Importance of film morphology on the performance of thermo-responsive waterborne pressure sensitive adhesives
[Display omitted] •Semicrystalline hard core-soft shell pressure sensitive adhesives (PSAs) were synthesized by miniemulsion polymerization.•Performance of core-shell PSAs was compared with other PSAs prepared by blending soft and hard latexes.•Better adhesive and mechanical properties were observed...
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| Published in: | European polymer journal Vol. 98; pp. 63 - 71 |
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| Main Authors: | , , , , , |
| Format: | Journal Article |
| Language: | English |
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Oxford
Elsevier Ltd
01-01-2018
Elsevier BV |
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| Abstract | [Display omitted]
•Semicrystalline hard core-soft shell pressure sensitive adhesives (PSAs) were synthesized by miniemulsion polymerization.•Performance of core-shell PSAs was compared with other PSAs prepared by blending soft and hard latexes.•Better adhesive and mechanical properties were observed for the blend adhesives.•Crystalline domains provided strong temperature-responsiveness to the blend adhesives.•Differences in performance of core-shell and blend PSAs were attributed to the differences in film morphologies.
Temperature responsive pressure sensitive adhesives (PSAs) are of interests in many applications due to the possibility of removing strong adhesives by moderate heating. In this work, semicrystalline poly(octadecyl acrylate) obtained by miniemulsion polymerization is used as a key component of the thermal responsiveness. Comparison of the adhesive performance of crystalline hard core-soft shell PSAs with other PSAs of the same overall composition and similar molar mass distributions but prepared by blending soft and hard latexes shows that the arrangement of the phases in the film play a key role in performance of the PSAs. Good adhesive performance and thermal responsiveness is only achieved when the crystalline domains are dispersed in a continuous soft phase containing entangled nanogels. Interestingly, this morphology is achieved with blends, but no with core-shell dispersions. The reasons for this difference are investigated. |
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| AbstractList | Temperature responsive pressure sensitive adhesives (PSAs) are of interests in many applications due to the possibility of removing strong adhesives by moderate heating. In this work, semicrystalline poly(octadecyl acrylate) obtained by miniemulsion polymerization is used as a key component of the thermal responsiveness. Comparison of the adhesive performance of crystalline hard core-soft shell PSAs with other PSAs of the same overall composition and similar molar mass distributions but prepared by blending soft and hard latexes shows that the arrangement of the phases in the film play a key role in performance of the PSAs. Good adhesive performance and thermal responsiveness is only achieved when the crystalline domains are dispersed in a continuous soft phase containing entangled nanogels. Interestingly, this morphology is achieved with blends, but no with core-shell dispersions. The reasons for this difference are investigated. [Display omitted] •Semicrystalline hard core-soft shell pressure sensitive adhesives (PSAs) were synthesized by miniemulsion polymerization.•Performance of core-shell PSAs was compared with other PSAs prepared by blending soft and hard latexes.•Better adhesive and mechanical properties were observed for the blend adhesives.•Crystalline domains provided strong temperature-responsiveness to the blend adhesives.•Differences in performance of core-shell and blend PSAs were attributed to the differences in film morphologies. Temperature responsive pressure sensitive adhesives (PSAs) are of interests in many applications due to the possibility of removing strong adhesives by moderate heating. In this work, semicrystalline poly(octadecyl acrylate) obtained by miniemulsion polymerization is used as a key component of the thermal responsiveness. Comparison of the adhesive performance of crystalline hard core-soft shell PSAs with other PSAs of the same overall composition and similar molar mass distributions but prepared by blending soft and hard latexes shows that the arrangement of the phases in the film play a key role in performance of the PSAs. Good adhesive performance and thermal responsiveness is only achieved when the crystalline domains are dispersed in a continuous soft phase containing entangled nanogels. Interestingly, this morphology is achieved with blends, but no with core-shell dispersions. The reasons for this difference are investigated. |
| Author | Leiza, Jose R. Reck, Bernd Gross, Michael A. Agirre, Amaia Asua, José M. Mehravar, Ehsan |
| Author_xml | – sequence: 1 givenname: Ehsan surname: Mehravar fullname: Mehravar, Ehsan organization: POLYMAT and Kimika Aplikatua Saila, Kimika Zientzien Fakultatea, University of the Basque Country UPV/EHU, Joxe Mari Korta Zentroa, Tolosa Hiribidea 72, Donostia-San Sebastian 20018, Spain – sequence: 2 givenname: Michael A. surname: Gross fullname: Gross, Michael A. organization: BASF SE, RAD Dispersions & Colloidal Materials Research – B001, Carl-Bosch-Strasse 38, 67056 Ludwigshafen, Germany – sequence: 3 givenname: Amaia surname: Agirre fullname: Agirre, Amaia organization: POLYMAT and Kimika Aplikatua Saila, Kimika Zientzien Fakultatea, University of the Basque Country UPV/EHU, Joxe Mari Korta Zentroa, Tolosa Hiribidea 72, Donostia-San Sebastian 20018, Spain – sequence: 4 givenname: Bernd surname: Reck fullname: Reck, Bernd organization: BASF SE, RAD Dispersions & Colloidal Materials Research – B001, Carl-Bosch-Strasse 38, 67056 Ludwigshafen, Germany – sequence: 5 givenname: Jose R. surname: Leiza fullname: Leiza, Jose R. organization: POLYMAT and Kimika Aplikatua Saila, Kimika Zientzien Fakultatea, University of the Basque Country UPV/EHU, Joxe Mari Korta Zentroa, Tolosa Hiribidea 72, Donostia-San Sebastian 20018, Spain – sequence: 6 givenname: José M. surname: Asua fullname: Asua, José M. email: jm.asua@ehu.es organization: POLYMAT and Kimika Aplikatua Saila, Kimika Zientzien Fakultatea, University of the Basque Country UPV/EHU, Joxe Mari Korta Zentroa, Tolosa Hiribidea 72, Donostia-San Sebastian 20018, Spain |
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| Keywords | Temperature-responsive behavior Blend Miniemulsion polymerization Mechanical properties Crystallinity Adhesive properties Pressure-sensitive adhesives Core-shell |
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•Semicrystalline hard core-soft shell pressure sensitive adhesives (PSAs) were synthesized by miniemulsion polymerization.•Performance of... Temperature responsive pressure sensitive adhesives (PSAs) are of interests in many applications due to the possibility of removing strong adhesives by... |
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| SubjectTerms | Adhesive properties Adhesives Blend Core-shell Crystal structure Crystallinity Emulsion polymerization Mechanical properties Miniemulsion polymerization Morphology Pressure sensitive adhesives Temperature-responsive behavior |
| Title | Importance of film morphology on the performance of thermo-responsive waterborne pressure sensitive adhesives |
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