Synthesis of AucorePdshell Nanoparticles by a Green Chemistry Method and Characterization by HAADF-STEM Imaging

In the present work, an environmentally friendly synthesis of inverted Au core Pd shell nanoparticles and its detailed structural characterization are reported. Aberration corrected HAADF-STEM shows that the synthesized nanoparticles have a core–shell structure, where gold is localized in the core a...

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Published in:	Journal of cluster science Vol. 28; no. 4; pp. 2075 - 2086
Main Authors:	Larios-Rodríguez, Eduardo A., Castillón-Barraza, F. F., Herrera-Urbina, Ronaldo, Santiago, Ulises, Posada-Amarillas, Alvaro
Format:	Journal Article
Language:	English
Published:	New York Springer US 01-07-2017 Springer Nature B.V
Subjects:	Acids Aqueous solutions Catalysis Chemical analysis Chemical elements Chemistry Chemistry and Materials Science Core-shell structure Fourier transforms Gold Green chemistry Inorganic Chemistry Nanochemistry Nanoparticles Original Paper Oxidation Palladium Physical Chemistry Seeds Structural analysis Synthesis Transmission electron microscopy Aberration corrected HAADF-STEM EDS Core–shell structure
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Abstract	In the present work, an environmentally friendly synthesis of inverted Au core Pd shell nanoparticles and its detailed structural characterization are reported. Aberration corrected HAADF-STEM shows that the synthesized nanoparticles have a core–shell structure, where gold is localized in the core and palladium in the shell. Core size ranged from 15 to 35 nm, and the shell was about 2 nm, which means that ~11 monolayers of palladium are coating the gold core. EDS chemical analysis validates the presence of gold in the core and the formation of a palladium shell.
AbstractList	In the present work, an environmentally friendly synthesis of inverted Au core Pd shell nanoparticles and its detailed structural characterization are reported. Aberration corrected HAADF-STEM shows that the synthesized nanoparticles have a core–shell structure, where gold is localized in the core and palladium in the shell. Core size ranged from 15 to 35 nm, and the shell was about 2 nm, which means that ~11 monolayers of palladium are coating the gold core. EDS chemical analysis validates the presence of gold in the core and the formation of a palladium shell. In the present work, an environmentally friendly synthesis of inverted AucorePdshell nanoparticles and its detailed structural characterization are reported. Aberration corrected HAADF-STEM shows that the synthesized nanoparticles have a core–shell structure, where gold is localized in the core and palladium in the shell. Core size ranged from 15 to 35 nm, and the shell was about 2 nm, which means that ~11 monolayers of palladium are coating the gold core. EDS chemical analysis validates the presence of gold in the core and the formation of a palladium shell.
Author	Herrera-Urbina, Ronaldo Larios-Rodríguez, Eduardo A. Posada-Amarillas, Alvaro Castillón-Barraza, F. F. Santiago, Ulises
Author_xml	– sequence: 1 givenname: Eduardo A. surname: Larios-Rodríguez fullname: Larios-Rodríguez, Eduardo A. email: elariosg@gmail.com organization: Departamento de Ingeniería Química y Metalurgia, Universidad de Sonora, Department of Physics and Astronomy, University of Texas at San Antonio – sequence: 2 givenname: F. F. surname: Castillón-Barraza fullname: Castillón-Barraza, F. F. organization: Centro de Nanociencias y Nanotecnología, Universidad Nacional Autónoma de México – sequence: 3 givenname: Ronaldo surname: Herrera-Urbina fullname: Herrera-Urbina, Ronaldo organization: Departamento de Ingeniería Química y Metalurgia, Universidad de Sonora – sequence: 4 givenname: Ulises surname: Santiago fullname: Santiago, Ulises organization: Department of Physics and Astronomy, University of Texas at San Antonio – sequence: 5 givenname: Alvaro surname: Posada-Amarillas fullname: Posada-Amarillas, Alvaro email: posada@cifus.uson.mx organization: Departamento de Investigación En Física, Universidad de Sonora
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Cites_doi	10.1021/cr00039a007 10.1021/cr0509861 10.1002/qua.25217 10.1021/ja0704131 10.1039/c1jm12020d 10.1126/science.1128383 10.1016/S0040-4039(01)95429-2 10.1021/nn700021x 10.1021/jo00979a024 10.1016/j.apcatb.2006.06.005 10.1126/science.1159639 10.1103/PhysRevLett.100.206101 10.1021/ar800078m 10.1039/C4CP06012A 10.1002/adma.201003695 10.1021/es048560b 10.1016/j.jcat.2007.10.025 10.1246/bcsj.44.581 10.1007/s11051-012-1106-z 10.1021/jp411500j 10.1021/cr0505674 10.1002/tcr.10053 10.1016/j.jcat.2006.06.001 10.1021/acs.jpcc.6b11923 10.1002/anie.200500659 10.1038/nature04190 10.1021/nl102025s 10.1002/anie.200602454
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Snippet	In the present work, an environmentally friendly synthesis of inverted Au core Pd shell nanoparticles and its detailed structural characterization are... In the present work, an environmentally friendly synthesis of inverted AucorePdshell nanoparticles and its detailed structural characterization are reported....
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SubjectTerms	Acids Aqueous solutions Catalysis Chemical analysis Chemical elements Chemistry Chemistry and Materials Science Core-shell structure Fourier transforms Gold Green chemistry Inorganic Chemistry Nanochemistry Nanoparticles Original Paper Oxidation Palladium Physical Chemistry Seeds Structural analysis Synthesis Transmission electron microscopy
Title	Synthesis of AucorePdshell Nanoparticles by a Green Chemistry Method and Characterization by HAADF-STEM Imaging
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