Graphene facilitated visible light photodegradation of methylene blue over titanium dioxide photocatalysts
[Display omitted] ► Graphene–titania composites (G–TiO2) were synthesized by a sol–gel method. ► G–TiO2 catalysts showed high efficiency in degradation of methylene blue under visible light. ► In situ prepared G–TiO2 presented higher activity than that of G–TiO2(P25). ► The mechanism of graphene in...
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| Published in: | Chemical engineering journal (Lausanne, Switzerland : 1996) Vol. 214; no. 1; pp. 298 - 303 |
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| Main Authors: | , , , |
| Format: | Journal Article |
| Language: | English |
| Published: |
Oxford
Elsevier B.V
01-01-2013
Elsevier |
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| Abstract | [Display omitted]
► Graphene–titania composites (G–TiO2) were synthesized by a sol–gel method. ► G–TiO2 catalysts showed high efficiency in degradation of methylene blue under visible light. ► In situ prepared G–TiO2 presented higher activity than that of G–TiO2(P25). ► The mechanism of graphene in the enhanced visible light photocatalytic activity was proposed.
Several graphene–titania composites (G–TiO2) were synthesized by a sol–gel method using titanium isopropoxide (or P25) as Ti-precursors and reduced graphene oxide (RGO). The structural, morphological, and physicochemical properties of the samples were thoroughly investigated by X-ray diffraction (XRD), Fourier transform infrared spectroscopy (FT-IR), field emission scanning electron microscopy (FE-SEM), UV–vis diffuse reflectance (UV–vis DRS), and thermogravimetric-differential thermal analysis (TG-DTA). A significant increase in light absorption to visible light was observed by G–TiO2 compared with that of naked TiO2. The photocatalytic activity of G–TiO2 in methylene blue bleaching under visible light (>430nm) is much enhanced. G–TiO2 synthesized from titanium isopropoxide hydrolysis presented higher activity than that of G–TiO2(P25). Contribution of graphene on the enhancement of visible-light photocatalytic activity of the composite was discussed. |
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| AbstractList | Several graphene–titania composites (G–TiO₂) were synthesized by a sol–gel method using titanium isopropoxide (or P25) as Ti-precursors and reduced graphene oxide (RGO). The structural, morphological, and physicochemical properties of the samples were thoroughly investigated by X-ray diffraction (XRD), Fourier transform infrared spectroscopy (FT-IR), field emission scanning electron microscopy (FE-SEM), UV–vis diffuse reflectance (UV–vis DRS), and thermogravimetric-differential thermal analysis (TG-DTA). A significant increase in light absorption to visible light was observed by G–TiO₂ compared with that of naked TiO₂. The photocatalytic activity of G–TiO₂ in methylene blue bleaching under visible light (>430nm) is much enhanced. G–TiO₂ synthesized from titanium isopropoxide hydrolysis presented higher activity than that of G–TiO₂(P25). Contribution of graphene on the enhancement of visible-light photocatalytic activity of the composite was discussed. [Display omitted] ► Graphene–titania composites (G–TiO2) were synthesized by a sol–gel method. ► G–TiO2 catalysts showed high efficiency in degradation of methylene blue under visible light. ► In situ prepared G–TiO2 presented higher activity than that of G–TiO2(P25). ► The mechanism of graphene in the enhanced visible light photocatalytic activity was proposed. Several graphene–titania composites (G–TiO2) were synthesized by a sol–gel method using titanium isopropoxide (or P25) as Ti-precursors and reduced graphene oxide (RGO). The structural, morphological, and physicochemical properties of the samples were thoroughly investigated by X-ray diffraction (XRD), Fourier transform infrared spectroscopy (FT-IR), field emission scanning electron microscopy (FE-SEM), UV–vis diffuse reflectance (UV–vis DRS), and thermogravimetric-differential thermal analysis (TG-DTA). A significant increase in light absorption to visible light was observed by G–TiO2 compared with that of naked TiO2. The photocatalytic activity of G–TiO2 in methylene blue bleaching under visible light (>430nm) is much enhanced. G–TiO2 synthesized from titanium isopropoxide hydrolysis presented higher activity than that of G–TiO2(P25). Contribution of graphene on the enhancement of visible-light photocatalytic activity of the composite was discussed. |
| Author | Wang, Shaobin Liu, Shizhen Sun, Hongqi Liu, Shaomin |
| Author_xml | – sequence: 1 givenname: Shizhen surname: Liu fullname: Liu, Shizhen – sequence: 2 givenname: Hongqi surname: Sun fullname: Sun, Hongqi – sequence: 3 givenname: Shaomin surname: Liu fullname: Liu, Shaomin – sequence: 4 givenname: Shaobin surname: Wang fullname: Wang, Shaobin email: shaobin.wang@curtin.edu.au |
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| Keywords | Visible light Graphene Photocatalysis TiO2 Methylene blue Scanning electron microscopy Thermogravimetry Differential thermal analysis X ray diffraction Precursor Composite material Hydrolysis Ultraviolet radiation Bleaching Visible radiation Light absorption Fourier-transformed infrared spectrometry TiO Titanium oxide Catalyst Physicochemical properties Photochemical degradation Reflectance |
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► Graphene–titania composites (G–TiO2) were synthesized by a sol–gel method. ► G–TiO2 catalysts showed high efficiency in degradation of... Several graphene–titania composites (G–TiO₂) were synthesized by a sol–gel method using titanium isopropoxide (or P25) as Ti-precursors and reduced graphene... |
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| SubjectTerms | absorption Applied sciences bleaching Catalysis Catalytic reactions Chemical engineering Chemistry Exact sciences and technology Fourier transform infrared spectroscopy General and physical chemistry Graphene hydrolysis Methylene blue Photocatalysis photolysis physicochemical properties Reactors reflectance scanning electron microscopy Theory of reactions, general kinetics. Catalysis. Nomenclature, chemical documentation, computer chemistry thermal analysis TiO2 titanium titanium dioxide Visible light X-ray diffraction |
| Title | Graphene facilitated visible light photodegradation of methylene blue over titanium dioxide photocatalysts |
| URI | https://dx.doi.org/10.1016/j.cej.2012.10.058 |
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