Sorption and Diffusion of Methanol and Ethanol in Macroporous Sulfonic Resin Amberlyst 15
The sorption and diffusion of methanol and ethanol on Amberlyst 15 were studied by the quartz crystal microbalance technique in the temperature range of 20-120°C at relative pressure p/ps < 0.04. The heats of sorption (∆H) and the activation energy of diffusion (E a ) of methanol and ethanol were...
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| Published in: | Theoretical and experimental chemistry Vol. 55; no. 5; pp. 354 - 359 |
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| Abstract | The sorption and diffusion of methanol and ethanol on Amberlyst 15 were studied by the quartz crystal microbalance technique in the temperature range of 20-120°C at relative pressure p/ps < 0.04. The heats of sorption (∆H) and the activation energy of diffusion (E
a
) of methanol and ethanol were determined from the temperature dependence of the Henry constant and the effective diffusion coefficient of the alcohols in the gel phase of Amberlyst 15. The proximity of the ∆H and E
a
values for each of the sorbates indicates that mass transfer within the Amberlyst 15 gel phase takes place by a sorption–desorption mechanism. |
|---|---|
| AbstractList | The sorption and diffusion of methanol and ethanol on Amberlyst 15 were studied by the quartz crystal microbalance technique in the temperature range of 20-120°C at relative pressure p/ps < 0.04. The heats of sorption (∆H) and the activation energy of diffusion (E
a
) of methanol and ethanol were determined from the temperature dependence of the Henry constant and the effective diffusion coefficient of the alcohols in the gel phase of Amberlyst 15. The proximity of the ∆H and E
a
values for each of the sorbates indicates that mass transfer within the Amberlyst 15 gel phase takes place by a sorption–desorption mechanism. The sorption and diffusion of methanol and ethanol on Amberlyst 15 were studied by the quartz crystal microbalance technique in the temperature range of 20-120°C at relative pressure p/ps < 0.04. The heats of sorption (âH) and the activation energy of diffusion (E.sub.a) of methanol and ethanol were determined from the temperature dependence of the Henry constant and the effective diffusion coefficient of the alcohols in the gel phase of Amberlyst 15. The proximity of the âH and E.sub.a values for each of the sorbates indicates that mass transfer within the Amberlyst 15 gel phase takes place by a sorption-desorption mechanism. The sorption and diffusion of methanol and ethanol on Amberlyst 15 were studied by the quartz crystal microbalance technique in the temperature range of 20-120°C at relative pressure p/ps < 0.04. The heats of sorption (∆H) and the activation energy of diffusion (Ea) of methanol and ethanol were determined from the temperature dependence of the Henry constant and the effective diffusion coefficient of the alcohols in the gel phase of Amberlyst 15. The proximity of the ∆H and Ea values for each of the sorbates indicates that mass transfer within the Amberlyst 15 gel phase takes place by a sorption–desorption mechanism. |
| Audience | Academic |
| Author | Filippov, A. P. Vlasenko, N. V. Strizhak, P. E. Serebrii, T. G. |
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| Keywords | Amberlyst 15 quartz crystal microbalance diffusion alcohols sulfonic resin sorption |
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| References | VlasenkoNVKochkinYNFilippovAPAdsorpt. Sci. Technol.2017357/86306401:CAS:528:DC%2BC2sXhvFKhsr3I10.1177/0263617417703758 FilippovAPStrizhakPEVlasenkoNVAdsorpt. Sci. Technol.201432108078201:CAS:528:DC%2BC2MXjtVChsrs%3D10.1260/0263-6174.32.10.807 IhmS-KAhnJ-HJoY-DInd. Eng. Chem. Res.1996359294629541:CAS:528:DyaK28XkvFCgtbY%3D10.1021/ie950724x VlasenkoNVKochkinYNFilippovAPSerebriiTGCatal. Commun.201112114211451:CAS:528:DC%2BC3MXmvFajtLw%3D10.1016/j.catcom.2011.03.023 BadiaJHFitéCBringuéRTop. Catal.2015589199321:CAS:528:DC%2BC2MXhtlKksb%2FE10.1007/s11244-015-0460-3 AguileraAFTolvanenPOgerAJ. Chem. Technol. Biotechnol.2019949302030311:CAS:528:DC%2BC1MXhtlejtrfE10.1002/jctb.6112 FilippovAPAdsorpt. Sci. Technol.20123054254431:CAS:528:DC%2BC38XhsV2itLjO10.1260/0263-6174.30.5.425 SontakkeMMBhaskarCSBeradBNLett. Org. Chem.20151221151211:CAS:528:DC%2BC2MXjvVCltrY%3D10.2174/1570178612666150108002716 T. Dogu, E. Aydin, N. Boz, et al., Int. J. Chem. React. Eng., 1, No. 1., ISSN (On line) 1542-6580. DOI: https://doi.org/10.2202/1542-6580.1012. XuZPChuangKTChem. Eng. Sci.19975217301130171:CAS:528:DyaK2sXlvFCjuro%3D10.1016/S0009-2509(97)00082-1 TimofeevDPKinetics of Adsorption [in Russian], Izd1962MoscowAN SSSR CrankJThe Mathematics of Diffusion1975Oxford, New YorkOxford Univ. Press ShanCWangYNieJAdv. Polym. Technol.20193848546201:CAS:528:DC%2BC1MXhtVSkt77N10.1155/2019/4854620 RuckensteinEVaidyanathanASYoungquistGRChem. Eng. Sci.1971269130513181:CAS:528:DyaE38XmvF2j10.1016/0009-2509(71)80051-9 LiuJGeYSongYCatal. Commun.201911957611:CAS:528:DC%2BC1cXitVWqtrnM10.1016/j.catcom.2018.09.019 CorainBZeccaMJerabekKJ. Mol. Catal. A.200117713201:CAS:528:DC%2BD3MXptVSisr0%3D10.1016/S1381-1169(01)00305-3 AF Aguilera (9628_CR2) 2019; 94 C Shan (9628_CR7) 2019; 38 9628_CR9 B Corain (9628_CR8) 2001; 177 ZP Xu (9628_CR10) 1997; 52 E Ruckenstein (9628_CR11) 1971; 26 AP Filippov (9628_CR12) 2012; 30 J Liu (9628_CR1) 2019; 119 MM Sontakke (9628_CR3) 2015; 12 JH Badia (9628_CR6) 2015; 58 DP Timofeev (9628_CR15) 1962 J Crank (9628_CR14) 1975 AP Filippov (9628_CR13) 2014; 32 S-K Ihm (9628_CR4) 1996; 35 NV Vlasenko (9628_CR5) 2011; 12 NV Vlasenko (9628_CR16) 2017; 35 |
| References_xml | – volume: 12 start-page: 115 issue: 2 year: 2015 ident: 9628_CR3 publication-title: Lett. Org. Chem. doi: 10.2174/1570178612666150108002716 contributor: fullname: MM Sontakke – volume-title: Kinetics of Adsorption [in Russian], Izd year: 1962 ident: 9628_CR15 contributor: fullname: DP Timofeev – volume: 94 start-page: 3020 issue: 9 year: 2019 ident: 9628_CR2 publication-title: J. Chem. Technol. Biotechnol. doi: 10.1002/jctb.6112 contributor: fullname: AF Aguilera – volume: 119 start-page: 57 year: 2019 ident: 9628_CR1 publication-title: Catal. Commun. doi: 10.1016/j.catcom.2018.09.019 contributor: fullname: J Liu – volume: 35 start-page: 2946 issue: 9 year: 1996 ident: 9628_CR4 publication-title: Ind. Eng. Chem. Res. doi: 10.1021/ie950724x contributor: fullname: S-K Ihm – volume: 12 start-page: 1142 year: 2011 ident: 9628_CR5 publication-title: Catal. Commun. doi: 10.1016/j.catcom.2011.03.023 contributor: fullname: NV Vlasenko – volume: 58 start-page: 919 year: 2015 ident: 9628_CR6 publication-title: Top. Catal. doi: 10.1007/s11244-015-0460-3 contributor: fullname: JH Badia – volume: 35 start-page: 630 issue: 7/8 year: 2017 ident: 9628_CR16 publication-title: Adsorpt. Sci. Technol. doi: 10.1177/0263617417703758 contributor: fullname: NV Vlasenko – volume: 38 start-page: 4854620 year: 2019 ident: 9628_CR7 publication-title: Adv. Polym. Technol. doi: 10.1155/2019/4854620 contributor: fullname: C Shan – volume: 177 start-page: 3 issue: 1 year: 2001 ident: 9628_CR8 publication-title: J. Mol. Catal. A. doi: 10.1016/S1381-1169(01)00305-3 contributor: fullname: B Corain – volume: 52 start-page: 3011 issue: 17 year: 1997 ident: 9628_CR10 publication-title: Chem. Eng. Sci. doi: 10.1016/S0009-2509(97)00082-1 contributor: fullname: ZP Xu – ident: 9628_CR9 doi: 10.2202/1542-6580.1012 – volume: 26 start-page: 1305 issue: 9 year: 1971 ident: 9628_CR11 publication-title: Chem. Eng. Sci. doi: 10.1016/0009-2509(71)80051-9 contributor: fullname: E Ruckenstein – volume: 32 start-page: 807 issue: 10 year: 2014 ident: 9628_CR13 publication-title: Adsorpt. Sci. Technol. doi: 10.1260/0263-6174.32.10.807 contributor: fullname: AP Filippov – volume: 30 start-page: 425 issue: 5 year: 2012 ident: 9628_CR12 publication-title: Adsorpt. Sci. Technol. doi: 10.1260/0263-6174.30.5.425 contributor: fullname: AP Filippov – volume-title: The Mathematics of Diffusion year: 1975 ident: 9628_CR14 contributor: fullname: J Crank |
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| SubjectTerms | Activation energy Alcohol Alcohol, Denatured Chemistry Chemistry and Materials Science Chemistry/Food Science Diffusion Diffusion coefficient Ethanol Mass transfer Methanol Microbalances Quartz crystals Sorbates Sorption Temperature dependence |
| Title | Sorption and Diffusion of Methanol and Ethanol in Macroporous Sulfonic Resin Amberlyst 15 |
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