Simultaneously enhanced strength and strain hardening capacity in FeMnCoCr high-entropy alloy via harmonic structure design

Harmonic structure (HS), consisting of coarse-grained (CG) areas uniformly embedded in three dimensional continuously connected ultrafine-grained (UFG) areas, is considered as an effective microstructural design strategy to achieve enhanced strength and ductility in metallic materials. In the presen...

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Published in:Scripta materialia Vol. 191; pp. 196 - 201
Main Authors: Li, Guodong, Liu, Maowen, Lyu, Shaoyuan, Nakatani, Masashi, Zheng, Ruixiao, Ma, Chaoli, Li, Qiushi, Ameyama, Kei
Format: Journal Article
Language:English
Published: Elsevier Ltd 15-01-2021
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Abstract Harmonic structure (HS), consisting of coarse-grained (CG) areas uniformly embedded in three dimensional continuously connected ultrafine-grained (UFG) areas, is considered as an effective microstructural design strategy to achieve enhanced strength and ductility in metallic materials. In the present study, HS designed non-equiatomic FeMnCoCr high-entropy alloy samples with tunable shell fractions (ranging from ~16% to ~70%) were successfully prepared via controlled mechanical milling and subsequent sintering. Microstructure observations suggested that the shell region was composed of fully recrystallized UFGs with a mean grain size below 1 µm. Tensile test revealed that the HS designed samples exhibited simultaneously enhanced strength and strain hardening capability than those of the homogeneous structured counterpart. Particularly, the ultimate tensile strength and uniform elongation of the sample with a shell fraction of ~70% were 1228MPa and 12.4%, respectively, demonstrating superior strength-ductility synergy. The underlying mechanisms responsible for the enhanced mechanical properties were discussed. [Display omitted]
AbstractList Harmonic structure (HS), consisting of coarse-grained (CG) areas uniformly embedded in three dimensional continuously connected ultrafine-grained (UFG) areas, is considered as an effective microstructural design strategy to achieve enhanced strength and ductility in metallic materials. In the present study, HS designed non-equiatomic FeMnCoCr high-entropy alloy samples with tunable shell fractions (ranging from ~16% to ~70%) were successfully prepared via controlled mechanical milling and subsequent sintering. Microstructure observations suggested that the shell region was composed of fully recrystallized UFGs with a mean grain size below 1 µm. Tensile test revealed that the HS designed samples exhibited simultaneously enhanced strength and strain hardening capability than those of the homogeneous structured counterpart. Particularly, the ultimate tensile strength and uniform elongation of the sample with a shell fraction of ~70% were 1228MPa and 12.4%, respectively, demonstrating superior strength-ductility synergy. The underlying mechanisms responsible for the enhanced mechanical properties were discussed. [Display omitted]
Author Nakatani, Masashi
Ma, Chaoli
Liu, Maowen
Zheng, Ruixiao
Li, Qiushi
Lyu, Shaoyuan
Li, Guodong
Ameyama, Kei
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  organization: Department of Mechanical Engineering, Faculty of Science and Engineering, Ritsumeikan University, 1-1-1 Nojihigashi, Kusatsu, Shiga 525-8577, Japan
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SubjectTerms Harmonic structure
High-entropy alloy
Powder Metallurgy
Strain hardening
Strength and ductility
Title Simultaneously enhanced strength and strain hardening capacity in FeMnCoCr high-entropy alloy via harmonic structure design
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