Polystyrene‐supported Pd(II) complex‐catalysed carboacylation of 2‐arylpyridines with alcohols via C─H bond activation under solvent‐free conditions

Polystyrene‐supported N,N‐dimethylethylenediamine Pd(II) complex C was used as an efficient catalyst for the synthesis of aromatic ketones via ortho‐acylation of sp2 C─H bonds of 2‐arylpyridines with alcohols as effective coupling partners. The alcohols were oxidized with tert‐butyl hydroperoxide to...

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Published in:	Applied organometallic chemistry Vol. 31; no. 3; pp. np - n/a
Main Authors:	Perumgani, Pullaiah C., Parvathaneni, Sai Prathima, Keesara, Srinivas, Mandapati, Mohan Rao
Format:	Journal Article
Language:	English
Published:	Chichester Wiley Subscription Services, Inc 01-03-2017
Subjects:	Acylation Alcohol Alcohols Aldehydes Aromatic compounds Butyl hydroperoxide carboacylation Catalysts Chemical bonds Chemical synthesis Chemistry Coupling C─H activation Economic conditions Filtration Hydrogen bonds Ketones palladium(II) complex Polystyrene resins Solvents solvent‐free conditions Synthesis (chemistry)
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Abstract	Polystyrene‐supported N,N‐dimethylethylenediamine Pd(II) complex C was used as an efficient catalyst for the synthesis of aromatic ketones via ortho‐acylation of sp2 C─H bonds of 2‐arylpyridines with alcohols as effective coupling partners. The alcohols were oxidized with tert‐butyl hydroperoxide to their corresponding aldehydes in situ and efficiently coupled with 2‐arylpyridines to form aryl ketones under solvent‐free conditions. Furthermore, catalyst C could be easily recovered by simple filtration and reused for five cycles without any significant decrease in its activity. Polystyrene‐supported N,N‐dimethylethylenediamine Pd(II) complex C was used as an efficient catalyst for synthesis of aromatic ketones via ortho‐acylation of 2‐arylpyridines with benzyl alcohol as an effective coupling partner. The alcohols were oxidized to their corresponding aldehydes in situ and efficiently coupled with 2‐arylpyridines to form aryl ketones under solvent‐free conditions. Catalyst C could be easily recovered by simple filtration and reused for five cycles without any significant decrease in its activity.
AbstractList	Polystyrene-supported N,N-dimethylethylenediamine Pd(II) complex C was used as an efficient catalyst for the synthesis of aromatic ketones via ortho-acylation of sp super(2) C-H bonds of 2-arylpyridines with alcohols as effective coupling partners. The alcohols were oxidized with tert-butyl hydroperoxide to their corresponding aldehydes in situ and efficiently coupled with 2-arylpyridines to form aryl ketones under solvent-free conditions. Furthermore, catalyst C could be easily recovered by simple filtration and reused for five cycles without any significant decrease in its activity. Polystyrene-supported N,N-dimethylethylenediamine Pd(II) complex C was used as an efficient catalyst for synthesis of aromatic ketones via ortho-acylation of 2-arylpyridines with benzyl alcohol as an effective coupling partner. The alcohols were oxidized to their corresponding aldehydes in situ and efficiently coupled with 2-arylpyridines to form aryl ketones under solvent-free conditions. Catalyst C could be easily recovered by simple filtration and reused for five cycles without any significant decrease in its activity. Polystyrene‐supported N , N ‐dimethylethylenediamine Pd(II) complex C was used as an efficient catalyst for the synthesis of aromatic ketones via ortho ‐acylation of sp 2 C─H bonds of 2‐arylpyridines with alcohols as effective coupling partners. The alcohols were oxidized with tert ‐butyl hydroperoxide to their corresponding aldehydes in situ and efficiently coupled with 2‐arylpyridines to form aryl ketones under solvent‐free conditions. Furthermore, catalyst C could be easily recovered by simple filtration and reused for five cycles without any significant decrease in its activity. Polystyrene‐supported N,N‐dimethylethylenediamine Pd(II) complex C was used as an efficient catalyst for the synthesis of aromatic ketones via ortho‐acylation of sp2 C─H bonds of 2‐arylpyridines with alcohols as effective coupling partners. The alcohols were oxidized with tert‐butyl hydroperoxide to their corresponding aldehydes in situ and efficiently coupled with 2‐arylpyridines to form aryl ketones under solvent‐free conditions. Furthermore, catalyst C could be easily recovered by simple filtration and reused for five cycles without any significant decrease in its activity. Polystyrene‐supported N,N‐dimethylethylenediamine Pd(II) complex C was used as an efficient catalyst for synthesis of aromatic ketones via ortho‐acylation of 2‐arylpyridines with benzyl alcohol as an effective coupling partner. The alcohols were oxidized to their corresponding aldehydes in situ and efficiently coupled with 2‐arylpyridines to form aryl ketones under solvent‐free conditions. Catalyst C could be easily recovered by simple filtration and reused for five cycles without any significant decrease in its activity. Polystyrene-supported N,N-dimethylethylenediamine Pd(II) complex C was used as an efficient catalyst for the synthesis of aromatic ketones via ortho-acylation of sp2 C--H bonds of 2-arylpyridines with alcohols as effective coupling partners. The alcohols were oxidized with tert-butyl hydroperoxide to their corresponding aldehydes in situ and efficiently coupled with 2-arylpyridines to form aryl ketones under solvent-free conditions. Furthermore, catalyst C could be easily recovered by simple filtration and reused for five cycles without any significant decrease in its activity.
Author	Keesara, Srinivas Perumgani, Pullaiah C. Mandapati, Mohan Rao Parvathaneni, Sai Prathima
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Snippet	Polystyrene‐supported N,N‐dimethylethylenediamine Pd(II) complex C was used as an efficient catalyst for the synthesis of aromatic ketones via ortho‐acylation... Polystyrene‐supported N , N ‐dimethylethylenediamine Pd(II) complex C was used as an efficient catalyst for the synthesis of aromatic ketones via ortho... Polystyrene-supported N,N-dimethylethylenediamine Pd(II) complex C was used as an efficient catalyst for the synthesis of aromatic ketones via ortho-acylation...
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SubjectTerms	Acylation Alcohol Alcohols Aldehydes Aromatic compounds Butyl hydroperoxide carboacylation Catalysts Chemical bonds Chemical synthesis Chemistry Coupling C─H activation Economic conditions Filtration Hydrogen bonds Ketones palladium(II) complex Polystyrene resins Solvents solvent‐free conditions Synthesis (chemistry)
Title	Polystyrene‐supported Pd(II) complex‐catalysed carboacylation of 2‐arylpyridines with alcohols via C─H bond activation under solvent‐free conditions
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