Dinuclear metal complexes of bis-macrocycles
Three bis-macrocycles 7, 10, 11, consisting of two cyclononane units with a N 3, N 2S, and NS 2 donor set bridged by a pyrazole group, have been synthesized and their complexation potential studied. Several solid dinuclear compounds with Cu 2+ and Ni 2+ could be isolated and their structure elucidat...
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| Published in: | Coordination chemistry reviews Vol. 190; pp. 371 - 389 |
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| Format: | Journal Article |
| Language: | English |
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Elsevier B.V
01-09-1999
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| Abstract | Three bis-macrocycles
7,
10,
11, consisting of two cyclononane units with a N
3, N
2S, and NS
2 donor set bridged by a pyrazole group, have been synthesized and their complexation potential studied. Several solid dinuclear compounds with Cu
2+ and Ni
2+ could be isolated and their structure elucidated. In all cases, the two metal ions are bound by the three donor atoms of the macrocycle, by the deprotonated pyrazole group and by one atom of the exogenous ligand, which bridges the two metal centres. In the case of the Cu
2+ complexes, strong anti-ferromagnetic coupling was found. In solution, ligands
7 and
10 give a series of mononuclear [Cu(LH
n
)] (
n=1, 0, −1) and dinuclear [Cu
2(LH
m
)] (
m=0, −1, −2, −3) species which have been identified and characterized by potentiometric and spectrophotometric studies. Cyclic voltammetry and ES-MS have been used to study the ternary species in solution. |
|---|---|
| AbstractList | Three bis-macrocycles
7,
10,
11, consisting of two cyclononane units with a N
3, N
2S, and NS
2 donor set bridged by a pyrazole group, have been synthesized and their complexation potential studied. Several solid dinuclear compounds with Cu
2+ and Ni
2+ could be isolated and their structure elucidated. In all cases, the two metal ions are bound by the three donor atoms of the macrocycle, by the deprotonated pyrazole group and by one atom of the exogenous ligand, which bridges the two metal centres. In the case of the Cu
2+ complexes, strong anti-ferromagnetic coupling was found. In solution, ligands
7 and
10 give a series of mononuclear [Cu(LH
n
)] (
n=1, 0, −1) and dinuclear [Cu
2(LH
m
)] (
m=0, −1, −2, −3) species which have been identified and characterized by potentiometric and spectrophotometric studies. Cyclic voltammetry and ES-MS have been used to study the ternary species in solution. |
| Author | Kaden, Thomas A. |
| Author_xml | – sequence: 1 givenname: Thomas A. surname: Kaden fullname: Kaden, Thomas A. email: kaden@ubaclu.unibas.ch organization: Institute of Inorganic Chemistry, Spitalstrasse 51, CH-4056 Basel, Switzerland |
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| Cites_doi | 10.1016/0039-9140(85)80077-1 10.1021/ja00481a040 10.1016/1044-0305(94)80007-3 10.1016/0010-8545(90)80042-R 10.1021/cr00027a009 10.1038/306284a0 10.1351/pac198052112441 10.1002/hlca.19970800804 10.1021/ic00306a024 10.1002/hlca.19950780316 10.1016/S0277-5387(98)00287-3 10.1021/ja00845a031 10.1021/ic00048a035 10.1021/ja00096a027 10.1021/ic00072a024 10.1098/rspa.1952.0181 10.1080/00945718308059325 10.1039/C29700001682 10.1002/hlca.19940770105 |
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| Snippet | Three bis-macrocycles
7,
10,
11, consisting of two cyclononane units with a N
3, N
2S, and NS
2 donor set bridged by a pyrazole group, have been synthesized... |
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| SubjectTerms | Macrocycle Pyrazole group Solid dinuclear compounds |
| Title | Dinuclear metal complexes of bis-macrocycles |
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