Assessment of homogeneity and stability of new reference material of passion-flower fruits for proficiency testing: Pesticide residues in purple passion fruit (Passiflora pinnatistipula)
Passion-flowers are an important sub-group of fruits with beneficial and healthy properties. The incorporation of these fruits in the global market requires meeting safety requirements of pesticide residues in food. Assuring the absence of or low levels of pesticides in passion-flower fruits require...
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| Published in: | Accreditation and quality assurance Vol. 27; no. 1; pp. 9 - 17 |
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| Main Authors: | , , |
| Format: | Journal Article |
| Language: | English |
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01-02-2022
Springer Nature B.V |
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| Abstract | Passion-flowers are an important sub-group of fruits with beneficial and healthy properties. The incorporation of these fruits in the global market requires meeting safety requirements of pesticide residues in food. Assuring the absence of or low levels of pesticides in passion-flower fruits requires analytical measurements in competent laboratories. One way to demonstrate competence is to participate in proficiency testing using test items closely similar to samples routinely tested by these laboratories, with adequate homogeneity and stability. One feasible proficiency test item might be a reference material. However, currently there are a lack of reference materials of pesticides in Passiflora. This study describes the preparation of a new reference material for eight commonly used pesticides in passion-fruits to concentration levels around the maximum residue limit established by the European Union for this type of commodity. The present study aimed to assess the homogeneity and stability of the material according to ISO Guide 35. The results indicated that the material prepared was sufficiently homogeneous (
u
hom
<
5
%
for the studied pesticides) and stable (for at least 80 days at temperatures
≤
-
20
∘
C
) to be used in a proficiency test of pesticides in passion-flower fruits. |
|---|---|
| AbstractList | Passion-flowers are an important sub-group of fruits with beneficial and healthy properties. The incorporation of these fruits in the global market requires meeting safety requirements of pesticide residues in food. Assuring the absence of or low levels of pesticides in passion-flower fruits requires analytical measurements in competent laboratories. One way to demonstrate competence is to participate in proficiency testing using test items closely similar to samples routinely tested by these laboratories, with adequate homogeneity and stability. One feasible proficiency test item might be a reference material. However, currently there are a lack of reference materials of pesticides in Passiflora. This study describes the preparation of a new reference material for eight commonly used pesticides in passion-fruits to concentration levels around the maximum residue limit established by the European Union for this type of commodity. The present study aimed to assess the homogeneity and stability of the material according to ISO Guide 35. The results indicated that the material prepared was sufficiently homogeneous (uhom<5% for the studied pesticides) and stable (for at least 80 days at temperatures ≤-20∘C) to be used in a proficiency test of pesticides in passion-flower fruits. Passion-flowers are an important sub-group of fruits with beneficial and healthy properties. The incorporation of these fruits in the global market requires meeting safety requirements of pesticide residues in food. Assuring the absence of or low levels of pesticides in passion-flower fruits requires analytical measurements in competent laboratories. One way to demonstrate competence is to participate in proficiency testing using test items closely similar to samples routinely tested by these laboratories, with adequate homogeneity and stability. One feasible proficiency test item might be a reference material. However, currently there are a lack of reference materials of pesticides in Passiflora. This study describes the preparation of a new reference material for eight commonly used pesticides in passion-fruits to concentration levels around the maximum residue limit established by the European Union for this type of commodity. The present study aimed to assess the homogeneity and stability of the material according to ISO Guide 35. The results indicated that the material prepared was sufficiently homogeneous ( u hom < 5 % for the studied pesticides) and stable (for at least 80 days at temperatures ≤ - 20 ∘ C ) to be used in a proficiency test of pesticides in passion-flower fruits. |
| Author | González-Mónico, Sergio A. Guerrero Dallos, Jairo A. Paredes, Maira A. |
| Author_xml | – sequence: 1 givenname: Maira A. surname: Paredes fullname: Paredes, Maira A. organization: Science Faculty, Chemistry Department, Laboratorio de Análisis de Residuos de Plaguicidas, Universidad Nacional de Colombia – sequence: 2 givenname: Sergio A. surname: González-Mónico fullname: González-Mónico, Sergio A. organization: Science Faculty, Chemistry Department, Laboratorio de Análisis de Residuos de Plaguicidas, Universidad Nacional de Colombia – sequence: 3 givenname: Jairo A. surname: Guerrero Dallos fullname: Guerrero Dallos, Jairo A. email: jaguerrerod@unal.edu.co organization: Science Faculty, Chemistry Department, Laboratorio de Análisis de Residuos de Plaguicidas, Universidad Nacional de Colombia |
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| Cites_doi | 10.1007/s00216-020-02761-y 10.1007/s00606-017-1390-2 10.1016/j.envint.2020.106081 10.1007/s00216-015-8476-x 10.1093/jaoac/86.2.412 10.1007/s13765-017-0336-2 10.1351/PAC-REP-09-08-15 10.1351/pac200678010145 10.7585/kjps.2016.20.3.211 10.1385/1-59259-929-X:239 10.1080/13607863.2019.1571011 10.1186/s12263-020-00670-4 10.3945/an.112.003517 10.1016/S0165-9936(01)00091-7 10.5338/KJEA.2016.35.3.24 10.30635/2415-0142.2018.04.4 10.1016/j.foodcont.2017.06.020 10.3390/foods9030369 10.7585/kjps.2018.22.3.159 10.1016/j.chroma.2015.03.076 10.1016/j.foodchem.2011.10.071 10.1016/j.bjp.2016.02.005 |
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| Keywords | Reference material Homogeneity Uncertainty Stability Purple passion fruit Pesticides |
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| SubjectTerms | Analytical Chemistry Biochemistry Chemistry Chemistry and Materials Science Commercial Law Developing countries Ecotoxicology Food Science Fruits General Paper Global marketing Homogeneity Laboratories LDCs Marketing Passion fruit Pesticides Quality control Quality standards Reference materials Residues Software Stability analysis |
| Title | Assessment of homogeneity and stability of new reference material of passion-flower fruits for proficiency testing: Pesticide residues in purple passion fruit (Passiflora pinnatistipula) |
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