Silica Nanoparticles with Proton Donor and Proton Acceptor Groups: Synthesis and Aggregation
The effects of precursor structure and polycondensation conditions on the properties of hybrid nanoparticles synthesized from organo-trimethoxysilanes were studied. Hybrid nanoparticles containing groups capable of forming hydrogen bonds were synthesized from functional derivatives of 3-aminopropylt...
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| Published in: | SILICON Vol. 3; no. 1; pp. 5 - 12 |
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| Main Authors: | , , , , , , , , |
| Format: | Journal Article |
| Language: | English |
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2011
Springer Nature B.V |
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| Abstract | The effects of precursor structure and polycondensation conditions on the properties of hybrid nanoparticles synthesized from organo-trimethoxysilanes were studied. Hybrid nanoparticles containing groups capable of forming hydrogen bonds were synthesized from functional derivatives of 3-aminopropyltrimethoxysilane. For the synthesis of phenylurea-functionalized organosilica nanoparticles different approaches to nanoparticle preparation were used. It was shown that the nature of the functional groups (proton-donor or proton-acceptor) affects the aggregation of silica nanoparticles. Also, the difference in behavior of nanoparticles prepared using surface modification and polycondensation was demonstrated for different pH, ionic strength and solvent polarity. As a result, by changing the pH of the solutions, it is possible to shift the aggregation pattern of these nanoparticles, such as the size of the initially formed aggregates. |
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| AbstractList | The effects of precursor structure and polycondensation conditions on the properties of hybrid nanoparticles synthesized from organo-trimethoxysilanes were studied. Hybrid nanoparticles containing groups capable of forming hydrogen bonds were synthesized from functional derivatives of 3-aminopropyltrimethoxysilane. For the synthesis of phenylurea-functionalized organosilica nanoparticles different approaches to nanoparticle preparation were used. It was shown that the nature of the functional groups (proton-donor or proton-acceptor) affects the aggregation of silica nanoparticles. Also, the difference in behavior of nanoparticles prepared using surface modification and polycondensation was demonstrated for different pH, ionic strength and solvent polarity. As a result, by changing the pH of the solutions, it is possible to shift the aggregation pattern of these nanoparticles, such as the size of the initially formed aggregates. |
| Author | Zharov, Ilya Bizyaev, Dmitry A. Antipin, Igor S. Stoikov, Ivan I. Gorbachuk, Vladimir V. Yakimova, Luidmila S. Mostovaya, Olga A. Konovalov, Alexandr I. Bukharaev, Anastas A. |
| Author_xml | – sequence: 1 givenname: Vladimir V. surname: Gorbachuk fullname: Gorbachuk, Vladimir V. organization: A. M. Butlerov Chemical Institute, Kazan (Volga Region) Federal University – sequence: 2 givenname: Luidmila S. surname: Yakimova fullname: Yakimova, Luidmila S. organization: A. M. Butlerov Chemical Institute, Kazan (Volga Region) Federal University – sequence: 3 givenname: Olga A. surname: Mostovaya fullname: Mostovaya, Olga A. organization: A. M. Butlerov Chemical Institute, Kazan (Volga Region) Federal University – sequence: 4 givenname: Dmitry A. surname: Bizyaev fullname: Bizyaev, Dmitry A. organization: Zavoisky Physical−Technical Institute – sequence: 5 givenname: Anastas A. surname: Bukharaev fullname: Bukharaev, Anastas A. organization: Zavoisky Physical−Technical Institute – sequence: 6 givenname: Igor S. surname: Antipin fullname: Antipin, Igor S. organization: A. M. Butlerov Chemical Institute, Kazan (Volga Region) Federal University – sequence: 7 givenname: Alexandr I. surname: Konovalov fullname: Konovalov, Alexandr I. organization: A. M. Butlerov Chemical Institute, Kazan (Volga Region) Federal University – sequence: 8 givenname: Ilya surname: Zharov fullname: Zharov, Ilya email: i.zharov@utah.edu organization: Department of Chemistry, University of Utah – sequence: 9 givenname: Ivan I. surname: Stoikov fullname: Stoikov, Ivan I. email: ivan.stoikov@mail.ru organization: A. M. Butlerov Chemical Institute, Kazan (Volga Region) Federal University |
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| SubjectTerms | Chemistry Chemistry and Materials Science Environmental Chemistry Functional groups Hydrogen bonds Inorganic Chemistry Lasers Materials Science Nanoparticles Optical Devices Optics Original Paper Photonics Polymer Sciences Protons Silicon dioxide Synthesis |
| Title | Silica Nanoparticles with Proton Donor and Proton Acceptor Groups: Synthesis and Aggregation |
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