Addition of molybdate ions to the anodizing bath to improve the corrosion resistance of clad 2024-T3 alloy anodized in tartaric-sulfuric acid

Addition of molybdate ions to the anodizing bath to improve the corrosion resistance of clad 2024-T3 alloy anodized in tartaric-sulfuric acid

In the present investigation molybdates ions (MoO4−2) were added to a tartaric‑sulfuric acid (TSA) bath, which was employed to anodize AA2024-T3 clad samples. The incorporation of Mo into the anodized layer was investigated by different techniques: X-ray photoelectron spectroscopy (XPS), glow-discha...

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Published in:Surface & coatings technology Vol. 482; p. 130682
Main Authors: Almeida, Thassia Felix de, Prada Ramirez, Oscar Mauricio, Lanzutti, Alex, Rodrigues, Cleber Lima, Brabetz, Manfred, Kremmer, Thomas M., Hammer, Peter, de Melo, Hercilio Gomes
Format: Journal Article
Language:English
Published: Elsevier B.V 30-04-2024
Subjects:
2024-T3 clad
EIS
Modified anodizing bath
Sodium molybdate
Tartaric‑sulfuric acid
Sodium molybdate
Tartaric‑sulfuric acid
Modified anodizing bath
2024-T3 clad
EIS
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Abstract In the present investigation molybdates ions (MoO4−2) were added to a tartaric‑sulfuric acid (TSA) bath, which was employed to anodize AA2024-T3 clad samples. The incorporation of Mo into the anodized layer was investigated by different techniques: X-ray photoelectron spectroscopy (XPS), glow-discharge optical emission spectroscopy (GDOES), Rutherford backscattering spectrometry (RBS) and scanning electron microscopy (SEM), while the corrosion resistance was evaluated by electrochemical impedance spectroscopy (EIS) techniques in neutral (0.5 M) and acidic (0.1 M, pH = 4.0) NaCl solutions. The different characterization techniques indicate that small amounts of the modifier were incorporated into the anodized layer, while the SEM analysis confirmed that the morphology of the layer was not changed, although it was thicker when anodized in the Mo containing bath. Evaluation of corrosion resistance by EIS in both media showed that samples anodized in the molybdate containing bath were more corrosion resistant and durable. Fitting results of the electric equivalent circuit indicate that this may be a consequence of a thicker barrier layer for these samples.
AbstractList In the present investigation molybdates ions (MoO4−2) were added to a tartaric‑sulfuric acid (TSA) bath, which was employed to anodize AA2024-T3 clad samples. The incorporation of Mo into the anodized layer was investigated by different techniques: X-ray photoelectron spectroscopy (XPS), glow-discharge optical emission spectroscopy (GDOES), Rutherford backscattering spectrometry (RBS) and scanning electron microscopy (SEM), while the corrosion resistance was evaluated by electrochemical impedance spectroscopy (EIS) techniques in neutral (0.5 M) and acidic (0.1 M, pH = 4.0) NaCl solutions. The different characterization techniques indicate that small amounts of the modifier were incorporated into the anodized layer, while the SEM analysis confirmed that the morphology of the layer was not changed, although it was thicker when anodized in the Mo containing bath. Evaluation of corrosion resistance by EIS in both media showed that samples anodized in the molybdate containing bath were more corrosion resistant and durable. Fitting results of the electric equivalent circuit indicate that this may be a consequence of a thicker barrier layer for these samples.
ArticleNumber 130682
Author Brabetz, Manfred
Rodrigues, Cleber Lima
Almeida, Thassia Felix de
Prada Ramirez, Oscar Mauricio
de Melo, Hercilio Gomes
Lanzutti, Alex
Hammer, Peter
Kremmer, Thomas M.
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  surname: Almeida
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  organization: Departamento de Eng. Metalúrgica e de Materiais, Escola Politécnica da Universidade de São Paulo, Av. Prof. Mello de Moraes, 2463, Cidade Universitária, 05508-030 São Paulo, SP, Brazil
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  givenname: Oscar Mauricio
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  organization: Departamento de Eng. Metalúrgica e de Materiais, Escola Politécnica da Universidade de São Paulo, Av. Prof. Mello de Moraes, 2463, Cidade Universitária, 05508-030 São Paulo, SP, Brazil
– sequence: 3
  givenname: Alex
  surname: Lanzutti
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  organization: Polytechnic Department of Engineering and Architecture, University of Udine, Via delle Scienze 206, 33100 Udine, Italy
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  givenname: Cleber Lima
  surname: Rodrigues
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  organization: Instituto de Física da Universidade de São Paulo, Rua do Matão, trav. R 187, 05508-090 São Paulo, Brazil
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  givenname: Manfred
  surname: Brabetz
  fullname: Brabetz, Manfred
  organization: Alloy Development Group, Montanuniversitaet Leoben, Forschungszentrum Seibersdorf, 2444 Seibersdorf, Austria
– sequence: 6
  givenname: Thomas M.
  surname: Kremmer
  fullname: Kremmer, Thomas M.
  organization: Chair of Non-Ferrous Metallurgy, Montanuniversitaet Leoben, Franz-Josef-Strasse 18, 8700 Leoben, Austria
– sequence: 7
  givenname: Peter
  surname: Hammer
  fullname: Hammer, Peter
  organization: São Paulo State University (UNESP), Institute of Chemistry, Rua Prof. 55 Francisco Degni 55, Araraquara, SP 14800–060, Brazil
– sequence: 8
  givenname: Hercilio Gomes
  surname: de Melo
  fullname: de Melo, Hercilio Gomes
  organization: Departamento de Eng. Metalúrgica e de Materiais, Escola Politécnica da Universidade de São Paulo, Av. Prof. Mello de Moraes, 2463, Cidade Universitária, 05508-030 São Paulo, SP, Brazil
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Keywords Sodium molybdate
Tartaric‑sulfuric acid
Modified anodizing bath
2024-T3 clad
EIS
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Snippet In the present investigation molybdates ions (MoO4−2) were added to a tartaric‑sulfuric acid (TSA) bath, which was employed to anodize AA2024-T3 clad samples....
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StartPage 130682
SubjectTerms 2024-T3 clad
EIS
Modified anodizing bath
Sodium molybdate
Tartaric‑sulfuric acid
Title Addition of molybdate ions to the anodizing bath to improve the corrosion resistance of clad 2024-T3 alloy anodized in tartaric-sulfuric acid
URI https://dx.doi.org/10.1016/j.surfcoat.2024.130682
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