Application of factorial design for mercury determination by trapping and graphite furnace atomic absorption spectrometry

Application of factorial design for mercury determination by trapping and graphite furnace atomic absorption spectrometry

A trapping technique was developed for the determination of mercury traces in blood serum by graphite furnace atomic absorption spectrometry (GFAAS). The mercury was converted to metallic vapour in a reaction cell by tin chloride solution, swept by nitrogen into a gold-plated graphite tube and subse...

Full description

Saved in:
Bibliographic Details
Published in:Spectrochimica acta. Part B: Atomic spectroscopy Vol. 55; no. 7; pp. 971 - 977
Main Authors: Izgi, Belgin, Demir, Cevdet, Güçer, Şeref
Format: Journal Article
Language:English
Published: Elsevier B.V 01-07-2000
Subjects:
Atomic absorption spectrometry
Blood serum
Factorial design
Graphite furnace
Mercury determination
Mercury determination
Graphite furnace
Blood serum
Factorial design
Atomic absorption spectrometry
Online Access:Get full text
Tags: Add Tag
No Tags, Be the first to tag this record!
Description
Summary:A trapping technique was developed for the determination of mercury traces in blood serum by graphite furnace atomic absorption spectrometry (GFAAS). The mercury was converted to metallic vapour in a reaction cell by tin chloride solution, swept by nitrogen into a gold-plated graphite tube and subsequently atomized. The influence of four experimental factors on the sensitivity of mercury determination was examined using two level factorial designs. It was found that the solution volume is the most significant parameter.
ISSN:0584-8547
1873-3565
DOI:10.1016/S0584-8547(00)00234-2