Enhancing the recovery and concentration of polyphenols from camu-camu (Myrciaria dubia H.B.K. McVaugh) by aqueous two-phase flotation and scale-up process

In this study, polyphenols obtained from camu-camu pulp residue were recovered and concentrated from aqueous two-phase flotation (ATPF) by evaluating different operating conditions, such as solvent type, pH, ammonium sulfate concentration, flotation time, air flow, and volumetric ratio. Under optima...

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Published in:	Separation science and technology Vol. 53; no. 13; pp. 2126 - 2135
Main Authors:	de Araújo Padilha, Carlos Eduardo, Dantas, Paulo Victor Fortunato, Nogueira, Cleitiane da Costa, Leitão, Ana Laura de Sá, Almeida, Hanna Nóbrega, de Santana Souza, Domingos Fabiano, Oliveira, Jackson Araújo de, de Macedo, Gorete Ribeiro, dos Santos, Everaldo Silvino
Format:	Journal Article
Language:	English
Published:	Abingdon Taylor & Francis 02-09-2018 Taylor & Francis Ltd
Subjects:	Air flow Ammonium Ammonium compounds Ammonium sulfate Aqueous two-phase flotation camu-camu concentration Flotation Polyethylene glycol Polyphenols scale-up Sulfates
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Abstract	In this study, polyphenols obtained from camu-camu pulp residue were recovered and concentrated from aqueous two-phase flotation (ATPF) by evaluating different operating conditions, such as solvent type, pH, ammonium sulfate concentration, flotation time, air flow, and volumetric ratio. Under optimal conditions, the polyethylene glycol 400/ammonium sulfate ATPF system showed an efficiency of 81.02% and a concentration coefficient two times higher than traditional aqueous two-phase extraction. Experiments were also carried out on a semi-pilot scale, using an apparatus with a 2.5-L working volume. The results showed that the semi-pilot system was comparable to the smaller scale system.
AbstractList	In this study, polyphenols obtained from camu-camu pulp residue were recovered and concentrated from aqueous two-phase flotation (ATPF) by evaluating different operating conditions, such as solvent type, pH, ammonium sulfate concentration, flotation time, air flow, and volumetric ratio. Under optimal conditions, the polyethylene glycol 400/ammonium sulfate ATPF system showed an efficiency of 81.02% and a concentration coefficient two times higher than traditional aqueous two-phase extraction. Experiments were also carried out on a semi-pilot scale, using an apparatus with a 2.5-L working volume. The results showed that the semi-pilot system was comparable to the smaller scale system.
Author	dos Santos, Everaldo Silvino Leitão, Ana Laura de Sá Almeida, Hanna Nóbrega Oliveira, Jackson Araújo de de Santana Souza, Domingos Fabiano de Macedo, Gorete Ribeiro Nogueira, Cleitiane da Costa de Araújo Padilha, Carlos Eduardo Dantas, Paulo Victor Fortunato
Author_xml	– sequence: 1 givenname: Carlos Eduardo surname: de Araújo Padilha fullname: de Araújo Padilha, Carlos Eduardo email: carlospadilha.eq@gmail.com organization: Laboratory of Biochemical Engineering, Chemical Engineering Department, Federal University of Rio Grande do Norte (UFRN) – sequence: 2 givenname: Paulo Victor Fortunato surname: Dantas fullname: Dantas, Paulo Victor Fortunato organization: Laboratory of Biochemical Engineering, Chemical Engineering Department, Federal University of Rio Grande do Norte (UFRN) – sequence: 3 givenname: Cleitiane da Costa surname: Nogueira fullname: Nogueira, Cleitiane da Costa organization: Laboratory of Biochemical Engineering, Chemical Engineering Department, Federal University of Rio Grande do Norte (UFRN) – sequence: 4 givenname: Ana Laura de Sá surname: Leitão fullname: Leitão, Ana Laura de Sá organization: Laboratory of Biochemical Engineering, Chemical Engineering Department, Federal University of Rio Grande do Norte (UFRN) – sequence: 5 givenname: Hanna Nóbrega surname: Almeida fullname: Almeida, Hanna Nóbrega organization: Laboratory of Biochemical Engineering, Chemical Engineering Department, Federal University of Rio Grande do Norte (UFRN) – sequence: 6 givenname: Domingos Fabiano surname: de Santana Souza fullname: de Santana Souza, Domingos Fabiano organization: Laboratory of Biochemical Engineering, Chemical Engineering Department, Federal University of Rio Grande do Norte (UFRN) – sequence: 7 givenname: Jackson Araújo de surname: Oliveira fullname: Oliveira, Jackson Araújo de organization: Laboratory of Biochemical Engineering, Chemical Engineering Department, Federal University of Rio Grande do Norte (UFRN) – sequence: 8 givenname: Gorete Ribeiro surname: de Macedo fullname: de Macedo, Gorete Ribeiro organization: Laboratory of Biochemical Engineering, Chemical Engineering Department, Federal University of Rio Grande do Norte (UFRN) – sequence: 9 givenname: Everaldo Silvino surname: dos Santos fullname: dos Santos, Everaldo Silvino organization: Laboratory of Biochemical Engineering, Chemical Engineering Department, Federal University of Rio Grande do Norte (UFRN)
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SubjectTerms	Air flow Ammonium Ammonium compounds Ammonium sulfate Aqueous two-phase flotation camu-camu concentration Flotation Polyethylene glycol Polyphenols scale-up Sulfates
Title	Enhancing the recovery and concentration of polyphenols from camu-camu (Myrciaria dubia H.B.K. McVaugh) by aqueous two-phase flotation and scale-up process
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