Experimental Study of the Cr-Hf-Nb System: Liquidus Projection and 1200 °C Isothermal Section
Phase equilibria data from ternary Cr-Nb-X (X = Hf, Ta, Ti, Zr) systems are relevant to the development of Niobium-silicide based composites for use in jet engines. Such systems present at several temperatures a pseudo-binary of Cr 2 Nb-Cr 2 X Laves phases. This work presents the experimentally dete...
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| Published in: | Journal of phase equilibria and diffusion Vol. 41; no. 5; pp. 702 - 721 |
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| Format: | Journal Article |
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01-10-2020
Springer Nature B.V Springer Verlag |
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| Abstract | Phase equilibria data from ternary Cr-Nb-X (X = Hf, Ta, Ti, Zr) systems are relevant to the development of Niobium-silicide based composites for use in jet engines. Such systems present at several temperatures a pseudo-binary of Cr
2
Nb-Cr
2
X Laves phases. This work presents the experimentally determined liquidus projection and the 1200 °C isothermal section for the Cr-Hf-Nb system based on microstructural characterization of as-cast and heat-treated alloys. The microstructural characterization using x-ray diffractometry, scanning electron microscopy and electron probe microanalysis showed four eutectic-type monovariant reactions and two class II invariant reactions in the liquidus projection. The 1200 °C isothermal section showed complete solubility between Nb and Hf in (
C
15) phase and one three phase equilibria field. |
|---|---|
| AbstractList | Phase equilibria data from ternary Cr-Nb-X (X = Hf, Ta, Ti, Zr) systems are relevant to the development of Niobium-silicide based composites for use in jet engines. Such systems present at several temperatures a pseudo-binary of Cr
2
Nb-Cr
2
X Laves phases. This work presents the experimentally determined liquidus projection and the 1200 °C isothermal section for the Cr-Hf-Nb system based on microstructural characterization of as-cast and heat-treated alloys. The microstructural characterization using x-ray diffractometry, scanning electron microscopy and electron probe microanalysis showed four eutectic-type monovariant reactions and two class II invariant reactions in the liquidus projection. The 1200 °C isothermal section showed complete solubility between Nb and Hf in (
C
15) phase and one three phase equilibria field. Phase equilibria data from ternary Cr-Nb-X (X = Hf, Ta, Ti, Zr) systems are relevant to the development of Niobium-silicide based composites for use in jet engines. Such systems present at several temperatures a pseudo-binary of Cr2Nb-Cr2X Laves phases. This work presents the experimentally determined liquidus projection and the 1200 °C isothermal section for the Cr-Hf-Nb system based on microstructural characterization of as-cast and heat-treated alloys. The microstructural characterization using X-ray diffractometry, scanning electron microscopy and electron probe microanalysis showed four eutectic-type monovariant reactions and two class II invariant reactions in the liquidus projection. The Phase equilibria data from ternary Cr-Nb-X (X = Hf, Ta, Ti, Zr) systems are relevant to the development of Niobium-silicide based composites for use in jet engines. Such systems present at several temperatures a pseudo-binary of Cr2Nb-Cr2X Laves phases. This work presents the experimentally determined liquidus projection and the 1200 °C isothermal section for the Cr-Hf-Nb system based on microstructural characterization of as-cast and heat-treated alloys. The microstructural characterization using x-ray diffractometry, scanning electron microscopy and electron probe microanalysis showed four eutectic-type monovariant reactions and two class II invariant reactions in the liquidus projection. The 1200 °C isothermal section showed complete solubility between Nb and Hf in (C15) phase and one three phase equilibria field. |
| Author | Nunes, Carlos Angelo Coelho, Gilberto Carvalho da Silva, Antonio Augusto Araújo Pinto Gigolotti, João Carlos Jânio Joubert, Jean-Marc |
| Author_xml | – sequence: 1 givenname: João Carlos Jânio orcidid: 0000-0003-0481-3191 surname: Gigolotti fullname: Gigolotti, João Carlos Jânio email: carlosjanio@uol.com.br, jcjanio@gmail.com organization: Université Paris-Est Créteil, CNRS, ICMPE (UMR 7182), Departamento de Matemática, Física e Computação (DMFC), Faculdade de Tecnologia (FAT), Universidade Estadual do Rio de Janeiro (UERJ) – sequence: 2 givenname: Antonio Augusto Araújo Pinto surname: da Silva fullname: da Silva, Antonio Augusto Araújo Pinto organization: Instituto de Engenharia Mecânica (IEM), Universidade Federal de Itajubá (UNIFEI) – sequence: 3 givenname: Gilberto Carvalho surname: Coelho fullname: Coelho, Gilberto Carvalho organization: Departamento de Engenharia de Materiais (DEMAR), Escola de Engenharia de Lorena (EEL), Universidade de São Paulo (USP) – sequence: 4 givenname: Carlos Angelo surname: Nunes fullname: Nunes, Carlos Angelo organization: Departamento de Engenharia de Materiais (DEMAR), Escola de Engenharia de Lorena (EEL), Universidade de São Paulo (USP) – sequence: 5 givenname: Jean-Marc surname: Joubert fullname: Joubert, Jean-Marc organization: Université Paris-Est Créteil, CNRS, ICMPE (UMR 7182) |
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| CitedBy_id | crossref_primary_10_1016_j_jallcom_2022_167651 |
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| Keywords | Cr-hf-nb system intermetallics phase diagram microstructure phase stability Intermetallics Cr-Hf-Nb system |
| Language | English |
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| PublicationTitle | Journal of phase equilibria and diffusion |
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| Snippet | Phase equilibria data from ternary Cr-Nb-X (X = Hf, Ta, Ti, Zr) systems are relevant to the development of Niobium-silicide based composites for use in jet... Phase equilibria data from ternary Cr-Nb-X (X = Hf, Ta, Ti, Zr) systems are relevant to the development of Niobium-silicide based composites for use in jet... |
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| SubjectTerms | Ceramics Chemical Sciences Composites Crystallography and Scattering Methods Electron probe microanalysis Engineering Thermodynamics Eutectic reactions Glass Hafnium Heat and Mass Transfer Heat treatment Jet engines Laves phase Liquidus Material chemistry Metallic Materials Natural Materials Niobium Physics Physics and Astronomy Projection Silicides Ternary systems Thermodynamics Zirconium |
| Title | Experimental Study of the Cr-Hf-Nb System: Liquidus Projection and 1200 °C Isothermal Section |
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