Membranes of polysulfone and hybrid applied in dye separation
In this work, polysulfone (PSU) membranes were prepared with 1.0%, 3.0%, and 5.0% by weight of titanium dioxide (TiO2). The membranes were analyzed by viscosity, X-ray diffraction (XRD), Fourier transform infrared spectroscopy (FTIR), scanning electron microscopy (SEM), water vapor permeation, conta...
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| Published in: | Desalination and water treatment Vol. 230; pp. 298 - 309 |
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| Format: | Journal Article |
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01-08-2021
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| Abstract | In this work, polysulfone (PSU) membranes were prepared with 1.0%, 3.0%, and 5.0% by weight of titanium dioxide (TiO2). The membranes were analyzed by viscosity, X-ray diffraction (XRD), Fourier transform infrared spectroscopy (FTIR), scanning electron microscopy (SEM), water vapor permeation, contact angle (CA), flow measurements (FM), and yield. Through XRD and FTIR, the PSU membranes and their hybrids showed peaks and bands characteristic of PSU and TiO2 structure. By SEM and viscosity, it was observed that the addition of TiO2 promoted the formation of agglomerates on its surface, in addition to increasing the viscosities and thickness of these membranes. Through the CA and of water vapor permeation, it was found that the PSU membrane had the higher angle value and the smallest vapor permeation, probably because it presents a smooth filter skin with few pores and low interconnectivity of these with the porous layer. The separation tests indicated a decrease in flow, due to the fouling formed on the membranes surface and a significant reduction of dye in permeate, allowing the treatment of this contaminant. Furthermore, TiO2 for being a hydrophilic material and for acting as a porogenic agent, facilitated the passage of water, favoring the dye separation by hybrid membranes. |
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| AbstractList | In this work, polysulfone (PSU) membranes were prepared with 1.0%, 3.0%, and 5.0% by weight of titanium dioxide (TiO2). The membranes were analyzed by viscosity, X-ray diffraction (XRD), Fourier transform infrared spectroscopy (FTIR), scanning electron microscopy (SEM), water vapor permeation, contact angle (CA), flow measurements (FM), and yield. Through XRD and FTIR, the PSU membranes and their hybrids showed peaks and bands characteristic of PSU and TiO2 structure. By SEM and viscosity, it was observed that the addition of TiO2 promoted the formation of agglomerates on its surface, in addition to increasing the viscosities and thickness of these membranes. Through the CA and of water vapor permeation, it was found that the PSU membrane had the higher angle value and the smallest vapor permeation, probably because it presents a smooth filter skin with few pores and low interconnectivity of these with the porous layer. The separation tests indicated a decrease in flow, due to the fouling formed on the membranes surface and a significant reduction of dye in permeate, allowing the treatment of this contaminant. Furthermore, TiO2 for being a hydrophilic material and for acting as a porogenic agent, facilitated the passage of water, favoring the dye separation by hybrid membranes. |
| Author | Araújo, Bruna Aline Araújo, Edcleide Maria de Lima, Carlos Antônio Pereira Oliveira, Sandriely Sonaly Lima da Silva Barbosa Ferreira, Rodholfo de Medeiros, Keila Machado |
| Author_xml | – sequence: 1 givenname: Bruna Aline surname: Araújo fullname: Araújo, Bruna Aline email: brunaaaraujo15@gmail.com organization: Sanitary and Environmental Engineering Department, State University of Paraiba, Avenue Baraunas, 351 Bodocongo, 58429-500 Campina Grande, Paraiba, Brazil – sequence: 2 givenname: Edcleide Maria surname: Araújo fullname: Araújo, Edcleide Maria email: edcleide.araujo@ufcg.edu.br organization: Materials Engineering Department, Federal University of Campina Grande, Avenue Aprigio Veloso, 882 Bodocongo, 58429-900 Campina Grande, Paraiba, Brazil – sequence: 3 givenname: Sandriely Sonaly Lima surname: Oliveira fullname: Oliveira, Sandriely Sonaly Lima email: sandrielysonaly1@gmail.com organization: Materials Engineering Department, Federal University of Campina Grande, Avenue Aprigio Veloso, 882 Bodocongo, 58429-900 Campina Grande, Paraiba, Brazil – sequence: 4 givenname: Rodholfo surname: da Silva Barbosa Ferreira fullname: da Silva Barbosa Ferreira, Rodholfo email: rodholfoferreira@gmail.com organization: Materials Engineering Department, Federal University of Campina Grande, Avenue Aprigio Veloso, 882 Bodocongo, 58429-900 Campina Grande, Paraiba, Brazil – sequence: 5 givenname: Keila Machado surname: de Medeiros fullname: de Medeiros, Keila Machado email: keilamedeiros@ufrb.edu.br organization: Science and Technology Center in Energy and Sustainability, Federal University of Reconcavo da Bahia, Street Godofredo Rebello de Figueiredo Filho, 697 Sim, 44085-132 Feira de Santana, Bahia, Brazil – sequence: 6 givenname: Carlos Antônio Pereira surname: de Lima fullname: de Lima, Carlos Antônio Pereira email: caplima@uepb.edu.br organization: Sanitary and Environmental Engineering Department, State University of Paraiba, Avenue Baraunas, 351 Bodocongo, 58429-500 Campina Grande, Paraiba, Brazil |
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| Keywords | Phase inversion Membranes Hybrids Industrial effluent |
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| Title | Membranes of polysulfone and hybrid applied in dye separation |
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