Vapour pressure of diethyl phthalate

Measurements of vapour pressure in the liquid phase and of enthalpy of vaporisation and results of calculation of ideal-gas properties for diethyl phthalate are reported. The method of comparative ebulliometry, the static method, and the Knudsen mass-loss effusion method were employed to determine t...

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Published in:	The Journal of chemical thermodynamics Vol. 36; no. 11; pp. 929 - 937
Main Authors:	Roháč, Vladislav, Růžička, Květoslav, Růžička, Vlastimil, Zaitsau, Dzmitry H., Kabo, Gennady J., Diky, Vladimir, Aim, Karel
Format:	Journal Article
Language:	English
Published:	Kidlington Elsevier Ltd 01-11-2004 Elsevier
Subjects:	Chemical thermodynamics Chemistry Correlation Diethyl phthalate Enthalpy of vaporisation Exact sciences and technology Experimental data General and physical chemistry General. Theory Vapour pressure Vapour pressure Enthalpy of vaporisation Correlation Experimental data Diethyl phthalate Vapor pressure Heat of vaporization Diester Thermodynamic properties Phthalates
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Abstract	Measurements of vapour pressure in the liquid phase and of enthalpy of vaporisation and results of calculation of ideal-gas properties for diethyl phthalate are reported. The method of comparative ebulliometry, the static method, and the Knudsen mass-loss effusion method were employed to determine the vapour pressure. A Calvet-type differential microcalorimeter was used to measure the enthalpy of vaporisation. Simultaneous correlation of vapour pressure, of enthalpy of vaporisation and of difference in heat capacities of ideal gas and liquid/solid phases was used to generate parameters of the Cox equation that cover both the (vapour + solid) equilibrium (approximate temperature range from 220 K to 270 K) and (vapour + liquid) equilibrium (from 270 K to 520 K). Vapour pressure and enthalpy of vaporisation derived from the fit are reported at the triple-point temperature T = 269.92 K ( p = 0.0029 Pa, Δ vap H m = 85.10 kJ · mol −1 ), at T = 298.15 K ( p = 0.099 Pa, Δ vap H m = 82.09 kJ · mol −1), and at the normal boiling temperature T = 570.50 K (Δ vap H m = 56.49 kJ · mol −1). Measured vapour pressures and measured and calculated enthalpies of vaporisation are compared with literature data.
AbstractList	Measurements of vapour pressure in the liquid phase and of enthalpy of vaporisation and results of calculation of ideal-gas properties for diethyl phthalate are reported. The method of comparative ebulliometry, the static method, and the Knudsen mass-loss effusion method were employed to determine the vapour pressure. A Calvet-type differential microcalorimeter was used to measure the enthalpy of vaporisation. Simultaneous correlation of vapour pressure, of enthalpy of vaporisation and of difference in heat capacities of ideal gas and liquid/solid phases was used to generate parameters of the Cox equation that cover both the (vapour + solid) equilibrium (approximate temperature range from 220 K to 270 K) and (vapour + liquid) equilibrium (from 270 K to 520 K). Vapour pressure and enthalpy of vaporisation derived from the fit are reported at the triple-point temperature T = 269.92 K ( p = 0.0029 Pa, Δ vap H m = 85.10 kJ · mol −1 ), at T = 298.15 K ( p = 0.099 Pa, Δ vap H m = 82.09 kJ · mol −1), and at the normal boiling temperature T = 570.50 K (Δ vap H m = 56.49 kJ · mol −1). Measured vapour pressures and measured and calculated enthalpies of vaporisation are compared with literature data.
Author	Roháč, Vladislav Kabo, Gennady J. Diky, Vladimir Růžička, Květoslav Aim, Karel Růžička, Vlastimil Zaitsau, Dzmitry H.
Author_xml	– sequence: 1 givenname: Vladislav surname: Roháč fullname: Roháč, Vladislav organization: Department of Physical Chemistry, Institute of Chemical Technology, 166 28 Prague 6, Czech Republic – sequence: 2 givenname: Květoslav surname: Růžička fullname: Růžička, Květoslav organization: Department of Physical Chemistry, Institute of Chemical Technology, 166 28 Prague 6, Czech Republic – sequence: 3 givenname: Vlastimil surname: Růžička fullname: Růžička, Vlastimil email: vlastimil.ruzicka@vscht.cz organization: Department of Physical Chemistry, Institute of Chemical Technology, 166 28 Prague 6, Czech Republic – sequence: 4 givenname: Dzmitry H. surname: Zaitsau fullname: Zaitsau, Dzmitry H. organization: Department of Chemistry, Belarusian State University, Leningradskaya 14, Minsk 220050, Belarus – sequence: 5 givenname: Gennady J. surname: Kabo fullname: Kabo, Gennady J. organization: Department of Chemistry, Belarusian State University, Leningradskaya 14, Minsk 220050, Belarus – sequence: 6 givenname: Vladimir surname: Diky fullname: Diky, Vladimir organization: Thermodynamics Research Center, NIST Physical and Chemical Properties Division, 325 Broadway, Mailcode 838.00, Boulder, CO 80305-3328, USA – sequence: 7 givenname: Karel surname: Aim fullname: Aim, Karel organization: E. Hála Laboratory of Thermodynamics, Institute of Chemical Process Fundamentals, Academy of Sciences of the Czech Republic, 165 02 Prague 6, Czech Republic
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Snippet	Measurements of vapour pressure in the liquid phase and of enthalpy of vaporisation and results of calculation of ideal-gas properties for diethyl phthalate...
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SubjectTerms	Chemical thermodynamics Chemistry Correlation Diethyl phthalate Enthalpy of vaporisation Exact sciences and technology Experimental data General and physical chemistry General. Theory Vapour pressure
Title	Vapour pressure of diethyl phthalate
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