Toward durable and robust superhydrophobic cotton fabric through hydrothermal growth of ZnO for oil/water separation

In this study, an eco-friendly superhydrophobic cotton fabric (CF) with water contact angle of 155° was fabricated via a facile two-step approach: imparting surface roughness through hydrothermal growth of ZnO particles, and using stearic acid to create a low-energy surface. ZnO prepared by hydrothe...

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Published in:	Cellulose (London) Vol. 26; no. 13-14; pp. 8121 - 8133
Main Authors:	Wang, Meng, Peng, Min, Weng, Yun-Xuan, Li, Yi-Dong, Zeng, Jian-Bing
Format:	Journal Article
Language:	English
Published:	Dordrecht Springer Netherlands 01-09-2019 Springer Nature B.V
Subjects:	Abrasion Bioorganic Chemistry Ceramics Chemistry Chemistry and Materials Science Composites Contact angle Cotton Cotton fabrics Durability Erosion Glass Hydrophobic surfaces Hydrophobicity Hydrothermal reactions Natural Materials Organic Chemistry Original Research Physical Chemistry Polymer Sciences Robustness Sandpaper Separation Stearic acid Surface roughness Sustainable Development Water purification Water treatment Zinc oxide Durability ZnO Oil/water separation Superhydrophobic cotton fabric Hydrothermal reaction
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Abstract	In this study, an eco-friendly superhydrophobic cotton fabric (CF) with water contact angle of 155° was fabricated via a facile two-step approach: imparting surface roughness through hydrothermal growth of ZnO particles, and using stearic acid to create a low-energy surface. ZnO prepared by hydrothermal reaction was in a rod-like shape and had nano- or micro-scale sizes. It was located on the surface in loose aggregates. After modification with stearic acid, the aggregate structure of ZnO particles was changed from loose packing to compact packing. The superhydrophobic CF could be wetted by oil but could not be wetted by water, showing excellent oil/water separation performance. The superhydrophobic CF was able to absorb oils selectively from their mixtures with water and could be used as a filtering membrane to separate oil/water mixtures directly with separation efficiency and oil flux of 96–99% and 2000–9000 L m −2 h −1 , respectively, depending on the intrinsic property of the oils. In addition, the superhydrophobic CF showed excellent mechanical robustness and environmental durability with water contact angle almost remaining unchanged after exposure to sandpaper abrasion, ultrasonication, boiling water treatment and organic solvents erosion. With excellent robustness and durability, the superhydrophobic CF exhibits great potential in oil/water separation even under some harsh conditions. Graphic abstract
AbstractList	In this study, an eco-friendly superhydrophobic cotton fabric (CF) with water contact angle of 155° was fabricated via a facile two-step approach: imparting surface roughness through hydrothermal growth of ZnO particles, and using stearic acid to create a low-energy surface. ZnO prepared by hydrothermal reaction was in a rod-like shape and had nano- or micro-scale sizes. It was located on the surface in loose aggregates. After modification with stearic acid, the aggregate structure of ZnO particles was changed from loose packing to compact packing. The superhydrophobic CF could be wetted by oil but could not be wetted by water, showing excellent oil/water separation performance. The superhydrophobic CF was able to absorb oils selectively from their mixtures with water and could be used as a filtering membrane to separate oil/water mixtures directly with separation efficiency and oil flux of 96–99% and 2000–9000 L m −2 h −1 , respectively, depending on the intrinsic property of the oils. In addition, the superhydrophobic CF showed excellent mechanical robustness and environmental durability with water contact angle almost remaining unchanged after exposure to sandpaper abrasion, ultrasonication, boiling water treatment and organic solvents erosion. With excellent robustness and durability, the superhydrophobic CF exhibits great potential in oil/water separation even under some harsh conditions. Graphic abstract In this study, an eco-friendly superhydrophobic cotton fabric (CF) with water contact angle of 155° was fabricated via a facile two-step approach: imparting surface roughness through hydrothermal growth of ZnO particles, and using stearic acid to create a low-energy surface. ZnO prepared by hydrothermal reaction was in a rod-like shape and had nano- or micro-scale sizes. It was located on the surface in loose aggregates. After modification with stearic acid, the aggregate structure of ZnO particles was changed from loose packing to compact packing. The superhydrophobic CF could be wetted by oil but could not be wetted by water, showing excellent oil/water separation performance. The superhydrophobic CF was able to absorb oils selectively from their mixtures with water and could be used as a filtering membrane to separate oil/water mixtures directly with separation efficiency and oil flux of 96–99% and 2000–9000 L m−2 h−1, respectively, depending on the intrinsic property of the oils. In addition, the superhydrophobic CF showed excellent mechanical robustness and environmental durability with water contact angle almost remaining unchanged after exposure to sandpaper abrasion, ultrasonication, boiling water treatment and organic solvents erosion. With excellent robustness and durability, the superhydrophobic CF exhibits great potential in oil/water separation even under some harsh conditions.Graphic abstract
Author	Weng, Yun-Xuan Wang, Meng Zeng, Jian-Bing Peng, Min Li, Yi-Dong
Author_xml	– sequence: 1 givenname: Meng surname: Wang fullname: Wang, Meng organization: Chongqing Key Laboratory of Soft-Matter Material Chemistry and Function Manufacturing, School of Chemistry and Chemical Engineering, Southwest University – sequence: 2 givenname: Min surname: Peng fullname: Peng, Min organization: Chongqing Key Laboratory of Soft-Matter Material Chemistry and Function Manufacturing, School of Chemistry and Chemical Engineering, Southwest University – sequence: 3 givenname: Yun-Xuan surname: Weng fullname: Weng, Yun-Xuan email: wyxuan@th.btbu.edu.cn organization: Beijing Key Laboratory of Quality Evaluation Technology for Hygiene and Safety of Plastics, Beijing Technology and Business University – sequence: 4 givenname: Yi-Dong surname: Li fullname: Li, Yi-Dong organization: Chongqing Key Laboratory of Soft-Matter Material Chemistry and Function Manufacturing, School of Chemistry and Chemical Engineering, Southwest University – sequence: 5 givenname: Jian-Bing orcidid: 0000-0003-1822-446X surname: Zeng fullname: Zeng, Jian-Bing email: jbzeng@swu.edu.cn organization: Chongqing Key Laboratory of Soft-Matter Material Chemistry and Function Manufacturing, School of Chemistry and Chemical Engineering, Southwest University
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Copyright	Springer Nature B.V. 2019 Cellulose is a copyright of Springer, (2019). All Rights Reserved.
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Keywords	Durability ZnO Oil/water separation Superhydrophobic cotton fabric Hydrothermal reaction
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Snippet	In this study, an eco-friendly superhydrophobic cotton fabric (CF) with water contact angle of 155° was fabricated via a facile two-step approach: imparting...
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SubjectTerms	Abrasion Bioorganic Chemistry Ceramics Chemistry Chemistry and Materials Science Composites Contact angle Cotton Cotton fabrics Durability Erosion Glass Hydrophobic surfaces Hydrophobicity Hydrothermal reactions Natural Materials Organic Chemistry Original Research Physical Chemistry Polymer Sciences Robustness Sandpaper Separation Stearic acid Surface roughness Sustainable Development Water purification Water treatment Zinc oxide
Title	Toward durable and robust superhydrophobic cotton fabric through hydrothermal growth of ZnO for oil/water separation
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