Photocatalytic hydrogen evolution over the isostructural titanates: Ba3Li2Ti8O20 and Na2Ti6O13 modified with metal oxide nanoparticles

Isostructural titanates exhibiting rectangular tunnel structure with the general formula Na2Ti6O13 and Ba3Li2Ti8O20, were synthesized by solid state and sol-gel methods. The structural, morphological, optical, textural and electrical properties of the materials were characterized by XRD, SEM, UV-vis...

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Published in:	International journal of hydrogen energy Vol. 43; no. 4; pp. 2148 - 2159
Main Authors:	Garay-Rodríguez, Luis F., Huerta-Flores, Ali M., Torres-Martínez, Leticia M., Moctezuma, Edgar
Format:	Journal Article
Language:	English
Published:	Elsevier Ltd 25-01-2018
Subjects:	Cocatalysts Hydrogen evolution Titanates Tunnel structure Tunnel structure Cocatalysts Titanates Hydrogen evolution
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Abstract	Isostructural titanates exhibiting rectangular tunnel structure with the general formula Na2Ti6O13 and Ba3Li2Ti8O20, were synthesized by solid state and sol-gel methods. The structural, morphological, optical, textural and electrical properties of the materials were characterized by XRD, SEM, UV-vis, BET and EIS. The photocatalytic activity for hydrogen evolution of the materials was evaluated under UV light. Na2Ti6O13 exhibited higher activity (120 μmol/gh) than Ba3Li2Ti8O20 (30 μmol/gh), and it was attributed to the distortion of the octahedrons in Ba3Li2Ti8O20, which increases the recombination of charges in the material. Additionally, the 1D dimension obtained in Na2Ti6O13 promotes a better charge separation, transport and utilization in this phase. The activity of the materials was enhanced with the incorporation of metal oxide nanoparticles MO (M = Cu, Ni) as cocatalysts. The activity of Ba3Li2Ti8O20 increased 10 times with the addition of CuO (240 μmol/gh), while the activity of Na2Ti6O13 increased 3.5 times (416 μmol/gh). This improvement in the photocatalytic activity of the isostructural titanates was attributed to the formation of a p-n heterostructure between n-type titanates and p-type CuO, which promoted an enhanced charge separation, transference and utilization. [Display omitted] •Photocatalytic H2 evolution on Ba and Na tunnel isostructural titanates is studied.•Activity of Ba3Li2Ti8O20 (30 μmol/gh) is reported herein for the first time.•A correlation of physicochemical properties with catalytic activity is discussed.•Deposition of CuO and NiO nanoparticles increased significantly the H2 evolution.•The highest activity was obtained by Na2Ti6O13 modified with CuO (416 μmol/gh).
AbstractList	Isostructural titanates exhibiting rectangular tunnel structure with the general formula Na2Ti6O13 and Ba3Li2Ti8O20, were synthesized by solid state and sol-gel methods. The structural, morphological, optical, textural and electrical properties of the materials were characterized by XRD, SEM, UV-vis, BET and EIS. The photocatalytic activity for hydrogen evolution of the materials was evaluated under UV light. Na2Ti6O13 exhibited higher activity (120 μmol/gh) than Ba3Li2Ti8O20 (30 μmol/gh), and it was attributed to the distortion of the octahedrons in Ba3Li2Ti8O20, which increases the recombination of charges in the material. Additionally, the 1D dimension obtained in Na2Ti6O13 promotes a better charge separation, transport and utilization in this phase. The activity of the materials was enhanced with the incorporation of metal oxide nanoparticles MO (M = Cu, Ni) as cocatalysts. The activity of Ba3Li2Ti8O20 increased 10 times with the addition of CuO (240 μmol/gh), while the activity of Na2Ti6O13 increased 3.5 times (416 μmol/gh). This improvement in the photocatalytic activity of the isostructural titanates was attributed to the formation of a p-n heterostructure between n-type titanates and p-type CuO, which promoted an enhanced charge separation, transference and utilization. [Display omitted] •Photocatalytic H2 evolution on Ba and Na tunnel isostructural titanates is studied.•Activity of Ba3Li2Ti8O20 (30 μmol/gh) is reported herein for the first time.•A correlation of physicochemical properties with catalytic activity is discussed.•Deposition of CuO and NiO nanoparticles increased significantly the H2 evolution.•The highest activity was obtained by Na2Ti6O13 modified with CuO (416 μmol/gh).
Author	Huerta-Flores, Ali M. Garay-Rodríguez, Luis F. Moctezuma, Edgar Torres-Martínez, Leticia M.
Author_xml	– sequence: 1 givenname: Luis F. surname: Garay-Rodríguez fullname: Garay-Rodríguez, Luis F. organization: Universidad Autónoma de Nuevo León, UANL, Facultad de Ingeniería Civil, Departamento de Ecomateriales y Energía, Av. Universidad S/N Ciudad Universitaria, San Nicolás de los Garza, Nuevo León, C.P. 66455, Mexico – sequence: 2 givenname: Ali M. surname: Huerta-Flores fullname: Huerta-Flores, Ali M. organization: Universidad Autónoma de Nuevo León, UANL, Facultad de Ingeniería Civil, Departamento de Ecomateriales y Energía, Av. Universidad S/N Ciudad Universitaria, San Nicolás de los Garza, Nuevo León, C.P. 66455, Mexico – sequence: 3 givenname: Leticia M. surname: Torres-Martínez fullname: Torres-Martínez, Leticia M. email: lettorresg@yahoo.com organization: Universidad Autónoma de Nuevo León, UANL, Facultad de Ingeniería Civil, Departamento de Ecomateriales y Energía, Av. Universidad S/N Ciudad Universitaria, San Nicolás de los Garza, Nuevo León, C.P. 66455, Mexico – sequence: 4 givenname: Edgar orcidid: 0000-0002-6350-3786 surname: Moctezuma fullname: Moctezuma, Edgar organization: Facultad de Ciencias Químicas, Universidad Autónoma de San Luis Potosí, Av. Manuel Nava #6, San Luis Potosí, S.L.P 78290, Mexico
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Snippet	Isostructural titanates exhibiting rectangular tunnel structure with the general formula Na2Ti6O13 and Ba3Li2Ti8O20, were synthesized by solid state and...
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SubjectTerms	Cocatalysts Hydrogen evolution Titanates Tunnel structure
Title	Photocatalytic hydrogen evolution over the isostructural titanates: Ba3Li2Ti8O20 and Na2Ti6O13 modified with metal oxide nanoparticles
URI	https://dx.doi.org/10.1016/j.ijhydene.2017.12.004
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