Reversible photo-controllable surface wettability of epoxy-polyurethane smart coating
Light-responsive materials, in which a rapid and reversible response can be achieved, are of particular interest for several technological applications. The transformation of external stimuli into mechanical energy is very promising in the field of molecular motors and energy convertors. Azobenzene...
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| Published in: | Progress in organic coatings Vol. 179; p. 107509 |
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| Main Authors: | , , |
| Format: | Journal Article |
| Language: | English |
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Elsevier B.V
01-06-2023
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| Abstract | Light-responsive materials, in which a rapid and reversible response can be achieved, are of particular interest for several technological applications. The transformation of external stimuli into mechanical energy is very promising in the field of molecular motors and energy convertors. Azobenzene chromophores undergo photon-driven reversible cis-trans isomerization. In these stimuli-responsive materials, reversible molecular motion can be responsible for switching surface properties, such as surface wettability. In this work, the authors synthesized a fluorinated epoxy - isocyanate thermosetting coating (EPUF) modified with an azobenzene derivative (AZO). The increase in AZO content on the surface by migration during synthesis, as a consequence fluorine presence, leads to changes in the surface hydrophobicity, when UV light is used as a stimulus. First, polyurethane precursors (PUs) based on isophorone diisocyanate (IPDI), a fluorinated diol, and AZO were synthesized. Size-Exclusion Chromatography (SEC), Fourier Transform Infrared Spectroscopy (FTIR), and Ultraviolet-Visible Spectroscopy (UV) techniques were used to characterize the precursors. The polyurethane – epoxy reaction obtained allowed to prepare AZO modified epoxy networks. The resulting materials were characterized using different techniques. Fluorinated and pristine networks were compared. The changes in contact angle, roughness, and mechanical behavior by UV irradiation were analyzed. The reversible photo-induced switching of the surface properties of the fluorine-AZO modified coatings renders them potentially useful for multiple technological applications, in which cycling surface properties are of great use.
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•A novel smart photo-responsive thermosetting coating, with high Tg, was synthesized•Hydrophobicity degree was successfully changed by UV irradiation at 365cm-1•Azo-chromophores were successfully concentrated near the free surface by cooperative migration with fluorinated compounds•Cycling of the hydrophobicity degree is possible, due to the high recovery ability of the fluorine-modified coating•A photoinduced roughness diminution was found to be responsible for an increment in the wetting degree |
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| AbstractList | Light-responsive materials, in which a rapid and reversible response can be achieved, are of particular interest for several technological applications. The transformation of external stimuli into mechanical energy is very promising in the field of molecular motors and energy convertors. Azobenzene chromophores undergo photon-driven reversible cis-trans isomerization. In these stimuli-responsive materials, reversible molecular motion can be responsible for switching surface properties, such as surface wettability. In this work, the authors synthesized a fluorinated epoxy - isocyanate thermosetting coating (EPUF) modified with an azobenzene derivative (AZO). The increase in AZO content on the surface by migration during synthesis, as a consequence fluorine presence, leads to changes in the surface hydrophobicity, when UV light is used as a stimulus. First, polyurethane precursors (PUs) based on isophorone diisocyanate (IPDI), a fluorinated diol, and AZO were synthesized. Size-Exclusion Chromatography (SEC), Fourier Transform Infrared Spectroscopy (FTIR), and Ultraviolet-Visible Spectroscopy (UV) techniques were used to characterize the precursors. The polyurethane – epoxy reaction obtained allowed to prepare AZO modified epoxy networks. The resulting materials were characterized using different techniques. Fluorinated and pristine networks were compared. The changes in contact angle, roughness, and mechanical behavior by UV irradiation were analyzed. The reversible photo-induced switching of the surface properties of the fluorine-AZO modified coatings renders them potentially useful for multiple technological applications, in which cycling surface properties are of great use.
[Display omitted]
•A novel smart photo-responsive thermosetting coating, with high Tg, was synthesized•Hydrophobicity degree was successfully changed by UV irradiation at 365cm-1•Azo-chromophores were successfully concentrated near the free surface by cooperative migration with fluorinated compounds•Cycling of the hydrophobicity degree is possible, due to the high recovery ability of the fluorine-modified coating•A photoinduced roughness diminution was found to be responsible for an increment in the wetting degree |
| ArticleNumber | 107509 |
| Author | Herrera, J.M. Penoff, M.E. Galante, M.J. |
| Author_xml | – sequence: 1 givenname: J.M. surname: Herrera fullname: Herrera, J.M. email: jesica.herrera@fi.mdp.edu.ar organization: División Polímeros Nanoestructurados, INTEMA-CONICET-Facultad de Ingeniería, UNMdP, Av. Colón, 10850 Mar del Plata, Argentina – sequence: 2 givenname: M.E. surname: Penoff fullname: Penoff, M.E. email: elisabeth@fi.mdp.edu.ar organization: División Compuestos Termorrígidos, INTEMA-CONICET-Facultad de Ingeniería, UNMdP, Av. Colón, 10850 Mar del Plata, Argentina – sequence: 3 givenname: M.J. surname: Galante fullname: Galante, M.J. email: galant@fi.mdp.edu.ar organization: División Polímeros Nanoestructurados, INTEMA-CONICET-Facultad de Ingeniería, UNMdP, Av. Colón, 10850 Mar del Plata, Argentina |
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| Cites_doi | 10.1021/ma00086a060 10.1021/la980400o 10.1002/adfm.201101922 10.1021/ja0655901 10.1016/j.ccr.2015.04.005 10.1016/S0022-0728(00)00455-1 10.1140/epje/i2002-10014-4 10.1021/acsami.5b07336 10.1021/acsami.6b15446 10.1002/app.1995.070550109 10.1002/adma.201501578 10.1002/app.42690 10.1016/j.scriptamat.2005.09.025 10.1140/epje/e2003-00015-0 10.1016/j.optmat.2021.111032 10.1080/10587250108023673 10.1002/macp.200500015 10.1021/cm00029a001 10.1016/j.jcis.2020.07.130 10.1002/anie.201814441 10.1002/(SICI)1097-4628(20000509)76:6<962::AID-APP24>3.0.CO;2-Z 10.1021/cr970155y 10.1021/la9610664 10.1021/acs.macromol.6b01848 10.1002/pola.22808 10.1021/acsami.7b06483 10.1016/j.colsurfa.2004.10.022 10.1002/app.1982.070270125 10.1063/1.2966365 10.1016/j.polymer.2011.08.047 10.1080/10587259708036164 |
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| Copyright | 2023 Elsevier B.V. |
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| Keywords | Photo-responsive Cis-trans isomerization Hydrophobicity Azobenzene chromophore |
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| Title | Reversible photo-controllable surface wettability of epoxy-polyurethane smart coating |
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