Enantiomeric Distribution Studies of Linalool and Linalyl Acetate. A Powerful Tool for Authenticity Control of Essential Oils
The enantiomeric distributions of linalool and linalyl acetate in various natural products are measured by enantioselective gas chromatography on alkyl‐substituted cyclodextrins. Different plant cultivars were investigated by four extraction processes: steam distillation, solvent extraction, supercr...
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| Published in: | Journal of high resolution chromatography Vol. 21; no. 2; pp. 107 - 112 |
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| Format: | Journal Article |
| Language: | English |
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| Abstract | The enantiomeric distributions of linalool and linalyl acetate in various natural products are measured by enantioselective gas chromatography on alkyl‐substituted cyclodextrins. Different plant cultivars were investigated by four extraction processes: steam distillation, solvent extraction, supercritical fluid extraction, and headspace analysis. Careful attention must be paid to linalool which undergoes partial racemization under certain processing conditions. In most cases, enantiomeric distribution is a powerful tool for authenticity testing. |
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| AbstractList | The enantiomeric distributions of linalool and linalyl acetate in various natural products are measured by enantioselective gas chromatography on alkyl‐substituted cyclodextrins. Different plant cultivars were investigated by four extraction processes: steam distillation, solvent extraction, supercritical fluid extraction, and headspace analysis. Careful attention must be paid to linalool which undergoes partial racemization under certain processing conditions. In most cases, enantiomeric distribution is a powerful tool for authenticity testing. |
| Author | Faugier, V. Grenier, C. Fleig, F. Casabianca, H. Graff, J. B. |
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| Cites_doi | 10.1080/10412905.1991.9697933 10.1002/ffj.2730070404 10.1002/pca.2800020405 10.1016/S0021-9673(01)94078-6 10.1007/BF01193223 10.1002/jhrc.1240170314 10.1002/jhrc.1240160603 10.1002/ffj.2730070411 10.1002/jhrc.1240140803 10.1016/0021-9673(91)85182-F 10.1002/jhrc.1240161003 |
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| Copyright | 1998 WILEY‐VCH Verlag GmbH, Weinheim, Fed. Rep. of Germany 1998 INIST-CNRS |
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| Keywords | Distillation Electron impact Multidimensional chromatography Separation Coupled method Chiral stationary phase Dienic compound Solvent extraction Gas chromatography Cyclodextrin Sample preparation Vapor phase Optical resolution Tertiary alcohol Enantiomer Quality control Headspace Enantiomeric excess Monoterpene Essential oil Cultivated plant Acylate Supercritical fluid extraction Mass spectrometry |
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| References_xml | – start-page: 217 year: 1990 end-page: 220 – volume: 396 start-page: 378 year: 1987 end-page: 381 publication-title: J. Chromatogr. – volume: 2 start-page: 167 year: 1991 end-page: 170 publication-title: Phytochem. Anal. – volume: 194 start-page: 372 year: 1992 publication-title: Z. Lebensm. Unters. Forsch. – start-page: 215 year: 1987 end-page: 258 – volume: 16 start-page: 37 year: 1991 end-page: 39 publication-title: Perfum Flavor – start-page: 127 year: 1996 end-page: 133 – start-page: 46 year: 1994 end-page: 53 – start-page: 563 year: 1985 end-page: 576 – volume: 17 start-page: 184 year: 1994 end-page: 186 publication-title: J. High Resol. Chromatogr. – start-page: 593 year: 1992 end-page: 602 – volume: 7 start-page: 187 year: 1992 end-page: 193 publication-title: Flavour Frangrance J. – volume: 3 start-page: 229 year: 1991 end-page: 236 publication-title: J. Essent. 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Essent. Oil Res. doi: 10.1080/10412905.1991.9697933 contributor: fullname: Nykänen – volume: 7 start-page: 187 year: 1992 ident: 10.1002/(SICI)1521-4168(19980201)21:2<107::AID-JHRC107>3.0.CO;2-A-BIB5 publication-title: Flavour Frangrance J. doi: 10.1002/ffj.2730070404 contributor: fullname: Kreis – volume: 2 start-page: 167 year: 1991 ident: 10.1002/(SICI)1521-4168(19980201)21:2<107::AID-JHRC107>3.0.CO;2-A-BIB3 publication-title: Phytochem. Anal. doi: 10.1002/pca.2800020405 contributor: fullname: Schreier – volume: 396 start-page: 378 year: 1987 ident: 10.1002/(SICI)1521-4168(19980201)21:2<107::AID-JHRC107>3.0.CO;2-A-BIB14 publication-title: J. Chromatogr. doi: 10.1016/S0021-9673(01)94078-6 contributor: fullname: Gaydou – volume: 194 start-page: 372 year: 1992 ident: 10.1002/(SICI)1521-4168(19980201)21:2<107::AID-JHRC107>3.0.CO;2-A-BIB17 publication-title: Z. Lebensm. Unters. Forsch. doi: 10.1007/BF01193223 contributor: fullname: Köpke – volume: 17 start-page: 184 year: 1994 ident: 10.1002/(SICI)1521-4168(19980201)21:2<107::AID-JHRC107>3.0.CO;2-A-BIB8 publication-title: J. High Resol. Chromatogr. doi: 10.1002/jhrc.1240170314 contributor: fullname: Casabianca – volume: 16 start-page: 338 year: 1993 ident: 10.1002/(SICI)1521-4168(19980201)21:2<107::AID-JHRC107>3.0.CO;2-A-BIB2 publication-title: J. High Resol. Chromatogr. doi: 10.1002/jhrc.1240160603 contributor: fullname: König – start-page: 215 volume-title: Capillary Gas Chromatography in Essential Oil Analysis year: 1987 ident: 10.1002/(SICI)1521-4168(19980201)21:2<107::AID-JHRC107>3.0.CO;2-A-BIB18 contributor: fullname: Teisseire – year: 1992 ident: 10.1002/(SICI)1521-4168(19980201)21:2<107::AID-JHRC107>3.0.CO;2-A-BIB20 contributor: fullname: Remy – year: 1996 ident: 10.1002/(SICI)1521-4168(19980201)21:2<107::AID-JHRC107>3.0.CO;2-A-BIB19 contributor: fullname: Remy – volume: 5/6 start-page: 149 year: 1993 ident: 10.1002/(SICI)1521-4168(19980201)21:2<107::AID-JHRC107>3.0.CO;2-A-BIB6 publication-title: Pharm. Ztg. Wiss. contributor: fullname: Kreis – start-page: 563 volume-title: Progress in Flavour research year: 1985 ident: 10.1002/(SICI)1521-4168(19980201)21:2<107::AID-JHRC107>3.0.CO;2-A-BIB13 contributor: fullname: Morin – volume: 7 start-page: 227 year: 1992 ident: 10.1002/(SICI)1521-4168(19980201)21:2<107::AID-JHRC107>3.0.CO;2-A-BIB11 publication-title: Flavour Fragrance J. doi: 10.1002/ffj.2730070411 contributor: fullname: Reverchon – year: 1994 ident: 10.1002/(SICI)1521-4168(19980201)21:2<107::AID-JHRC107>3.0.CO;2-A-BIB15 contributor: fullname: Remy – volume: 14 start-page: 507 year: 1991 ident: 10.1002/(SICI)1521-4168(19980201)21:2<107::AID-JHRC107>3.0.CO;2-A-BIB1 publication-title: J. High Resol. Chromatogr. doi: 10.1002/jhrc.1240140803 contributor: fullname: Keim – start-page: 217 volume-title: Flavour Science and Technology year: 1990 ident: 10.1002/(SICI)1521-4168(19980201)21:2<107::AID-JHRC107>3.0.CO;2-A-BIB9 contributor: fullname: Nykänen – volume: 587 start-page: 347 year: 1991 ident: 10.1002/(SICI)1521-4168(19980201)21:2<107::AID-JHRC107>3.0.CO;2-A-BIB16 publication-title: J. Chromatogr. doi: 10.1016/0021-9673(91)85182-F contributor: fullname: Karl – volume: 16 start-page: 569 year: 1993 ident: 10.1002/(SICI)1521-4168(19980201)21:2<107::AID-JHRC107>3.0.CO;2-A-BIB4 publication-title: J. High Resol. Chromatogr. doi: 10.1002/jhrc.1240161003 contributor: fullname: König – volume: 14 start-page: 129 year: 1992 ident: 10.1002/(SICI)1521-4168(19980201)21:2<107::AID-JHRC107>3.0.CO;2-A-BIB7 publication-title: Chem. Mikrobiol. Technol. Lebensm. contributor: fullname: Hener |
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| SubjectTerms | Applied sciences Chemical industry and chemicals enantiomer distributions in natural products obtained by different extraction processes enantioseparation by enantioselective gas chromatography Essential oils, perfumes Exact sciences and technology Linalool Linalool; linalyl acetate linalyl acetate Washing products. Cosmetics and toiletries. Perfumes |
| Title | Enantiomeric Distribution Studies of Linalool and Linalyl Acetate. A Powerful Tool for Authenticity Control of Essential Oils |
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