Synthesis, structural, dielectric and magnetic properties of cobalt ferrite nanomaterial prepared by sol-gel autocombustion technique
Cubic spinel structured CoFe2O4 nanocrystalline material has been synthesized using the sol-gel auto combustion route. Structural parameters and phase formation were studied using room temperature powder X-ray diffraction (XRD). The result shows a pure cubic spinel structured sample formation with a...
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| Published in: | Physica. B, Condensed matter Vol. 581; p. 411769 |
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| Main Authors: | , , , , , , , , , |
| Format: | Journal Article |
| Language: | English |
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Elsevier B.V
15-03-2020
Elsevier BV |
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| Abstract | Cubic spinel structured CoFe2O4 nanocrystalline material has been synthesized using the sol-gel auto combustion route. Structural parameters and phase formation were studied using room temperature powder X-ray diffraction (XRD). The result shows a pure cubic spinel structured sample formation with a lattice parameter of 8.4277 Å. Field emission scanning electron microscopy (FESEM) microstructural characterization revealed the nanocrystalline structure of the so synthesized sample with non-homogeneous grain sizes and grain shapes. Fourier transform infrared (FT-IR) characterization confirmed the spinel structure formation by exhibiting the cation stretching-vibrations at the tetrahedral and octahedral sites. The DC resistivity measurement has been carried out using a two-probe technique and confirmed the high resistive nature of the sample. The room temperature dielectric and AC properties were investigated in the frequency ranges of 100 Hz–5 MHz. The dielectric dispersion has been observed at lower frequencies. Higher magnetization value has been measured using the VSM technique. |
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| AbstractList | Cubic spinel structured CoFe2O4 nanocrystalline material has been synthesized using the sol-gel auto combustion route. Structural parameters and phase formation were studied using room temperature powder X-ray diffraction (XRD). The result shows a pure cubic spinel structured sample formation with a lattice parameter of 8.4277 Å. Field emission scanning electron microscopy (FESEM) microstructural characterization revealed the nanocrystalline structure of the so synthesized sample with non-homogeneous grain sizes and grain shapes. Fourier transform infrared (FT-IR) characterization confirmed the spinel structure formation by exhibiting the cation stretching-vibrations at the tetrahedral and octahedral sites. The DC resistivity measurement has been carried out using a two-probe technique and confirmed the high resistive nature of the sample. The room temperature dielectric and AC properties were investigated in the frequency ranges of 100 Hz–5 MHz. The dielectric dispersion has been observed at lower frequencies. Higher magnetization value has been measured using the VSM technique. |
| ArticleNumber | 411769 |
| Author | Margarette, S.J. Vemuri, Raghavendra Ramakrishna, Y. Samatha, K. Vijaya Prasad, K.L. Mammo, Tulu Wegayehu Murali, N. Kumari, Ch Vijaya Ramakrishna, A. Shankar Rao, Y.B. |
| Author_xml | – sequence: 1 givenname: Tulu Wegayehu surname: Mammo fullname: Mammo, Tulu Wegayehu organization: Aksum University, Tigrai, Ethiopia – sequence: 2 givenname: N. surname: Murali fullname: Murali, N. email: muraliphdau@gmail.com organization: Department of Physics, Andhra University College of Engineering (A), Andhra University, Visakhapatnam, Andhra Pradesh, 530003, India – sequence: 3 givenname: Ch Vijaya surname: Kumari fullname: Kumari, Ch Vijaya organization: Department of Physics, SS&N College, Narasaraopet, Guntur, India – sequence: 4 givenname: S.J. surname: Margarette fullname: Margarette, S.J. organization: Department of Physics, Andhra University, Visakhapatnam, Andhra Pradesh, India – sequence: 5 givenname: A. surname: Ramakrishna fullname: Ramakrishna, A. organization: Department of Physics, Aditya College of Engineering and Technology (ACET), Surampalem, East Godavari, Andhra Pradesh, India – sequence: 6 givenname: Raghavendra surname: Vemuri fullname: Vemuri, Raghavendra organization: Department of Physics, Aditya College of Engineering and Technology (ACET), Surampalem, East Godavari, Andhra Pradesh, India – sequence: 7 givenname: Y.B. surname: Shankar Rao fullname: Shankar Rao, Y.B. organization: Department of Physics, Anil Neerukonda Institute of Technology & Sciences, Bheemunipatnam, Visakhapatnam, India – sequence: 8 givenname: K.L. surname: Vijaya Prasad fullname: Vijaya Prasad, K.L. organization: Department of ECE, Aditya College of Engineering and Technology (ACET), Surampalem, East Godavari, Andhra Pradesh, India – sequence: 9 givenname: Y. surname: Ramakrishna fullname: Ramakrishna, Y. organization: Department of Physics, Andhra University College of Engineering (A), Andhra University, Visakhapatnam, Andhra Pradesh, 530003, India – sequence: 10 givenname: K. surname: Samatha fullname: Samatha, K. organization: Department of Physics, Andhra University, Visakhapatnam, Andhra Pradesh, India |
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| Snippet | Cubic spinel structured CoFe2O4 nanocrystalline material has been synthesized using the sol-gel auto combustion route. Structural parameters and phase... |
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| SubjectTerms | Cobalt ferrites CoFe2O4 Crystal structure Cubic lattice DC resistivity Dielectric properties Electric resistance Field emission microscopy Fourier transforms Frequency ranges Grain size Magnetic properties Nanocrystalline Nanocrystals Nanomaterials NH3 Parameters Room temperature Sol-gel processes Spinel Spinel-structured Structural analysis Synthesis X ray powder diffraction |
| Title | Synthesis, structural, dielectric and magnetic properties of cobalt ferrite nanomaterial prepared by sol-gel autocombustion technique |
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