Equilibrium and kinetics of sorption and resorption of acid and basic dyes using the pulp of carob pods

Being an abundant product in Algeria, pulp of carob pods (PCP) was used in this study as a biosorbent for Methylene blue (MB) and Congo red (CR) removal from aqueous media in batch mode in two successive steps. Once the first dye is adsorbed, the biosorbent is used as is to adsorb the second dye in...

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Published in:	Journal of dispersion science and technology Vol. 44; no. 11; pp. 2137 - 2149
Main Authors:	Seghier, Abdelkarim, Boucherdoud, Ahmed, Seghier, Soraya, Benderdouche, Noureddine, Hadjel, Mohammed, Bestani, Benaouda
Format:	Journal Article
Language:	English
Published:	Philadelphia Taylor & Francis 01-09-2023 Taylor & Francis Ltd
Subjects:	Aqueous solutions Basic dyes Biosorption Carob pods congo red Dyes Functional groups Kinetics Methylene blue pulp of carob pods solid reuse
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Abstract	Being an abundant product in Algeria, pulp of carob pods (PCP) was used in this study as a biosorbent for Methylene blue (MB) and Congo red (CR) removal from aqueous media in batch mode in two successive steps. Once the first dye is adsorbed, the biosorbent is used as is to adsorb the second dye in order to study the interactions between them. Characterization of PCP by FTIR spectroscopy, Scanning Electron Microscopy (SEM), EDX, and point of zero charge showed that the principal functional groups present at the surface are oxygenated with a pH pzc value of the 7.2. Contact time of 60 min was amply sufficient to reach equilibrium for both dyes onto PCP and recuperated biosorbents. pH effect on the biosorption onto PCP shows a behavioral divergence between both dyes. Maximum biosorption uptake of CR was observed at pH value of 6.38 while pH variation has no remarkable influence on MB biosorption and the initial pH solution of 5.75 was taken for subsequent biosorption experiments. The adsorption isotherms obtained are in good agreement with the models of Langmuir and Freundlich and the kinetics are well described by the pseudo-second-order model.
AbstractList	Being an abundant product in Algeria, pulp of carob pods (PCP) was used in this study as a biosorbent for Methylene blue (MB) and Congo red (CR) removal from aqueous media in batch mode in two successive steps. Once the first dye is adsorbed, the biosorbent is used as is to adsorb the second dye in order to study the interactions between them. Characterization of PCP by FTIR spectroscopy, Scanning Electron Microscopy (SEM), EDX, and point of zero charge showed that the principal functional groups present at the surface are oxygenated with a pHpzc value of the 7.2. Contact time of 60 min was amply sufficient to reach equilibrium for both dyes onto PCP and recuperated biosorbents. pH effect on the biosorption onto PCP shows a behavioral divergence between both dyes. Maximum biosorption uptake of CR was observed at pH value of 6.38 while pH variation has no remarkable influence on MB biosorption and the initial pH solution of 5.75 was taken for subsequent biosorption experiments. The adsorption isotherms obtained are in good agreement with the models of Langmuir and Freundlich and the kinetics are well described by the pseudo-second-order model. Being an abundant product in Algeria, pulp of carob pods (PCP) was used in this study as a biosorbent for Methylene blue (MB) and Congo red (CR) removal from aqueous media in batch mode in two successive steps. Once the first dye is adsorbed, the biosorbent is used as is to adsorb the second dye in order to study the interactions between them. Characterization of PCP by FTIR spectroscopy, Scanning Electron Microscopy (SEM), EDX, and point of zero charge showed that the principal functional groups present at the surface are oxygenated with a pH pzc value of the 7.2. Contact time of 60 min was amply sufficient to reach equilibrium for both dyes onto PCP and recuperated biosorbents. pH effect on the biosorption onto PCP shows a behavioral divergence between both dyes. Maximum biosorption uptake of CR was observed at pH value of 6.38 while pH variation has no remarkable influence on MB biosorption and the initial pH solution of 5.75 was taken for subsequent biosorption experiments. The adsorption isotherms obtained are in good agreement with the models of Langmuir and Freundlich and the kinetics are well described by the pseudo-second-order model.
Author	Seghier, Abdelkarim Hadjel, Mohammed Benderdouche, Noureddine Seghier, Soraya Bestani, Benaouda Boucherdoud, Ahmed
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SubjectTerms	Aqueous solutions Basic dyes Biosorption Carob pods congo red Dyes Functional groups Kinetics Methylene blue pulp of carob pods solid reuse
Title	Equilibrium and kinetics of sorption and resorption of acid and basic dyes using the pulp of carob pods
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