Hyperbranched polyester poly(3-diethylamino)propionates and their copper(ii) complexes
Novel polydentate ligands were obtained from second and third generation hyperbranched polyesters containing terminal (3-diethylamino)propionate groups. Polynuclear Cu II complexes with these ligands were synthesized. The degree of diethylamination of the polyesters increases when moving from the se...
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| Published in: | Russian chemical bulletin Vol. 64; no. 11; pp. 2667 - 2677 |
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| Main Authors: | , , , , , |
| Format: | Journal Article |
| Language: | English |
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01-11-2015
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| Abstract | Novel polydentate ligands were obtained from second and third generation hyperbranched polyesters containing terminal (3-diethylamino)propionate groups. Polynuclear Cu
II
complexes with these ligands were synthesized. The degree of diethylamination of the polyesters increases when moving from the second to the third generation (from 56 to 81%). In polynuclear complexes, the ratios of Cu to hyperbranched ligand are 6 : 1 and 13 : 1 for second and third generation polyester polyamines, respectively. It was demonstrated using IR and ESR spectroscopy that each coordination polyhedron in the complexes is an isolated paramagnetic center of the formula CuN
2
O
2
Solv
2
(Solv = H
2
O, DMSO). |
|---|---|
| AbstractList | Novel polydentate ligands were obtained from second and third generation hyperbranched polyesters containing terminal (3-diethylamino)propionate groups. Polynuclear Cu
II
complexes with these ligands were synthesized. The degree of diethylamination of the polyesters increases when moving from the second to the third generation (from 56 to 81%). In polynuclear complexes, the ratios of Cu to hyperbranched ligand are 6 : 1 and 13 : 1 for second and third generation polyester polyamines, respectively. It was demonstrated using IR and ESR spectroscopy that each coordination polyhedron in the complexes is an isolated paramagnetic center of the formula CuN
2
O
2
Solv
2
(Solv = H
2
O, DMSO). |
| Author | Ulakhovich, N. A. Kutyrev, G. A. Yurtaeva, S. V. Kutyreva, M. P. Gataulina, A. R. Surnova, A. V. |
| Author_xml | – sequence: 1 givenname: M. P. surname: Kutyreva fullname: Kutyreva, M. P. email: mkutyreva@mail.ru organization: Kazan (Volga Region) Federal University – sequence: 2 givenname: A. R. surname: Gataulina fullname: Gataulina, A. R. organization: Kazan (Volga Region) Federal University – sequence: 3 givenname: G. A. surname: Kutyrev fullname: Kutyrev, G. A. organization: Kazan National Research Technological University – sequence: 4 givenname: N. A. surname: Ulakhovich fullname: Ulakhovich, N. A. organization: Kazan (Volga Region) Federal University – sequence: 5 givenname: A. V. surname: Surnova fullname: Surnova, A. V. organization: Kazan (Volga Region) Federal University – sequence: 6 givenname: S. V. surname: Yurtaeva fullname: Yurtaeva, S. V. organization: E. K. Zavoisky Kazan Institute of Physical Engineering, Kazan Research Center of the Russian Academy of Sciences |
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| Cites_doi | 10.1016/j.biomaterials.2009.06.057 10.1134/S1070363211050227 10.1016/j.progpolymsci.2008.09.001 10.1063/1.1727057 10.1134/S1070363211070206 10.1016/j.progpolymsci.2010.08.004 10.1016/j.chemphyslip.2004.09.001 10.1016/j.progpolymsci.2003.12.002 10.1021/bc060200l 10.1002/cber.19971300608 10.1021/ma021070o 10.1007/s11172-014-0419-8 10.1134/S1560090413040052 10.1134/S1070363213120074 10.1016/j.jconrel.2005.06.022 10.1016/j.biomaterials.2006.09.028 10.1021/bm025738i 10.1021/bc025633c 10.1016/j.ica.2005.05.001 10.1021/jp962857h |
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| Keywords | copper(II) complexes ionization hyperbranched polyester poly(3-diethylamino)propionates complexation |
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| Title | Hyperbranched polyester poly(3-diethylamino)propionates and their copper(ii) complexes |
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