Smart photochromic materials based on polylactic acid
The smart photochromic materials based on polylactic acid (PLA) were prepared by melt-blending and hot-pressing, in which photochromic microcapsules (PM) were used as a functional additive, and poly(vinyl acetate) (PVAc) was introduced into the photochromic PLA blends for the first time to improve t...
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| Published in: | International journal of biological macromolecules Vol. 241; p. 124465 |
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| Main Authors: | , , , , , , , , |
| Format: | Journal Article |
| Language: | English |
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Elsevier B.V
30-06-2023
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| Abstract | The smart photochromic materials based on polylactic acid (PLA) were prepared by melt-blending and hot-pressing, in which photochromic microcapsules (PM) were used as a functional additive, and poly(vinyl acetate) (PVAc) was introduced into the photochromic PLA blends for the first time to improve their properties. The crystallization and melting behavior, morphology, and photochromic performance of PLA/PVAc/PM blends were characterized by differential scanning calorimetry (DSC), scanning electron microscopy (SEM), and spectrophotometer, respectively. The results showed that PVAc significantly improved the photochromic properties of PLA/PM blends. Under 30 s UV irradiation, the blends reached a value of ΔE that could be recognized in 3 s by human eyes. This discriminative ΔE value could be maintained for at least 3 min after removal from UV irradiation. Meanwhile, the blend had outstanding photochromic durability and recyclability. Compared to ΔE for 0.5 h of continuous light irradiation, ΔE for 8 h of continuous light irradiation decreased by only about 1, to 14.1. In 25 cycles of 3 s UV irradiation, the values of ΔE for the first and 25th irradiation were 11.4 and 11.6, respectively. The blend showed different photochromic responses to different light intensities. The ΔE values of 8.6, 14.6, 14.6, and 18.4 for irradiation at 600, 800, 1000, and 1200 W/m2 of solar intensity, respectively. |
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| AbstractList | The smart photochromic materials based on polylactic acid (PLA) were prepared by melt-blending and hot-pressing, in which photochromic microcapsules (PM) were used as a functional additive, and poly(vinyl acetate) (PVAc) was introduced into the photochromic PLA blends for the first time to improve their properties. The crystallization and melting behavior, morphology, and photochromic performance of PLA/PVAc/PM blends were characterized by differential scanning calorimetry (DSC), scanning electron microscopy (SEM), and spectrophotometer, respectively. The results showed that PVAc significantly improved the photochromic properties of PLA/PM blends. Under 30 s UV irradiation, the blends reached a value of ΔE that could be recognized in 3 s by human eyes. This discriminative ΔE value could be maintained for at least 3 min after removal from UV irradiation. Meanwhile, the blend had outstanding photochromic durability and recyclability. Compared to ΔE for 0.5 h of continuous light irradiation, ΔE for 8 h of continuous light irradiation decreased by only about 1, to 14.1. In 25 cycles of 3 s UV irradiation, the values of ΔE for the first and 25th irradiation were 11.4 and 11.6, respectively. The blend showed different photochromic responses to different light intensities. The ΔE values of 8.6, 14.6, 14.6, and 18.4 for irradiation at 600, 800, 1000, and 1200 W/m
of solar intensity, respectively. The smart photochromic materials based on polylactic acid (PLA) were prepared by melt-blending and hot-pressing, in which photochromic microcapsules (PM) were used as a functional additive, and poly(vinyl acetate) (PVAc) was introduced into the photochromic PLA blends for the first time to improve their properties. The crystallization and melting behavior, morphology, and photochromic performance of PLA/PVAc/PM blends were characterized by differential scanning calorimetry (DSC), scanning electron microscopy (SEM), and spectrophotometer, respectively. The results showed that PVAc significantly improved the photochromic properties of PLA/PM blends. Under 30 s UV irradiation, the blends reached a value of ΔE that could be recognized in 3 s by human eyes. This discriminative ΔE value could be maintained for at least 3 min after removal from UV irradiation. Meanwhile, the blend had outstanding photochromic durability and recyclability. Compared to ΔE for 0.5 h of continuous light irradiation, ΔE for 8 h of continuous light irradiation decreased by only about 1, to 14.1. In 25 cycles of 3 s UV irradiation, the values of ΔE for the first and 25th irradiation were 11.4 and 11.6, respectively. The blend showed different photochromic responses to different light intensities. The ΔE values of 8.6, 14.6, 14.6, and 18.4 for irradiation at 600, 800, 1000, and 1200 W/m2 of solar intensity, respectively. |
| ArticleNumber | 124465 |
| Author | Mao, Wenwen Wang, Lanlan Zhou, Xingxing Li, Haoxuan Liu, Qingsheng Li, Dawei Deng, Bingyao Guo, Haiyang Yu, Dongzheng |
| Author_xml | – sequence: 1 givenname: Xingxing surname: Zhou fullname: Zhou, Xingxing organization: Key Laboratory of Eco-Textiles, Ministry of Education, Jiangnan University, Wuxi 214122, People's Republic of China – sequence: 2 givenname: Dongzheng surname: Yu fullname: Yu, Dongzheng organization: Key Laboratory of Eco-Textiles, Ministry of Education, Jiangnan University, Wuxi 214122, People's Republic of China – sequence: 3 givenname: Wenwen surname: Mao fullname: Mao, Wenwen organization: Key Laboratory of Eco-Textiles, Ministry of Education, Jiangnan University, Wuxi 214122, People's Republic of China – sequence: 4 givenname: Lanlan surname: Wang fullname: Wang, Lanlan organization: Key Laboratory of Eco-Textiles, Ministry of Education, Jiangnan University, Wuxi 214122, People's Republic of China – sequence: 5 givenname: Haiyang surname: Guo fullname: Guo, Haiyang organization: Jiangsu Doway New Materials Science & Technology Co. Ltd., Suqian 223800, People's Republic of China – sequence: 6 givenname: Dawei surname: Li fullname: Li, Dawei organization: Key Laboratory of Eco-Textiles, Ministry of Education, Jiangnan University, Wuxi 214122, People's Republic of China – sequence: 7 givenname: Haoxuan surname: Li fullname: Li, Haoxuan organization: Key Laboratory of Eco-Textiles, Ministry of Education, Jiangnan University, Wuxi 214122, People's Republic of China – sequence: 8 givenname: Bingyao surname: Deng fullname: Deng, Bingyao organization: Key Laboratory of Eco-Textiles, Ministry of Education, Jiangnan University, Wuxi 214122, People's Republic of China – sequence: 9 givenname: Qingsheng surname: Liu fullname: Liu, Qingsheng email: qsliu@jiangnan.edu.cn organization: Key Laboratory of Eco-Textiles, Ministry of Education, Jiangnan University, Wuxi 214122, People's Republic of China |
| BackLink | https://www.ncbi.nlm.nih.gov/pubmed/37060981$$D View this record in MEDLINE/PubMed |
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| CitedBy_id | crossref_primary_10_1016_j_molstruc_2023_137249 crossref_primary_10_1016_j_ijbiomac_2024_133136 crossref_primary_10_1016_j_nanoen_2024_109679 |
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| Keywords | Poly(vinyl acetate) (PVAc) Polylactic acid (PLA) Photochromic microcapsules Compatibilizer Photochromic |
| Language | English |
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| SubjectTerms | Calorimetry, Differential Scanning Compatibilizer Humans Lactic Acid - chemistry Photochromic Photochromic microcapsules Poly(vinyl acetate) (PVAc) Polyesters - chemistry Polylactic acid (PLA) Polymers - chemistry |
| Title | Smart photochromic materials based on polylactic acid |
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