A Novel Synthesis of triangular Pt Nanosheets on Pd surface with a Strong Electrocatalytic Activity for Oxidation of Methanol

A Novel Synthesis of triangular Pt Nanosheets on Pd surface with a Strong Electrocatalytic Activity for Oxidation of Methanol

The study presents three-dimensional Pd/Pt triangular nanosheets with controlled shape and composition synthesized by a novel approach that uses lemon extract as a biological reducing agent coupled with a microwave treatment at 80 W (~64°C) for 30 min, which proved to be a simple, rapid, and environ...

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Published in:International journal of electrochemical science Vol. 14; no. 8; pp. 6986 - 6998
Main Authors: Quyen, Tran Thi Bich, Qui, Nguyen Phu, An, Vo Le Nhat, Tho, Nguyen Thi, Thanh, Luong Huynh Vu, Tuan, Bui Le Anh, Huynh, Tan-Thanh
Format: Journal Article
Language:English
Published: Elsevier B.V 01-08-2019
Subjects:
catalytic activity
methanol oxidation reaction (MOR)
novel synthesis
Pd/Pt triangular nanosheets (Pd/Pt TANSs)
Pt nanotriangles (Pt NTAs)
methanol oxidation reaction (MOR)
Pd/Pt triangular nanosheets (Pd/Pt TANSs)
novel synthesis
catalytic activity
Pt nanotriangles (Pt NTAs)
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Abstract The study presents three-dimensional Pd/Pt triangular nanosheets with controlled shape and composition synthesized by a novel approach that uses lemon extract as a biological reducing agent coupled with a microwave treatment at 80 W (~64°C) for 30 min, which proved to be a simple, rapid, and environmentally-friendly method. The morphology, structure, and composition of prepared Pd/Pt triangular nanosheets were identified by transmission electronic microscopy (TEM), X-ray diffraction (XRD), and energy-dispersive X-ray (EDX) techniques. Moreover, the electrocatalytic properties of these synthesized Pd/Pt triangular nanosheets (Pd/Pt TANSs), and Pd@Au core/shell nanosheet (Pd@Au NS), and Pd nanosheet (Pd NS) electrocatalysts for methanol oxidation reaction (MOR) were systematically researched using the cyclic voltammetry method. The results showed that Pd/Pt triangular nanosheet (Pd/Pt TANS) electrocatalysts provided a stronger catalytic activity of about ~2.4 and ~1.4 times that of Pd NS and Pt@Au NS catalysts for MOR. In addition, these new triangular nanosheet electrocatalysts achieved a higher MOR performance with decreased use of Pt. This method can create a general approach for the shape-controlled synthesis of bimetallic Pt/M (M = Pd, Cu, Au, Mo, Mn, etc.) triangular nanocatalysts for promising applications in fuel cells in the future.
AbstractList The study presents three-dimensional Pd/Pt triangular nanosheets with controlled shape and composition synthesized by a novel approach that uses lemon extract as a biological reducing agent coupled with a microwave treatment at 80 W (~64°C) for 30 min, which proved to be a simple, rapid, and environmentally-friendly method. The morphology, structure, and composition of prepared Pd/Pt triangular nanosheets were identified by transmission electronic microscopy (TEM), X-ray diffraction (XRD), and energy-dispersive X-ray (EDX) techniques. Moreover, the electrocatalytic properties of these synthesized Pd/Pt triangular nanosheets (Pd/Pt TANSs), and Pd@Au core/shell nanosheet (Pd@Au NS), and Pd nanosheet (Pd NS) electrocatalysts for methanol oxidation reaction (MOR) were systematically researched using the cyclic voltammetry method. The results showed that Pd/Pt triangular nanosheet (Pd/Pt TANS) electrocatalysts provided a stronger catalytic activity of about ~2.4 and ~1.4 times that of Pd NS and Pt@Au NS catalysts for MOR. In addition, these new triangular nanosheet electrocatalysts achieved a higher MOR performance with decreased use of Pt. This method can create a general approach for the shape-controlled synthesis of bimetallic Pt/M (M = Pd, Cu, Au, Mo, Mn, etc.) triangular nanocatalysts for promising applications in fuel cells in the future.
Author Thanh, Luong Huynh Vu
Tuan, Bui Le Anh
Huynh, Tan-Thanh
Tho, Nguyen Thi
Quyen, Tran Thi Bich
An, Vo Le Nhat
Qui, Nguyen Phu
Author_xml – sequence: 1
  givenname: Tran Thi Bich
  surname: Quyen
  fullname: Quyen, Tran Thi Bich
  email: ttbquyen@ctu.edu.vn
  organization: Department of Chemical Engineering, College of Engineering Technology, Can Tho University, 3/2 Street, Ninh Kieu District, Can Tho City, Vietnam
– sequence: 2
  givenname: Nguyen Phu
  surname: Qui
  fullname: Qui, Nguyen Phu
  organization: Department of Chemical Engineering, College of Engineering Technology, Can Tho University, 3/2 Street, Ninh Kieu District, Can Tho City, Vietnam
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  givenname: Vo Le Nhat
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  fullname: An, Vo Le Nhat
  organization: Department of Chemical Engineering, College of Engineering Technology, Can Tho University, 3/2 Street, Ninh Kieu District, Can Tho City, Vietnam
– sequence: 4
  givenname: Nguyen Thi
  surname: Tho
  fullname: Tho, Nguyen Thi
  organization: Institute of Applied Science, Ho Chi Minh City University of Technology, 475B Dien Bien Phu Street, Ward 25, Binh Thanh District, HCM city, Vietnam
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  givenname: Luong Huynh Vu
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  organization: Department of Chemical Engineering, College of Engineering Technology, Can Tho University, 3/2 Street, Ninh Kieu District, Can Tho City, Vietnam
– sequence: 6
  givenname: Bui Le Anh
  surname: Tuan
  fullname: Tuan, Bui Le Anh
  organization: Department of Civil, College of Technology, Can Tho University, 3/2 Street, Ninh Kieu District, Can Tho City, Vietnam
– sequence: 7
  givenname: Tan-Thanh
  surname: Huynh
  fullname: Huynh, Tan-Thanh
  organization: Tra Vinh University, 126 Nguyen Thien Thanh, Ward 4, District 5, Tra Vinh City, Vietnam
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Copyright 2019 The Authors. Published by ESG
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Issue 8
Keywords methanol oxidation reaction (MOR)
Pd/Pt triangular nanosheets (Pd/Pt TANSs)
novel synthesis
catalytic activity
Pt nanotriangles (Pt NTAs)
Language English
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Snippet The study presents three-dimensional Pd/Pt triangular nanosheets with controlled shape and composition synthesized by a novel approach that uses lemon extract...
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SubjectTerms catalytic activity
methanol oxidation reaction (MOR)
novel synthesis
Pd/Pt triangular nanosheets (Pd/Pt TANSs)
Pt nanotriangles (Pt NTAs)
Title A Novel Synthesis of triangular Pt Nanosheets on Pd surface with a Strong Electrocatalytic Activity for Oxidation of Methanol
URI https://dx.doi.org/10.20964/2019.05.70
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