Desktop fast-field cycling nuclear magnetic resonance relaxometer
In this paper a new type of Fast Field Cycling (FFC) Nuclear Magnetic Resonance (NMR) relaxometer with low power consumption (200 W) and cycle to cycle field stability better than 10 −4 is described. The new high-permeability magnet was designed to allow for good magnetic field homogeneity and allow...
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| Published in: | Solid state nuclear magnetic resonance Vol. 38; no. 1; pp. 36 - 43 |
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| Main Authors: | , , , |
| Format: | Journal Article |
| Language: | English |
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01-07-2010
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| Abstract | In this paper a new type of Fast Field Cycling (FFC) Nuclear Magnetic Resonance (NMR) relaxometer with low power consumption (200
W) and cycle to cycle field stability better than 10
−4 is described. The new high-permeability magnet was designed to allow for good magnetic field homogeneity and allows for the sample rotation around an axis perpendicular to magnetic field, operating with magnetic fields between 0 and 0.21
T. The power supply of the new relaxometer was specially developed in order to have steady state accurate currents and allow for magnetic field switching times less than 3
ms. Additional control circuits were developed and included to compensate the Earth magnetic field component parallel to the field axis and to compensate for parasitic currents. The main aspects of the developed circuits together with some calibrating experimental results using the liquid crystal compounds 5CB and 8CB are presented and discussed. |
|---|---|
| AbstractList | In this paper a new type of Fast Field Cycling (FFC) Nuclear Magnetic Resonance (NMR) relaxometer with low power consumption (200 W) and cycle to cycle field stability better than 10 super(-4) is described. The new high-permeability magnet was designed to allow for good magnetic field homogeneity and allows for the sample rotation around an axis perpendicular to magnetic field, operating with magnetic fields between 0 and 0.21 T. The power supply of the new relaxometer was specially developed in order to have steady state accurate currents and allow for magnetic field switching times less than 3 ms. Additional control circuits were developed and included to compensate the Earth magnetic field component parallel to the field axis and to compensate for parasitic currents. The main aspects of the developed circuits together with some calibrating experimental results using the liquid crystal compounds 5CB and 8CB are presented and discussed. In this paper a new type of Fast Field Cycling (FFC) Nuclear Magnetic Resonance (NMR) relaxometer with low power consumption (200W) and cycle to cycle field stability better than 10(-4) is described. The new high-permeability magnet was designed to allow for good magnetic field homogeneity and allows for the sample rotation around an axis perpendicular to magnetic field, operating with magnetic fields between 0 and 0.21T. The power supply of the new relaxometer was specially developed in order to have steady state accurate currents and allow for magnetic field switching times less than 3ms. Additional control circuits were developed and included to compensate the Earth magnetic field component parallel to the field axis and to compensate for parasitic currents. The main aspects of the developed circuits together with some calibrating experimental results using the liquid crystal compounds 5CB and 8CB are presented and discussed. In this paper a new type of Fast Field Cycling (FFC) Nuclear Magnetic Resonance (NMR) relaxometer with low power consumption (200 W) and cycle to cycle field stability better than 10 −4 is described. The new high-permeability magnet was designed to allow for good magnetic field homogeneity and allows for the sample rotation around an axis perpendicular to magnetic field, operating with magnetic fields between 0 and 0.21 T. The power supply of the new relaxometer was specially developed in order to have steady state accurate currents and allow for magnetic field switching times less than 3 ms. Additional control circuits were developed and included to compensate the Earth magnetic field component parallel to the field axis and to compensate for parasitic currents. The main aspects of the developed circuits together with some calibrating experimental results using the liquid crystal compounds 5CB and 8CB are presented and discussed. |
| Author | José Sebastião, Pedro Mesquita Sousa, Duarte Domingos Marques, Gil Manuel Cascais, José |
| Author_xml | – sequence: 1 givenname: Duarte surname: Mesquita Sousa fullname: Mesquita Sousa, Duarte email: duarte.sousa@ist.utl.pt organization: DEEC AC-Energia /CIEEE, Instituto Superior Técnico, TU Lisbon—Av. Rovisco Pais, 1049-001 Lisboa, Portugal – sequence: 2 givenname: Gil surname: Domingos Marques fullname: Domingos Marques, Gil organization: DEEC AC-Energia /CIEEE, Instituto Superior Técnico, TU Lisbon—Av. Rovisco Pais, 1049-001 Lisboa, Portugal – sequence: 3 givenname: José surname: Manuel Cascais fullname: Manuel Cascais, José organization: DEEC AC-Energia /CIEEE, Instituto Superior Técnico, TU Lisbon—Av. Rovisco Pais, 1049-001 Lisboa, Portugal – sequence: 4 givenname: Pedro surname: José Sebastião fullname: José Sebastião, Pedro organization: Centro de Física da Matéria Condensada, Av. Prof. Gama Pinto 2, 1649-003 Lisboa, Portugal and TU Lisbon, IST/DF, Av. Rovisco Pais, 1049-001 Lisboa, Portugal |
| BackLink | https://www.ncbi.nlm.nih.gov/pubmed/20688489$$D View this record in MEDLINE/PubMed |
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| Cites_doi | 10.1006/jmre.2000.2279 10.1016/j.pnmrs.2004.03.002 10.1063/1.1147024 10.1016/0079-6565(86)80004-8 10.1103/PhysRevE.72.061702 10.1109/20.582639 10.1007/BF03162287 10.1016/j.ssnmr.2003.03.026 10.1109/20.825817 10.1063/1.1709950 10.1109/TMAG.2002.804803 10.1063/1.1610785 10.1103/PhysRevE.76.051708 10.1109/20.619678 10.1006/jmrb.1996.0088 10.1080/02678299608031148 10.1016/0022-2364(88)90158-8 |
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| Keywords | NMR relaxometer Spin–lattice relaxation Relaxometry Field-cycling NMR |
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| Snippet | In this paper a new type of Fast Field Cycling (FFC) Nuclear Magnetic Resonance (NMR) relaxometer with low power consumption (200
W) and cycle to cycle field... In this paper a new type of Fast Field Cycling (FFC) Nuclear Magnetic Resonance (NMR) relaxometer with low power consumption (200W) and cycle to cycle field... In this paper a new type of Fast Field Cycling (FFC) Nuclear Magnetic Resonance (NMR) relaxometer with low power consumption (200 W) and cycle to cycle field... |
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| SubjectTerms | Calibration Circuits Cycles Field-cycling NMR Homogeneity Magnetic fields NMR relaxometer Nuclear magnetic resonance Power consumption Relaxometry Spin–lattice relaxation Steady state |
| Title | Desktop fast-field cycling nuclear magnetic resonance relaxometer |
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