Synthesis and Structure of Tetraphenylantimony Methacrylate and Tetraphenylantimony Crotonate and Their Use for the Production of Antimony-Containing Polystyrene
Tetraphenylantimony methacrylate Ph 4 SbO 2 CC(CH 3 )=CH 2 and tetraphenylantimony crotonate Ph 4 SbO 2 CCH=CHCH 3 were synthesized by the action of acids on Ph 5 Sb or on Ph 4 SbBr in the presence of Et 2 NH. According to X-ray diffraction analysis data, both compounds are antimony complexes with d...
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| Published in: | Russian journal of general chemistry Vol. 91; no. 2; pp. 227 - 234 |
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| Main Authors: | , , , , , , |
| Format: | Journal Article |
| Language: | English |
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Pleiades Publishing
01-02-2021
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| Abstract | Tetraphenylantimony methacrylate Ph
4
SbO
2
CC(CH
3
)=CH
2
and tetraphenylantimony crotonate Ph
4
SbO
2
CCH=CHCH
3
were synthesized by the action of acids on Ph
5
Sb or on Ph
4
SbBr in the presence of Et
2
NH. According to X-ray diffraction analysis data, both compounds are antimony complexes with distorted tetragonal-pyramidal geometry. Polymerization of styrene with Ph
4
SbO
2
CC(CH
3
)=CH
2
and Ph
4
SbO
2
CCH=CHCH
3
additives gave transparent antimony-containing polystyrene soluble in chloroform, dichloromethane, and THF. |
|---|---|
| AbstractList | Tetraphenylantimony methacrylate Ph
4
SbO
2
CC(CH
3
)=CH
2
and tetraphenylantimony crotonate Ph
4
SbO
2
CCH=CHCH
3
were synthesized by the action of acids on Ph
5
Sb or on Ph
4
SbBr in the presence of Et
2
NH. According to X-ray diffraction analysis data, both compounds are antimony complexes with distorted tetragonal-pyramidal geometry. Polymerization of styrene with Ph
4
SbO
2
CC(CH
3
)=CH
2
and Ph
4
SbO
2
CCH=CHCH
3
additives gave transparent antimony-containing polystyrene soluble in chloroform, dichloromethane, and THF. Tetraphenylantimony methacrylate Ph.sub.4SbO.sub.2CC(CH.sub.3)=CH.sub.2 and tetraphenylantimony crotonate Ph.sub.4SbO.sub.2CCH=CHCH.sub.3 were synthesized by the action of acids on Ph.sub.5Sb or on Ph.sub.4SbBr in the presence of Et.sub.2NH. According to X-ray diffraction analysis data, both compounds are antimony complexes with distorted tetragonal-pyramidal geometry. Polymerization of styrene with Ph.sub.4SbO.sub.2CC(CH.sub.3)=CH.sub.2 and Ph.sub.4SbO.sub.2CCH=CHCH.sub.3 additives gave transparent antimony-containing polystyrene soluble in chloroform, dichloromethane, and THF. |
| Audience | Academic |
| Author | Ovsetsina, T. I. Gushchin, A. V. Maleeva, A. I. Somov, N. V. Tumanyan, A. S. Kipelkin, E. V. Andreev, P. V. |
| Author_xml | – sequence: 1 givenname: A. V. surname: Gushchin fullname: Gushchin, A. V. email: gushchin4@yandex.ru organization: Lobachevsky State University of Nizhny Novgorod – sequence: 2 givenname: A. I. surname: Maleeva fullname: Maleeva, A. I. organization: Lobachevsky State University of Nizhny Novgorod – sequence: 3 givenname: E. V. surname: Kipelkin fullname: Kipelkin, E. V. organization: Lobachevsky State University of Nizhny Novgorod – sequence: 4 givenname: A. S. surname: Tumanyan fullname: Tumanyan, A. S. organization: Lobachevsky State University of Nizhny Novgorod – sequence: 5 givenname: P. V. surname: Andreev fullname: Andreev, P. V. organization: Lobachevsky State University of Nizhny Novgorod – sequence: 6 givenname: T. I. surname: Ovsetsina fullname: Ovsetsina, T. I. organization: Lobachevsky State University of Nizhny Novgorod – sequence: 7 givenname: N. V. surname: Somov fullname: Somov, N. V. organization: Lobachevsky State University of Nizhny Novgorod |
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| CitedBy_id | crossref_primary_10_1016_j_mencom_2022_05_028 crossref_primary_10_31857_S0044460X23090093 crossref_primary_10_1134_S1070363223090098 crossref_primary_10_1134_S107032842208005X |
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| Keywords | antimony-containing polystyrene tetraphenylantimony methacrylate tetraphenylantimony crotonate |
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| Snippet | Tetraphenylantimony methacrylate Ph
4
SbO
2
CC(CH
3
)=CH
2
and tetraphenylantimony crotonate Ph
4
SbO
2
CCH=CHCH
3
were synthesized by the action of acids on... Tetraphenylantimony methacrylate Ph.sub.4SbO.sub.2CC(CH.sub.3)=CH.sub.2 and tetraphenylantimony crotonate Ph.sub.4SbO.sub.2CCH=CHCH.sub.3 were synthesized by... |
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| SubjectTerms | Acrylates Chemistry Chemistry and Materials Science Chemistry/Food Science Polymerization Polystyrene |
| Title | Synthesis and Structure of Tetraphenylantimony Methacrylate and Tetraphenylantimony Crotonate and Their Use for the Production of Antimony-Containing Polystyrene |
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