahuila, Mexico; odilia.perez@ciqa.edu.mx (O.P.-C.); victor.comparan@ciqa.edu.mx (V.E.C.-P.); christian.cabello@ciqa.edu.mx (C.J.C.-A.); esmeralda.saucedo@ciqa.edu.mx (E.S.-S.)
Author_xml	– sequence: 1 givenname: Marissa orcidid: 0000-0002-1276-4230 surname: Pérez-Alvarez fullname: Pérez-Alvarez, Marissa – sequence: 2 givenname: Gregorio orcidid: 0000-0002-2692-4995 surname: Cadenas-Pliego fullname: Cadenas-Pliego, Gregorio – sequence: 3 givenname: Odilia surname: Pérez-Camacho fullname: Pérez-Camacho, Odilia – sequence: 4 givenname: Víctor E. orcidid: 0000-0002-8418-2387 surname: Comparán-Padilla fullname: Comparán-Padilla, Víctor E. – sequence: 5 givenname: Christian J. orcidid: 0000-0002-9559-0976 surname: Cabello-Alvarado fullname: Cabello-Alvarado, Christian J. – sequence: 6 givenname: Esmeralda orcidid: 0000-0002-9985-1897 surname: Saucedo-Salazar fullname: Saucedo-Salazar, Esmeralda
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Snippet	Copper nanoparticles (CuNP) were obtained by a green synthesis method using cotton textile fibers and water as solvent, avoiding the use of toxic reducing...
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SubjectTerms	Antimicrobial agents Cellulose Chemical vapor deposition Copper Cotton COVID-19 Fourier transforms Functional groups Methods Nanocomposites Nanoparticles Oxidation Reducing agents Severe acute respiratory syndrome coronavirus 2 Spectrum analysis Stabilizers (agents) Stainless steel Textile fibers
Title	Green Synthesis of Copper Nanoparticles Using Cotton
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