Advanced toluene/n-heptane separation by pervaporation: investigating the potential of graphene oxide (GO)/PVA mixed matrix membrane

Advanced toluene/n-heptane separation by pervaporation: investigating the potential of graphene oxide (GO)/PVA mixed matrix membrane

•The effects of different molecular weights of PVA polymer on the membrane performance were investigated using a PV process.•PVA with a molecular weight of 130,000 showed the optimum toluene separation properties.•GO/PVA mixed matrix membranes with different loadings of GO were prepared, characteriz...

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Published in:Journal of the Taiwan Institute of Chemical Engineers Vol. 150; p. 105025
Main Authors: Pakizeh, Majid, Karami, Mahdi, Kooshki, Sahar, Rahimnia, Rasoul
Format: Journal Article
Language:English
Published: Elsevier B.V 01-09-2023
Subjects:
Aliphatic/Aromatic separation
Graphene oxide (GO)
MMM
Pervaporation
Polyvinyl alcohol (PVA)
Polyvinyl alcohol (PVA)
Aliphatic/Aromatic separation
Graphene oxide (GO)
MMM
Pervaporation
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Abstract •The effects of different molecular weights of PVA polymer on the membrane performance were investigated using a PV process.•PVA with a molecular weight of 130,000 showed the optimum toluene separation properties.•GO/PVA mixed matrix membranes with different loadings of GO were prepared, characterized and used for aromatic mixture separation.•Effective toluene separation from n-heptane was achieved at 1.5 wt.% of GO loading. The separation and purification of aromatic/aliphatic hydrocarbon mixtures from petroleum feedstocks is a significant industrial undertaking that poses several challenges. This task is commonly encountered during the production of ultralow-sulfur gasoline and naphtha reforming processes, both of which are critical for various industries. Recently, membrane pervaporation for separating aromatic/aliphatic mixtures is regarded as a promising option compared to conventional methods due to its energy efficiency. The preparation of a cross-linked polyvinyl alcohol (PVA) membrane with varying molecular weights, is aimed at effectively separating toluene/n-heptane. To further enhance the separation efficiency, mixed matrix membranes (MMMs) were fabricated by incorporating graphene oxide (GO) at different loadings. The PVA membrane with a molecular weight of 130,000 was utilized as the polymer phase, as it exhibited a permeation flux of 24.8 g/m2h and a separation factor of 5.5. Increasing the GO loading from 0.5 to 1.5 wt% increased total flux; however, further increments in GO content led to a decrease in flux. Notably, the PVA-1.5GO sample demonstrated optimum performance, with a total permeation flux of 30.6 g/m2h, separation factor of 11.9. For this sample, pervaporation separation index (PSI) of 333.54 was obtained, indicating a 199% increase compared to that of pure PVA membrane (111.4). [Display omitted]
AbstractList •The effects of different molecular weights of PVA polymer on the membrane performance were investigated using a PV process.•PVA with a molecular weight of 130,000 showed the optimum toluene separation properties.•GO/PVA mixed matrix membranes with different loadings of GO were prepared, characterized and used for aromatic mixture separation.•Effective toluene separation from n-heptane was achieved at 1.5 wt.% of GO loading. The separation and purification of aromatic/aliphatic hydrocarbon mixtures from petroleum feedstocks is a significant industrial undertaking that poses several challenges. This task is commonly encountered during the production of ultralow-sulfur gasoline and naphtha reforming processes, both of which are critical for various industries. Recently, membrane pervaporation for separating aromatic/aliphatic mixtures is regarded as a promising option compared to conventional methods due to its energy efficiency. The preparation of a cross-linked polyvinyl alcohol (PVA) membrane with varying molecular weights, is aimed at effectively separating toluene/n-heptane. To further enhance the separation efficiency, mixed matrix membranes (MMMs) were fabricated by incorporating graphene oxide (GO) at different loadings. The PVA membrane with a molecular weight of 130,000 was utilized as the polymer phase, as it exhibited a permeation flux of 24.8 g/m2h and a separation factor of 5.5. Increasing the GO loading from 0.5 to 1.5 wt% increased total flux; however, further increments in GO content led to a decrease in flux. Notably, the PVA-1.5GO sample demonstrated optimum performance, with a total permeation flux of 30.6 g/m2h, separation factor of 11.9. For this sample, pervaporation separation index (PSI) of 333.54 was obtained, indicating a 199% increase compared to that of pure PVA membrane (111.4). [Display omitted]
ArticleNumber 105025
Author Karami, Mahdi
Rahimnia, Rasoul
Pakizeh, Majid
Kooshki, Sahar
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  givenname: Rasoul
  surname: Rahimnia
  fullname: Rahimnia, Rasoul
  organization: Department of Chemical Engineering, Faculty of Engineering, Ferdowsi University of Mashhad, P.O. Box 9177948974, Mashhad, Iran
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Keywords Polyvinyl alcohol (PVA)
Aliphatic/Aromatic separation
Graphene oxide (GO)
MMM
Pervaporation
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Snippet •The effects of different molecular weights of PVA polymer on the membrane performance were investigated using a PV process.•PVA with a molecular weight of...
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elsevier
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Publisher
StartPage 105025
SubjectTerms Aliphatic/Aromatic separation
Graphene oxide (GO)
MMM
Pervaporation
Polyvinyl alcohol (PVA)
Title Advanced toluene/n-heptane separation by pervaporation: investigating the potential of graphene oxide (GO)/PVA mixed matrix membrane
URI https://dx.doi.org/10.1016/j.jtice.2023.105025
Volume 150
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