Nano-SiC implantation into the structure of carbon/graphite materials made by pyrolysis (carbonization) of the precursor system coal tar pitch/poly(dimethylsiloxane)
Conversion of the air-cured poly(dimethylsiloxane) {–O–Si(CH 3) 2–} n to SiC during co-pyrolysis with a coal tar pitch is studied with reference to the related SiO 2/pitch system. Each binary mixture is first homogenized at 160 °C followed by carbonization at 500 °C under argon to afford initial car...
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| Published in: | The Journal of physics and chemistry of solids Vol. 65; no. 2; pp. 647 - 653 |
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| Abstract | Conversion of the air-cured poly(dimethylsiloxane) {–O–Si(CH
3)
2–}
n
to SiC during co-pyrolysis with a coal tar pitch is studied with reference to the related SiO
2/pitch system. Each binary mixture is first homogenized at 160 °C followed by carbonization at 500 °C under argon to afford initial carbonizates. In both cases, one part of the initial carbonizate is further pyrolyzed at 1300 °C and another part at 1650 °C under an argon flow resulting in composite products. All products are studied with FT-IR, XRD, and XPS spectroscopic methods supplemented with SEM and ‘wet’ Si-analyses, when applicable. Carbothermally assisted conversion of both silicon precursors to nanocrystalline SiC embedded in the evolving C-matrix, i.e. nano-SiC/C composites, is evident only after the 1650 °C carbonization stage. |
|---|---|
| AbstractList | Conversion of the air-cured poly(dimethylsiloxane) {-O-Si(CH3)2-}n to SiC during co-pyrolysis with a coal tar pitch is studied with reference to the related SiO2/pitch system. Each binary mixture is first homogenized at 160 C followed by carbonization at 500 C under argon to afford initial carbonizates. In both cases, one part of the initial carbonizate is further pyrolyzed at 1300 C and another part at 1650 C under an argon flow resulting in composite products. All products are studied with FT-IR, XRD, and XPS spectroscopic methods supplemented with SEM and wet Si-analyses, when applicable. Carbothermally assisted conversion of both silicon precursors to nanocrystalline SiC embedded in the evolving C-matrix, i.e. nano-SiC/C composites, is evident only after the 1650 C carbonization stage. 13 refs. Conversion of the air-cured poly(dimethylsiloxane) {–O–Si(CH 3) 2–} n to SiC during co-pyrolysis with a coal tar pitch is studied with reference to the related SiO 2/pitch system. Each binary mixture is first homogenized at 160 °C followed by carbonization at 500 °C under argon to afford initial carbonizates. In both cases, one part of the initial carbonizate is further pyrolyzed at 1300 °C and another part at 1650 °C under an argon flow resulting in composite products. All products are studied with FT-IR, XRD, and XPS spectroscopic methods supplemented with SEM and ‘wet’ Si-analyses, when applicable. Carbothermally assisted conversion of both silicon precursors to nanocrystalline SiC embedded in the evolving C-matrix, i.e. nano-SiC/C composites, is evident only after the 1650 °C carbonization stage. |
| Author | Janik, Jerzy F. Czosnek, Cezary Drygaś, Mariusz Wolszczak, Janina Góra, Marta |
| Author_xml | – sequence: 1 givenname: Cezary surname: Czosnek fullname: Czosnek, Cezary organization: Faculty of Fuels and Energy, AGH University of Science and Technology, al. Mickiewicza 30, 30-059 Kraków, Poland – sequence: 2 givenname: Janina surname: Wolszczak fullname: Wolszczak, Janina organization: Faculty of Fuels and Energy, AGH University of Science and Technology, al. Mickiewicza 30, 30-059 Kraków, Poland – sequence: 3 givenname: Mariusz surname: Drygaś fullname: Drygaś, Mariusz organization: Faculty of Fuels and Energy, AGH University of Science and Technology, al. Mickiewicza 30, 30-059 Kraków, Poland – sequence: 4 givenname: Marta surname: Góra fullname: Góra, Marta organization: Faculty of Metallurgy and Materials Science, AGH University of Science and Technology, al. Mickiewicza 30, 30-059 Kraków, Poland – sequence: 5 givenname: Jerzy F. surname: Janik fullname: Janik, Jerzy F. email: janikj@uci.agh.edu.pl organization: Faculty of Fuels and Energy, AGH University of Science and Technology, al. Mickiewicza 30, 30-059 Kraków, Poland |
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| Keywords | Carbonization Pitch Composites Silicon carbide Poly(methylsiloxane) Nanocrystalline Scanning electron microscopy Pyrolysis Fourier transformation Carbothermy Organic siloxane Implantation Raw materials Dispersion reinforced material XRD Infrared spectra Experimental study Binary mixtures Carbon Fabrication Nanoparticles Chemical conversion Composite materials Silicon Carbides Coal tar pitch Silicones Nanocrystal X-ray photoelectron spectra |
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Ceram. doi: 10.1007/BF02767925 contributor: fullname: Semchenko – volume: 34 start-page: 89 year: 1996 ident: 10.1016/j.jpcs.2003.10.045_BIB2_2 article-title: Carbon materials obtained from organometallic modification of pitch and its oxidation resistance properties publication-title: Carbon doi: 10.1016/0008-6223(95)00139-5 contributor: fullname: Paul – volume: 42 start-page: 2395 year: 2001 ident: 10.1016/j.jpcs.2003.10.045_BIB8 article-title: Polydimethylsiloxane thermal degradation. Part 1. Kinetic aspects publication-title: Polymer doi: 10.1016/S0032-3861(00)00652-2 contributor: fullname: Camino – volume: 73 start-page: 505 year: 2001 ident: 10.1016/j.jpcs.2003.10.045_BIB13 article-title: Characterization and oxidative degradation of a room-temperature vulcanized poly(dimethylsiloxane) rubber publication-title: Polym. Degrad. Stab. doi: 10.1016/S0141-3910(01)00139-2 contributor: fullname: Chaudhury |
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| Snippet | Conversion of the air-cured poly(dimethylsiloxane) {–O–Si(CH
3)
2–}
n
to SiC during co-pyrolysis with a coal tar pitch is studied with reference to the related... Conversion of the air-cured poly(dimethylsiloxane) {-O-Si(CH3)2-}n to SiC during co-pyrolysis with a coal tar pitch is studied with reference to the related... |
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| SubjectTerms | Carbonization Composites Cross-disciplinary physics: materials science; rheology Exact sciences and technology Materials science Nanocrystalline New materials: theory, design, and fabrication Other materials Physics Pitch Poly(methylsiloxane) Silicon carbide Specific materials |
| Title | Nano-SiC implantation into the structure of carbon/graphite materials made by pyrolysis (carbonization) of the precursor system coal tar pitch/poly(dimethylsiloxane) |
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