A phosphorous/nitrogen/silicon containing diphenylphosphoramide silicon oil toward effective flame retardancy for polycarbonate with comparable mechanical properties
A P/N/Si containing diphenylphosphoramide silicone oil (PASO) was synthesized using amino phenyl silicone oil and diphenylphosphinyl chloride as raw materials. The as‐synthesized PASO displayed better flame retardancy toward polycarbonate (PC) meanwhile maintaining the mechanical performances of PC....
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| Published in: | Journal of applied polymer science Vol. 139; no. 10 |
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| Format: | Journal Article |
| Language: | English |
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| Abstract | A P/N/Si containing diphenylphosphoramide silicone oil (PASO) was synthesized using amino phenyl silicone oil and diphenylphosphinyl chloride as raw materials. The as‐synthesized PASO displayed better flame retardancy toward polycarbonate (PC) meanwhile maintaining the mechanical performances of PC. At loading level of 1 wt% PASO, UL 94V‐0 rating and a high limited oxygen index value of 31% were achieved for the flame retardant composite in the presence of 5 wt% talc as anti‐dripping agent. Additionally, it gave a tensile strength of 65.5 MPa, elongation at break of 96.4%, and impact strength of 52.6 kJ/m2, which were comparable to the pure PC. The analysis of the char residue after cone calorimeter test and the pyrolysis gaseous products demonstrated that PASO exhibited flame retardant mechanism of both gas and condensed phases. |
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| AbstractList | A P/N/Si containing diphenylphosphoramide silicone oil (PASO) was synthesized using amino phenyl silicone oil and diphenylphosphinyl chloride as raw materials. The as‐synthesized PASO displayed better flame retardancy toward polycarbonate (PC) meanwhile maintaining the mechanical performances of PC. At loading level of 1 wt% PASO, UL 94V‐0 rating and a high limited oxygen index value of 31% were achieved for the flame retardant composite in the presence of 5 wt% talc as anti‐dripping agent. Additionally, it gave a tensile strength of 65.5 MPa, elongation at break of 96.4%, and impact strength of 52.6 kJ/m
2
, which were comparable to the pure PC. The analysis of the char residue after cone calorimeter test and the pyrolysis gaseous products demonstrated that PASO exhibited flame retardant mechanism of both gas and condensed phases. A P/N/Si containing diphenylphosphoramide silicone oil (PASO) was synthesized using amino phenyl silicone oil and diphenylphosphinyl chloride as raw materials. The as‐synthesized PASO displayed better flame retardancy toward polycarbonate (PC) meanwhile maintaining the mechanical performances of PC. At loading level of 1 wt% PASO, UL 94V‐0 rating and a high limited oxygen index value of 31% were achieved for the flame retardant composite in the presence of 5 wt% talc as anti‐dripping agent. Additionally, it gave a tensile strength of 65.5 MPa, elongation at break of 96.4%, and impact strength of 52.6 kJ/m2, which were comparable to the pure PC. The analysis of the char residue after cone calorimeter test and the pyrolysis gaseous products demonstrated that PASO exhibited flame retardant mechanism of both gas and condensed phases. |
| Author | Luo, Zhonglin Jiang, Qing Wang, Biaobing |
| Author_xml | – sequence: 1 givenname: Qing surname: Jiang fullname: Jiang, Qing organization: Changzhou University – sequence: 2 givenname: Zhonglin surname: Luo fullname: Luo, Zhonglin organization: Changzhou University – sequence: 3 givenname: Biaobing orcidid: 0000-0003-4897-3920 surname: Wang fullname: Wang, Biaobing email: biaobing@cczu.edu.cn organization: Changzhou University |
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| CitedBy_id | crossref_primary_10_1002_app_53152 crossref_primary_10_1007_s11356_023_29012_8 crossref_primary_10_1016_j_polymer_2024_126948 crossref_primary_10_1016_j_compositesa_2023_107812 crossref_primary_10_1007_s10337_023_04248_1 crossref_primary_10_1016_j_conbuildmat_2024_136707 crossref_primary_10_1002_app_54513 |
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Polym. Sci. contributor: fullname: Yuan D. D. |
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| Snippet | A P/N/Si containing diphenylphosphoramide silicone oil (PASO) was synthesized using amino phenyl silicone oil and diphenylphosphinyl chloride as raw materials.... |
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| SubjectTerms | Cone calorimeters Elongation flame retardance Flame retardants Impact strength Materials science Mechanical properties Nitrogen Polycarbonate resins Polymers Pyrolysis Raw materials Reagents Silicon Silicone resins Synthesis Tensile strength thermal properties |
| Title | A phosphorous/nitrogen/silicon containing diphenylphosphoramide silicon oil toward effective flame retardancy for polycarbonate with comparable mechanical properties |
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