Application of sol-gel methods to obtain silica materials decorated with ferrocenyl-ureidopyrimidine moieties. Preparation of hollow spheres and modification of a carbon electrode
The application of a sol-gel method, starting from N-(4-ferrocenyl-6-phenylpyrimidin-2-yl)-N’-(3-(triethoxysilyl)prop-1-yl)-urea (4), tetraethoxysilane and a structure directing agent, led to the formation of hollow spherical particles with organic moieties concentrated on the inner surface. A simil...
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| Published in: | Microporous and mesoporous materials Vol. 308; p. 110380 |
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| Main Authors: | , , , , , , |
| Format: | Journal Article |
| Language: | English |
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01-12-2020
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| Abstract | The application of a sol-gel method, starting from N-(4-ferrocenyl-6-phenylpyrimidin-2-yl)-N’-(3-(triethoxysilyl)prop-1-yl)-urea (4), tetraethoxysilane and a structure directing agent, led to the formation of hollow spherical particles with organic moieties concentrated on the inner surface. A similar sol-gel electrodeposition technique was used for the modification of the surface of a spectral graphite electrode. The solid materials were characterized by solid phase NMR and IR measurements, thermal analysis, SEM and TEM. The functional group attached to the ferrocene core offers the possibility to form H-bonds with various guest molecules that makes it a potential electrochemical sensor.
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•Ferrocene-containing hollow spheres were obtained by a sol-gel method in one step.•Organic moieties were shown to be concentrated on the inner surface .•Porous structure of shells was proved by TEM measurements .•Direct co-condensation was used to prepare a ferrocene functionalized electrode. |
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| AbstractList | The application of a sol-gel method, starting from N-(4-ferrocenyl-6-phenylpyrimidin-2-yl)-N’-(3-(triethoxysilyl)prop-1-yl)-urea (4), tetraethoxysilane and a structure directing agent, led to the formation of hollow spherical particles with organic moieties concentrated on the inner surface. A similar sol-gel electrodeposition technique was used for the modification of the surface of a spectral graphite electrode. The solid materials were characterized by solid phase NMR and IR measurements, thermal analysis, SEM and TEM. The functional group attached to the ferrocene core offers the possibility to form H-bonds with various guest molecules that makes it a potential electrochemical sensor.
[Display omitted]
•Ferrocene-containing hollow spheres were obtained by a sol-gel method in one step.•Organic moieties were shown to be concentrated on the inner surface .•Porous structure of shells was proved by TEM measurements .•Direct co-condensation was used to prepare a ferrocene functionalized electrode. |
| ArticleNumber | 110380 |
| Author | Keszei, Soma J. Jakab, Miklós Pekker, Péter Skoda-Földes, Rita Nagy, Lívia Balogh, Szabolcs Fehér, Csaba |
| Author_xml | – sequence: 1 givenname: Soma J. orcidid: 0000-0001-9481-0802 surname: Keszei fullname: Keszei, Soma J. organization: University of Pannonia, Institute of Chemistry, Department of Organic Chemistry, Egyetem u. 10, P.O.Box 158, Veszprém, H-8200, Hungary – sequence: 2 givenname: Péter surname: Pekker fullname: Pekker, Péter organization: Research Institute of Biomolecular and Chemical Engineering, NANOLAB, University of Pannonia, Egyetem u. 10, P.O.Box 158, Veszprém, H-8200, Hungary – sequence: 3 givenname: Csaba surname: Fehér fullname: Fehér, Csaba organization: University of Pannonia, Institute of Chemistry, Department of Organic Chemistry, Egyetem u. 10, P.O.Box 158, Veszprém, H-8200, Hungary – sequence: 4 givenname: Szabolcs surname: Balogh fullname: Balogh, Szabolcs organization: Institute of Chemistry, NMR Laboratory, University of Pannonia, Egyetem u. 10, Veszprém, H-8200, Hungary – sequence: 5 givenname: Miklós surname: Jakab fullname: Jakab, Miklós organization: Institute of Materials Engineering, University of Pannonia, Egyetem u. 10, Veszprém, H-8200, Hungary – sequence: 6 givenname: Lívia surname: Nagy fullname: Nagy, Lívia organization: János Szentágothai Research Center, University of Pécs, Ifjúság útja 20, Pécs, H-7624, Hungary – sequence: 7 givenname: Rita surname: Skoda-Földes fullname: Skoda-Földes, Rita email: skodane@almos.uni-pannon.hu organization: University of Pannonia, Institute of Chemistry, Department of Organic Chemistry, Egyetem u. 10, P.O.Box 158, Veszprém, H-8200, Hungary |
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| Keywords | Immobilization Hollow sphere Electrode-modification Sol-gel method Ferrocene |
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| Snippet | The application of a sol-gel method, starting from N-(4-ferrocenyl-6-phenylpyrimidin-2-yl)-N’-(3-(triethoxysilyl)prop-1-yl)-urea (4), tetraethoxysilane and a... |
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| SubjectTerms | Electrode-modification Ferrocene Hollow sphere Immobilization Sol-gel method |
| Title | Application of sol-gel methods to obtain silica materials decorated with ferrocenyl-ureidopyrimidine moieties. Preparation of hollow spheres and modification of a carbon electrode |
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