Two-dimensional gadolinium-doped ceria nanosheets for low temperature sintering of solid oxide fuel cells barrier layer
A novel method for bottom-up synthesis of two-dimensional (2D) gadolinium-doped cerium oxide (CGO) nanosheets is developed and demonstrated as an efficient precursor for interdiffusion barrier layer deposition in solid oxide fuel cells. The CGO is the standard material used as an interlayer in inter...
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| Published in: | Journal of alloys and compounds Vol. 967; p. 171766 |
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| Main Authors: | , , , , , |
| Format: | Journal Article |
| Language: | English |
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Elsevier B.V
10-12-2023
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| Abstract | A novel method for bottom-up synthesis of two-dimensional (2D) gadolinium-doped cerium oxide (CGO) nanosheets is developed and demonstrated as an efficient precursor for interdiffusion barrier layer deposition in solid oxide fuel cells. The CGO is the standard material used as an interlayer in intermediate-temperature solid oxide fuel cells to avoid undesirable reactions between lanthanum strontium cobalt ferrite (LSCF) cathode and yttria-stabilized zirconia (YSZ) electrolyte materials. Herein, the shape-control of the 2D CGO by a low-cost wet-chemical method allowing for the fabrication of fully dense barrier layer of CGO is reported. The high surface coverage promoted by the 2D CGO nanosheets resulted in a thin (∼ 1 µm) and dense interdiffusion barrier layer sintered at 1150 °C preventing the undesirable reaction between oxide ion conducting phases occurring at higher temperatures. The electrochemical properties of solid oxide fuel cells confirmed the CGO nanosheet as an efficient layer for preventing the formation of resistive phases at the electrolyte/cathode interface.
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•Innovative synthesis method for efficient 2D-layered gadolinium doped-ceria (CGO) electrolytes.•2D CGO nanosheets, with high surface coverage, result in dense layer at mild sintering temperature.•CGO nanosheets prevent resistive phases and enhance solid oxide fuel cell performance. |
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| AbstractList | A novel method for bottom-up synthesis of two-dimensional (2D) gadolinium-doped cerium oxide (CGO) nanosheets is developed and demonstrated as an efficient precursor for interdiffusion barrier layer deposition in solid oxide fuel cells. The CGO is the standard material used as an interlayer in intermediate-temperature solid oxide fuel cells to avoid undesirable reactions between lanthanum strontium cobalt ferrite (LSCF) cathode and yttria-stabilized zirconia (YSZ) electrolyte materials. Herein, the shape-control of the 2D CGO by a low-cost wet-chemical method allowing for the fabrication of fully dense barrier layer of CGO is reported. The high surface coverage promoted by the 2D CGO nanosheets resulted in a thin (∼ 1 µm) and dense interdiffusion barrier layer sintered at 1150 °C preventing the undesirable reaction between oxide ion conducting phases occurring at higher temperatures. The electrochemical properties of solid oxide fuel cells confirmed the CGO nanosheet as an efficient layer for preventing the formation of resistive phases at the electrolyte/cathode interface.
[Display omitted]
•Innovative synthesis method for efficient 2D-layered gadolinium doped-ceria (CGO) electrolytes.•2D CGO nanosheets, with high surface coverage, result in dense layer at mild sintering temperature.•CGO nanosheets prevent resistive phases and enhance solid oxide fuel cell performance. |
| ArticleNumber | 171766 |
| Author | Machado, Marina Rodrigues, Lays N. Sun, Ziqi Moraes, Leticia P.R. Marani, Debora Fonseca, Fabio C. |
| Author_xml | – sequence: 1 givenname: Leticia P.R. surname: Moraes fullname: Moraes, Leticia P.R. organization: Nuclear and Energy Research Institute, IPEN-CNEN, São Paulo, Brazil – sequence: 2 givenname: Marina orcidid: 0000-0002-9668-3859 surname: Machado fullname: Machado, Marina organization: Nuclear and Energy Research Institute, IPEN-CNEN, São Paulo, Brazil – sequence: 3 givenname: Lays N. surname: Rodrigues fullname: Rodrigues, Lays N. organization: Nuclear and Energy Research Institute, IPEN-CNEN, São Paulo, Brazil – sequence: 4 givenname: Ziqi surname: Sun fullname: Sun, Ziqi organization: Queensland University of Technology, Brisbane, Australia – sequence: 5 givenname: Debora surname: Marani fullname: Marani, Debora organization: Addifab ApS, Mårkærvej 2, 2630 Taastrup, Denmark – sequence: 6 givenname: Fabio C. surname: Fonseca fullname: Fonseca, Fabio C. email: fabiocf@usp.br organization: Nuclear and Energy Research Institute, IPEN-CNEN, São Paulo, Brazil |
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| Copyright | 2023 Elsevier B.V. |
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| Keywords | Coprecipitation synthesis Barrier layer 2D doped-ceria Gadolinium-doped ceria SOFC |
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