Sol–gel synthesis of erbium-doped yttrium silicate glass–ceramics
Yttrium silicate glasses and glass–ceramics were prepared by the sol–gel process. Yttrium nitrate was added to tetraethyl orthosilicate in amounts representing between 0.2 and 20 mol%, as well as amounts corresponding to the disilicate composition. Some samples were doped with erbium acetate. The so...
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| Published in: | Journal of non-crystalline solids Vol. 354; no. 30; pp. 3567 - 3571 |
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Elsevier B.V
15-07-2008
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| Abstract | Yttrium silicate glasses and glass–ceramics were prepared by the sol–gel process. Yttrium nitrate was added to tetraethyl orthosilicate in amounts representing between 0.2 and 20
mol%, as well as amounts corresponding to the disilicate composition. Some samples were doped with erbium acetate. The solutions underwent gellation in 2–7 days and were dried for 2 weeks. Differential thermal analysis was used to design a multi-step heat treatment to 1000
°C to densify samples to transparent or translucent monoliths. Above 1000
°C, samples crystallized to yttrium disilicate and cristobalite. Phase separation before crystallization influenced the formation of the crystal phases. |
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| AbstractList | Yttrium silicate glasses and glass–ceramics were prepared by the sol–gel process. Yttrium nitrate was added to tetraethyl orthosilicate in amounts representing between 0.2 and 20
mol%, as well as amounts corresponding to the disilicate composition. Some samples were doped with erbium acetate. The solutions underwent gellation in 2–7 days and were dried for 2 weeks. Differential thermal analysis was used to design a multi-step heat treatment to 1000
°C to densify samples to transparent or translucent monoliths. Above 1000
°C, samples crystallized to yttrium disilicate and cristobalite. Phase separation before crystallization influenced the formation of the crystal phases. |
| Author | Klein, Lisa C. Ranganathan, Varadharajan |
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| CitedBy_id | crossref_primary_10_1016_j_mssp_2018_04_017 crossref_primary_10_1111_j_1551_2916_2010_04306_x crossref_primary_10_1111_jace_13935 crossref_primary_10_1111_ijac_13938 crossref_primary_10_1007_s10971_018_4583_4 crossref_primary_10_1016_j_jeurceramsoc_2017_06_040 crossref_primary_10_1016_j_matchemphys_2016_05_022 crossref_primary_10_1016_j_jnoncrysol_2014_08_042 crossref_primary_10_1007_s10973_017_6453_7 crossref_primary_10_1080_17458080903383308 crossref_primary_10_1111_j_1551_2916_2011_04395_x crossref_primary_10_1016_j_ceramint_2019_03_157 crossref_primary_10_3938_jkps_61_858 crossref_primary_10_1016_j_jnoncrysol_2020_120499 |
| Cites_doi | 10.1016/S0925-3467(03)00262-3 10.1016/S0022-2313(02)00648-8 10.1063/1.366265 10.1063/1.120216 10.1016/0022-3093(90)90786-L 10.1063/1.109136 10.1063/1.336810 10.1007/s00339-002-1886-6 10.1023/A:1011261431938 10.1016/S1359-6454(98)00405-4 10.1021/cr010305b 10.1016/S0925-8388(01)01053-2 10.1016/S0022-3093(02)01951-8 10.1093/jmicro/dfi040 10.1016/S0022-3093(01)00716-5 10.1016/j.optmat.2004.10.018 10.1016/S0254-0584(03)00031-2 10.1063/1.1629772 10.1006/jssc.1999.8474 10.1364/OL.12.000888 10.1016/j.optmat.2004.02.023 10.1063/1.1347026 10.1557/S0883769400031018 10.1016/S0079-6727(02)00014-9 10.1016/j.jnoncrysol.2005.07.032 |
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| Keywords | Glass–ceramics Sol–gels (xerogels) 78.55.Qr 81.20.Pw Rare-earths in glasses Ternary systems Crystallization Glass Differential thermal analysis XRD Silicates Heat treatments Phase separation Glass-ceramics Chemical composition Erbium oxides Yttrium oxide Glass ceramics Sol-gel process Sol-gels (xerogels) |
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| SubjectTerms | Cross-disciplinary physics: materials science; rheology Exact sciences and technology Glasses (including metallic glasses) Glass–ceramics Materials science Physics Rare-earths in glasses Sol–gels (xerogels) Specific materials |
| Title | Sol–gel synthesis of erbium-doped yttrium silicate glass–ceramics |
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