Enhancing water resistance of welded dowel wood joints by acetylated lignin

Low molecular mass acetylated organosolv lignin from wheat straw and from depolymerised low sulphur organosolv wood lignin have been shown to markedly improve both the water resistance and the mechanical performance of welded dowel wood joints. The acetylated oligomers distribution and extent of ace...

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Published in:	Journal of adhesion science and technology Vol. 27; no. 3; pp. 252 - 262
Main Authors:	Pizzi, A., Zhou, X., Navarrete, P., Segovia, C., Mansouri, H.R., Placentia Pena, M.I., Pichelin, F.
Format:	Journal Article
Language:	English
Published:	Abingdon Routledge 01-02-2013 Taylor & Francis
Subjects:	acetylated lignin Applied sciences biosourced additives Degradation and preservation ductile behaviour environment friendly Exact sciences and technology interpenetrating network lignin Polymer industry, paints, wood water resistance waterproofing additives welded dowels Wood wood welding Wood. Paper. Non wovens Lignin ductile behaviour Welding water resistance Oligomer interpenetrating network Straw Additive Welded joint acetylated lignin Chemical composition Acetylation Agricultural waste Chemical properties environment friendly Lignin derivatives wood welding biosourced additives welded dowels Mechanical properties Hardwood Tensile property Experimental study waterproofing additives Wood preservative Chemical modification Peg Waterproofness Cereal Wheat
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Abstract	Low molecular mass acetylated organosolv lignin from wheat straw and from depolymerised low sulphur organosolv wood lignin have been shown to markedly improve both the water resistance and the mechanical performance of welded dowel wood joints. The acetylated oligomers distribution and extent of acetylation of the two lignins were determined by Matrix assisted laser desorption ionization-time-of-flight mass spectrometry. Extensive acetylation was confirmed by CP-MAS 13 C NMR spectrometry. Force-displacement measurements on welded dowel joints to which acetylated wood lignins were added showed a ductile behaviour. This is due to the interpenetration of the elastic acetylated lignin network into the more rigid composite network of the welded interphase.
AbstractList	Low molecular mass acetylated organosolv lignin from wheat straw and from depolymerised low sulphur organosolv wood lignin have been shown to markedly improve both the water resistance and the mechanical performance of welded dowel wood joints. The acetylated oligomers distribution and extent of acetylation of the two lignins were determined by Matrix assisted laser desorption ionization-time-of-flight mass spectrometry. Extensive acetylation was confirmed by CP-MAS 13 C NMR spectrometry. Force-displacement measurements on welded dowel joints to which acetylated wood lignins were added showed a ductile behaviour. This is due to the interpenetration of the elastic acetylated lignin network into the more rigid composite network of the welded interphase.
Author	Pizzi, A. Segovia, C. Placentia Pena, M.I. Mansouri, H.R. Pichelin, F. Navarrete, P. Zhou, X.
Author_xml	– sequence: 1 givenname: A. surname: Pizzi fullname: Pizzi, A. email: antonio.pizzi@enstib.uhp-nancy.fr organization: ENSTIB, University of Lorraine – sequence: 2 givenname: X. surname: Zhou fullname: Zhou, X. organization: ENSTIB, University of Lorraine – sequence: 3 givenname: P. surname: Navarrete fullname: Navarrete, P. organization: ENSTIB, University of Lorraine – sequence: 4 givenname: C. surname: Segovia fullname: Segovia, C. organization: ENSTIB, University of Lorraine – sequence: 5 givenname: H.R. surname: Mansouri fullname: Mansouri, H.R. organization: Department of Wood Science and Technology , Zabol University – sequence: 6 givenname: M.I. surname: Placentia Pena fullname: Placentia Pena, M.I. organization: Architecture, Wood and Civil Engineering , Bern University of Applied Sciences – sequence: 7 givenname: F. surname: Pichelin fullname: Pichelin, F. organization: Architecture, Wood and Civil Engineering , Bern University of Applied Sciences
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Cites_doi	10.1002/(SICI)1097-4628(19971010)66:2<255::AID-APP6>3.0.CO;2-V 10.1163/156856108X335595 10.1515/hfsg.1996.50.3.215 10.1163/1568561041588192 10.1163/156856104839310 10.1002/app.1994.070510723 10.1163/156856107781393910 10.1163/156856105774429037 10.1163/156856106777144327 10.1002/app.25098 10.1002/(SICI)1097-4628(20000725)77:4<841::AID-APP18>3.0.CO;2-0 10.1163/156856108X306939 10.1163/156856105774382444 10.1007/s00107-007-0220-6 10.1002/app.23714 10.1002/app.1993.070491212 10.1163/156856103769207419 10.1163/016942411X556088 10.1002/app.24744
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Keywords	Lignin ductile behaviour Welding water resistance Oligomer interpenetrating network Straw Additive Welded joint acetylated lignin Chemical composition Acetylation Agricultural waste Chemical properties environment friendly Lignin derivatives wood welding biosourced additives welded dowels Mechanical properties Hardwood Tensile property Experimental study waterproofing additives Wood preservative Chemical modification Peg Waterproofness Cereal Wheat
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SubjectTerms	acetylated lignin Applied sciences biosourced additives Degradation and preservation ductile behaviour environment friendly Exact sciences and technology interpenetrating network lignin Polymer industry, paints, wood water resistance waterproofing additives welded dowels Wood wood welding Wood. Paper. Non wovens
Title	Enhancing water resistance of welded dowel wood joints by acetylated lignin
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