Synthesis and thermodynamics of lead(II), manganese(II), and cobalt(II) pivalate complexes
Manganese and cobalt oxopivalates and lead pivalate have been synthesized, mass spectral and thermogravimetric analysis have been performed. Sublimation enthalpies of cobalt and manganese oxopivalates have been determined for the first time, while the sublimation enthalpy of lead pivalate has been f...
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| Published in: | Russian journal of inorganic chemistry Vol. 62; no. 10; pp. 1379 - 1383 |
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| Main Authors: | , , , , , |
| Format: | Journal Article |
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Moscow
Pleiades Publishing
01-10-2017
Springer Nature B.V |
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| Abstract | Manganese and cobalt oxopivalates and lead pivalate have been synthesized, mass spectral and thermogravimetric analysis have been performed. Sublimation enthalpies of cobalt and manganese oxopivalates have been determined for the first time, while the sublimation enthalpy of lead pivalate has been found to agree well with literature data. Low sublimation enthalpy, high volatility, and monomolecular composition of gas phase allow one to use these complexes as precursors for preparing oxide films and materials by MOCVD method. |
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| AbstractList | Manganese and cobalt oxopivalates and lead pivalate have been synthesized, mass spectral and thermogravimetric analysis have been performed. Sublimation enthalpies of cobalt and manganese oxopivalates have been determined for the first time, while the sublimation enthalpy of lead pivalate has been found to agree well with literature data. Low sublimation enthalpy, high volatility, and monomolecular composition of gas phase allow one to use these complexes as precursors for preparing oxide films and materials by MOCVD method. |
| Author | Dement’ev, A.I. Yaryshev, N.G. Kamkin, N.N. Kayumova, D.B. Rodyakina, S.N. Alikhanyan, A.S. |
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| Cites_doi | 10.1021/jp0632438 10.1134/S0036023610090184 10.1016/0040-6031(94)80273-4 10.1002/adfm.200400429 10.1016/j.catcom.2008.08.030 10.1016/j.jssc.2011.09.033 10.1016/j.jmmm.2009.11.019 10.1021/nl035139x |
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| SubjectTerms | Chemistry Chemistry and Materials Science Cobalt Enthalpy Inorganic Chemistry Manganese Oxide coatings Physical Methods of Investigation Sublimation Thermogravimetric analysis Volatility |
| Title | Synthesis and thermodynamics of lead(II), manganese(II), and cobalt(II) pivalate complexes |
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