Different corrosion behaviour of autoclaves made of nickel base alloy 718 in ammonobasic and ammonoacidic environments
•Metallographic investigation of corrosion behaviour of ammonothermal autoclaves.•Ammonobasic conditions lead to formation of corrosion layer.•Ammonoacidic environment cause vast general corrosion and stress corrosion cracking. The ammonothermal process is a promising technique for cost-effective gr...
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| Published in: | The Journal of supercritical fluids Vol. 95; pp. 158 - 166 |
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| Format: | Journal Article |
| Language: | English |
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Elsevier B.V
01-11-2014
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| Abstract | •Metallographic investigation of corrosion behaviour of ammonothermal autoclaves.•Ammonobasic conditions lead to formation of corrosion layer.•Ammonoacidic environment cause vast general corrosion and stress corrosion cracking.
The ammonothermal process is a promising technique for cost-effective growth of nitride based bulk-semiconductors. Degeneration of growth reactors made of a NiFeCr alloy is a limiting factor of the growth process. Corrosion is initiated by supercritical ammonia and acidic as well as basic mineralizer up to 600°C and 300MPa. We investigated the corrosion processes with microscopic (optical and scanning electron microscopy) and spectroscopic (energy dispersive X-ray and auger electron spectroscopy) methods. It showed that ammonobasic environments lead to the formation of a nitrited layer. Composition and thickness changes depending on the number of loads. The corrosion layer does not reach a steady state and therefore degenerates as consequence of cyclic ammonothermal loads. For ammonoacidic conditions on the other hand significant general corrosion occurred which is connected to the dissolution of the metal phase in the supercritical. Moreover, a high tendency to stress corrosion cracking was observed. |
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| AbstractList | The ammonothermal process is a promising technique for cost-effective growth of nitride based bulk-semiconductors. Degeneration of growth reactors made of a Nisingle bondFesingle bondCr alloy is a limiting factor of the growth process. Corrosion is initiated by supercritical ammonia and acidic as well as basic mineralizer up to 600 degree C and 300 MPa. We investigated the corrosion processes with microscopic (optical and scanning electron microscopy) and spectroscopic (energy dispersive X-ray and auger electron spectroscopy) methods. It showed that ammonobasic environments lead to the formation of a nitrited layer. Composition and thickness changes depending on the number of loads. The corrosion layer does not reach a steady state and therefore degenerates as consequence of cyclic ammonothermal loads. For ammonoacidic conditions on the other hand significant general corrosion occurred which is connected to the dissolution of the metal phase in the supercritical. Moreover, a high tendency to stress corrosion cracking was observed. •Metallographic investigation of corrosion behaviour of ammonothermal autoclaves.•Ammonobasic conditions lead to formation of corrosion layer.•Ammonoacidic environment cause vast general corrosion and stress corrosion cracking. The ammonothermal process is a promising technique for cost-effective growth of nitride based bulk-semiconductors. Degeneration of growth reactors made of a NiFeCr alloy is a limiting factor of the growth process. Corrosion is initiated by supercritical ammonia and acidic as well as basic mineralizer up to 600°C and 300MPa. We investigated the corrosion processes with microscopic (optical and scanning electron microscopy) and spectroscopic (energy dispersive X-ray and auger electron spectroscopy) methods. It showed that ammonobasic environments lead to the formation of a nitrited layer. Composition and thickness changes depending on the number of loads. The corrosion layer does not reach a steady state and therefore degenerates as consequence of cyclic ammonothermal loads. For ammonoacidic conditions on the other hand significant general corrosion occurred which is connected to the dissolution of the metal phase in the supercritical. Moreover, a high tendency to stress corrosion cracking was observed. |
| Author | Hertweck, Benjamin Steigerwald, Thomas G. Alt, Nicolas S.A. Schluecker, Eberhard |
| Author_xml | – sequence: 1 givenname: Benjamin surname: Hertweck fullname: Hertweck, Benjamin email: benjamin.hertweck@fau.de organization: Institute of Process Machinery and Systems Engineering, Friedrich-Alexander-Universität Erlangen-Nürnberg, Cauerstr. 4, 91052 Erlangen, Germany – sequence: 2 givenname: Thomas G. surname: Steigerwald fullname: Steigerwald, Thomas G. organization: Institute of Process Machinery and Systems Engineering, Friedrich-Alexander-Universität Erlangen-Nürnberg, Cauerstr. 4, 91052 Erlangen, Germany – sequence: 3 givenname: Nicolas S.A. surname: Alt fullname: Alt, Nicolas S.A. organization: Institute of Process Machinery and Systems Engineering, Friedrich-Alexander-Universität Erlangen-Nürnberg, Cauerstr. 4, 91052 Erlangen, Germany – sequence: 4 givenname: Eberhard surname: Schluecker fullname: Schluecker, Eberhard organization: Institute of Process Machinery and Systems Engineering, Friedrich-Alexander-Universität Erlangen-Nürnberg, Cauerstr. 4, 91052 Erlangen, Germany |
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| Snippet | •Metallographic investigation of corrosion behaviour of ammonothermal autoclaves.•Ammonobasic conditions lead to formation of corrosion layer.•Ammonoacidic... The ammonothermal process is a promising technique for cost-effective growth of nitride based bulk-semiconductors. Degeneration of growth reactors made of a... |
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| SubjectTerms | Ammonothermal crystal growth Auger electron spectroscopy Autoclaves Bonding Corrosion Dissolution Nickel base alloy Nitrides Optical data processing Stress corrosion cracking Supercritical ammonia |
| Title | Different corrosion behaviour of autoclaves made of nickel base alloy 718 in ammonobasic and ammonoacidic environments |
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