Application of 2D correlation spectroscopy on olive stones acid hydrolysates: Effect of overliming
In order to valorize olive stones we are studying their dilute-acid hydrolysate (DAH) composition, and trying to highlight the effect of the overliming process on DAH composition in order to perform an effective treatment that maximize sugars concentrations (xylose) and minimizes the amount of toxic...
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| Published in: | Chemometrics and intelligent laboratory systems Vol. 113; pp. 58 - 67 |
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Elsevier B.V
15-04-2012
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| Abstract | In order to valorize olive stones we are studying their dilute-acid hydrolysate (DAH) composition, and trying to highlight the effect of the overliming process on DAH composition in order to perform an effective treatment that maximize sugars concentrations (xylose) and minimizes the amount of toxic materials (FF and HMF). An 2231 experimental design was established to describe the effects of three controlled factors with distinct levels: pH (10 and 12), temperature (25 and 60°C) and detoxification time (15, 30 and 60min) on the concentration of xylose, FF and HMF. A better understanding of this overliming process was possible by exploring the chromatograms obtained with 2D Correlation Spectroscopy (2DCOS). 2D correlation spectroscopy gave information about the relations that exist between chromatographic peaks and chromatograms. The order in which the constituents vary can be deduced from the sign of peaks in the synchronous and asynchronous matrices, facilitating the interpretation of kinetic studies. |
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| AbstractList | In order to valorize olive stones we are studying their dilute-acid hydrolysate (DAH) composition, and trying to highlight the effect of the overliming process on DAH composition in order to perform an effective treatment that maximize sugars concentrations (xylose) and minimizes the amount of toxic materials (FF and HMF). An 2(2)3(1) experimental design was established to describe the effects of three controlled factors with distinct levels: pH (10 and 12), temperature (25 and 60 degrees C) and detoxification time (15,30 and 60 min) on the concentration of xylose, FF and HMF. A better understanding of this overliming process was possible by exploring the chromatograms obtained with 2D Correlation Spectroscopy (2DCOS). 2D correlation spectroscopy gave information about the relations that exist between chromatographic peaks and chromatograms. The order in which the constituents vary can be deduced from the sign of peaks in the synchronous and asynchronous matrices, facilitating the interpretation of kinetic studies. (c) 2011 Published by Elsevier B.V. In order to valorize olive stones we are studying their dilute-acid hydrolysate (DAH) composition, and trying to highlight the effect of the overliming process on DAH composition in order to perform an effective treatment that maximize sugars concentrations (xylose) and minimizes the amount of toxic materials (FF and HMF). An 2231 experimental design was established to describe the effects of three controlled factors with distinct levels: pH (10 and 12), temperature (25 and 60°C) and detoxification time (15, 30 and 60min) on the concentration of xylose, FF and HMF. A better understanding of this overliming process was possible by exploring the chromatograms obtained with 2D Correlation Spectroscopy (2DCOS). 2D correlation spectroscopy gave information about the relations that exist between chromatographic peaks and chromatograms. The order in which the constituents vary can be deduced from the sign of peaks in the synchronous and asynchronous matrices, facilitating the interpretation of kinetic studies. |
| Author | Andary, Jeanne Maalouly, Jacqueline Rutledge, Douglas N. Chebib, Hanna Ouaini, Naim Ouaini, Rosette |
| Author_xml | – sequence: 1 givenname: Jeanne surname: Andary fullname: Andary, Jeanne email: jeanne_andary@hotmail.com organization: AgroParisTech, Laboratoire de Chimie Analytique, 16 rue Claude Bernard, 75005 Paris, France – sequence: 2 givenname: Jacqueline surname: Maalouly fullname: Maalouly, Jacqueline organization: URA (CNRS/USEK/UL) GREVE, Departement of Chemistry, Faculty of Science, Lebanese University, 90656, Jdaideth El Maten, Fanar, Lebanon – sequence: 3 givenname: Rosette surname: Ouaini fullname: Ouaini, Rosette organization: URA (CNRS/USEK/UL) GREVE, Departement of Chemistry, Faculty of Science, Lebanese University, 90656, Jdaideth El Maten, Fanar, Lebanon – sequence: 4 givenname: Hanna surname: Chebib fullname: Chebib, Hanna organization: URA (CNRS/USEK/UL) GREVE, Departement of Chemistry, Faculty of Science, Lebanese University, 90656, Jdaideth El Maten, Fanar, Lebanon – sequence: 5 givenname: Douglas N. surname: Rutledge fullname: Rutledge, Douglas N. organization: AgroParisTech, Laboratoire de Chimie Analytique, 16 rue Claude Bernard, 75005 Paris, France – sequence: 6 givenname: Naim surname: Ouaini fullname: Ouaini, Naim organization: URA (CNRS/USEK/UL) GREVE, Departement of Chemistry and Life Science, Université Saint-Esprit de Kaslik, 446 Jounieh, Lebanon |
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| Keywords | Xylose Hydroxyl-methylfurfural Dilute acid hydrolysate Olive stones Furfural 2DCOS DETOXIFICATION ALKALINE-DEGRADATION TOXICITY INHIBITION TEMPERATURE PRODUCTS GLUCOSE FERMENTATION LIGNOCELLULOSE CELLULOSE |
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| SubjectTerms | 2DCOS Agricultural sciences Dilute acid hydrolysate Furfural Hydroxyl-methylfurfural Life Sciences Olive stones Xylose |
| Title | Application of 2D correlation spectroscopy on olive stones acid hydrolysates: Effect of overliming |
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