Optimization and kinetic modeling of waste lard methanolysis in a continuous reciprocating plate reactor
Continuous biodiesel production from a waste pig-roasting lard, methanol and KOH was carried out in a reciprocating plate reactor (RPR) using a factorial design containing three process factors, namely methanol/lard molar ratio, catalyst loading, and normalized height of the reactor. The main goals...
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| Published in: | Chinese journal of chemical engineering Vol. 27; no. 10; pp. 2481 - 2490 |
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| Main Authors: | , , , , , |
| Format: | Journal Article |
| Language: | English |
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Elsevier B.V
01-10-2019
University of Ni?, Faculty of Technology, Bulevar oslobo?enja 124, Leskovac 16000, Serbia%University of Belgrade, Faculty of Technology and Metallurgy, Karnegijeva 4, Belgrade 11000, Serbia%University of Ni?, Faculty of Technology, Bulevar oslobo?enja 124, Leskovac 16000, Serbia Serbian Academy of Sciences and Arts (SASA), Knez Mihailova 35, Belgrade 11000, Serbia |
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| Abstract | Continuous biodiesel production from a waste pig-roasting lard, methanol and KOH was carried out in a reciprocating plate reactor (RPR) using a factorial design containing three process factors, namely methanol/lard molar ratio, catalyst loading, and normalized height of the reactor. The main goals were to optimize the influential process factors with respect to biodiesel purity using the response surface methodology and to model the kinetics of the transesterification reaction in order to describe the change of triacylglycerols (TAG) and fatty acid methyl esters (FAME) concentrations along the RPR height. The first-order rate law was proved for both the reaction and the mass transfer. The model of the changing reaction mechanism and mass transfer of TAG was also applicable. Both kinetic models agreed with the experimental concentrations of TAG and FAME determined along the RPR height. |
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| AbstractList | Continuous biodiesel production from a waste pig-roasting lard, methanol and KOH was carried out in a reciprocating plate reactor (RPR) using a factorial design containing three process factors, namely methanol/lard molar ratio, catalyst loading, and normalized height of the reactor. The main goals were to optimize the influential process factors with respect to biodiesel purity using the response surface methodology and to model the kinetics of the transesterification reaction in order to describe the change of triacylglycerols (TAG) and fatty acid methyl esters (FAME) concentrations along the RPR height. The first-order rate law was proved for both the reaction and the mass transfer. The model of the changing reaction mechanism and mass transfer of TAG was also applicable. Both kinetic models agreed with the experimental concentrations of TAG and FAME determined along the RPR height. |
| Author | Veličković, Ana V. Stamenković, Olivera S. Stojković, Ivan J. Veljković, Vlada B. Banković-Ilić, Ivana B. Miladinović, Marija R. |
| AuthorAffiliation | University of Ni?, Faculty of Technology, Bulevar oslobo?enja 124, Leskovac 16000, Serbia%University of Belgrade, Faculty of Technology and Metallurgy, Karnegijeva 4, Belgrade 11000, Serbia%University of Ni?, Faculty of Technology, Bulevar oslobo?enja 124, Leskovac 16000, Serbia;Serbian Academy of Sciences and Arts (SASA), Knez Mihailova 35, Belgrade 11000, Serbia |
| AuthorAffiliation_xml | – name: University of Ni?, Faculty of Technology, Bulevar oslobo?enja 124, Leskovac 16000, Serbia%University of Belgrade, Faculty of Technology and Metallurgy, Karnegijeva 4, Belgrade 11000, Serbia%University of Ni?, Faculty of Technology, Bulevar oslobo?enja 124, Leskovac 16000, Serbia;Serbian Academy of Sciences and Arts (SASA), Knez Mihailova 35, Belgrade 11000, Serbia |
| Author_xml | – sequence: 1 givenname: Marija R. surname: Miladinović fullname: Miladinović, Marija R. organization: University of Niš, Faculty of Technology, Bulevar oslobođenja 124, Leskovac 16000, Serbia – sequence: 2 givenname: Ivan J. surname: Stojković fullname: Stojković, Ivan J. organization: University of Belgrade, Faculty of Technology and Metallurgy, Karnegijeva 4, Belgrade 11000, Serbia – sequence: 3 givenname: Ana V. surname: Veličković fullname: Veličković, Ana V. organization: University of Niš, Faculty of Technology, Bulevar oslobođenja 124, Leskovac 16000, Serbia – sequence: 4 givenname: Olivera S. surname: Stamenković fullname: Stamenković, Olivera S. organization: University of Niš, Faculty of Technology, Bulevar oslobođenja 124, Leskovac 16000, Serbia – sequence: 5 givenname: Ivana B. surname: Banković-Ilić fullname: Banković-Ilić, Ivana B. organization: University of Niš, Faculty of Technology, Bulevar oslobođenja 124, Leskovac 16000, Serbia – sequence: 6 givenname: Vlada B. surname: Veljković fullname: Veljković, Vlada B. email: veljkovic@tf.ni.ac.rs organization: University of Niš, Faculty of Technology, Bulevar oslobođenja 124, Leskovac 16000, Serbia |
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| CitedBy_id | crossref_primary_10_12677_CES_2020_85110 crossref_primary_10_1002_bbb_2186 crossref_primary_10_1016_j_bcab_2020_101558 crossref_primary_10_3390_catal10111266 crossref_primary_10_1016_j_renene_2020_12_055 crossref_primary_10_1002_bbb_2094 crossref_primary_10_3390_mi12020120 |
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| Copyright | 2019 Elsevier B.V. Copyright © Wanfang Data Co. Ltd. All Rights Reserved. |
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| Keywords | Waste lard Reciprocating plate reactor Kinetics Biodiesel Optimization |
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| Title | Optimization and kinetic modeling of waste lard methanolysis in a continuous reciprocating plate reactor |
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