Colloidal Crystals of Monodisperse FePt Nanoparticles Grown by a Three-Layer Technique of Controlled Oversaturation

Colloidal crystals of FePt nanocrystals have been produced by a three‐layer oversaturation technique. Faceted triangular and hexagonal platelets, pyramids, and tetrahedrons have been obtained (see Figure), consisting of individual monodisperse FePt nanocrystals aligned in a 3D superlattice. Transiti...

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Published in:	Advanced materials (Weinheim) Vol. 14; no. 4; pp. 287 - 290
Main Authors:	Shevchenko, E., Talapin, D., Kornowski, A., Wiekhorst, F., Kötzler, J., Haase, M., Rogach, A., Weller, H.
Format:	Journal Article
Language:	English
Published:	Weinheim WILEY-VCH Verlag Gmbh 19-02-2002 WILEY‐VCH Verlag Gmbh
Subjects:	Colloidal crystals ferrite Nanocomposites Nanoparticles platinum Nanoparticles platinum, ferrite
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Abstract	Colloidal crystals of FePt nanocrystals have been produced by a three‐layer oversaturation technique. Faceted triangular and hexagonal platelets, pyramids, and tetrahedrons have been obtained (see Figure), consisting of individual monodisperse FePt nanocrystals aligned in a 3D superlattice. Transition from superparamagnetic to ferromagnetic behavior is observed at 14 K.
AbstractList	Nanotechnology, defined as the creation and utilization of materials, systems, and devices through control over matter on the manometer length scale, is expected to become one of the main driving forces in materials research for the 21st century. A number of synthetic routes based on colloidal chemistry have been developed leading to monodisperse metal and semiconductor nanocrystals. Fabrication of superstructures using individual nanocrystals as building blocks and investigation of collective properties of ordered arrays is a current trend in nanoparticle research. In our previous work we have presented a three-layer technique based on slow diffusion of a non-solvent into the bulk of the concentrated solution of nanoparticles through a buffer layer of a third component with low, but not negligible, solubility for nanocrystals (Scheme 1). This method led to crystallization of monodisperse CdSe nanocrystals into perfectly faceted hexagonal colloidal crystals with sizes of about 100 mu m. In this paper we report the successful application of this crystallization technique to another nanoparticulate system-monodisperse FePt particles. Studies of the magnetic properties of the FePt colloidal crystals have been performed using zero-field-cooling and field-cooling procedures and field-dependent magnetization measurements. A hysteric behavior and the increase of coercivity with decreasing temperature were observed below the blocking temperature, with is typical for the region of stable ferromagnetism. Colloidal crystals of FePt nanocrystals have been produced by a three‐layer oversaturation technique. Faceted triangular and hexagonal platelets, pyramids, and tetrahedrons have been obtained (see Figure), consisting of individual monodisperse FePt nanocrystals aligned in a 3D superlattice. Transition from superparamagnetic to ferromagnetic behavior is observed at 14 K.
Author	Haase, M. Shevchenko, E. Rogach, A. Talapin, D. Kötzler, J. Wiekhorst, F. Weller, H. Kornowski, A.
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Snippet	Colloidal crystals of FePt nanocrystals have been produced by a three‐layer oversaturation technique. Faceted triangular and hexagonal platelets, pyramids, and... Nanotechnology, defined as the creation and utilization of materials, systems, and devices through control over matter on the manometer length scale, is...
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SubjectTerms	Colloidal crystals ferrite Nanocomposites Nanoparticles platinum Nanoparticles platinum, ferrite
Title	Colloidal Crystals of Monodisperse FePt Nanoparticles Grown by a Three-Layer Technique of Controlled Oversaturation
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