Influence of process variables on chemically activated carbon from pistachio shell with ZnCl2 and KOH
Activated carbons are prepared by chemical activation from pistachio shell with ZnCl 2 and KOH. Activation consisted of impregnation of a precursor followed by carbonization in N 2 and CO 2 at various temperatures, dwell times, heating rates and chemical ratios. Activation with KOH resulted in a low...
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| Published in: | Research on chemical intermediates Vol. 41; no. 1; pp. 71 - 81 |
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| Main Authors: | , , , |
| Format: | Journal Article |
| Language: | English |
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2015
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| Abstract | Activated carbons are prepared by chemical activation from pistachio shell with ZnCl
2
and KOH. Activation consisted of impregnation of a precursor followed by carbonization in N
2
and CO
2
at various temperatures, dwell times, heating rates and chemical ratios. Activation with KOH resulted in a lower yield than the ZnCl
2
. The results suggest KOH as a base is not suitable for preparing high-porosity carbons from pistachio shell. Study of various parameters during activation of pistachio shell with ZnCl
2
revealed that the most important variables are concentration and ratio of the chemical agent. The maximum surface areas obtained from the activation with ZnCl
2
was 2,024 m
2
/g. It was found that the yield of all experiments was above 35 % regardless of preparation conditions, and in optimum conditions, it reached 47.4 %. The yield was decreased by increasing temperature and dwell time, but increasing heating rate, ZnCl
2
concentration, and chemical ratio, increased the yield. |
|---|---|
| AbstractList | Activated carbons are prepared by chemical activation from pistachio shell with ZnCl
2
and KOH. Activation consisted of impregnation of a precursor followed by carbonization in N
2
and CO
2
at various temperatures, dwell times, heating rates and chemical ratios. Activation with KOH resulted in a lower yield than the ZnCl
2
. The results suggest KOH as a base is not suitable for preparing high-porosity carbons from pistachio shell. Study of various parameters during activation of pistachio shell with ZnCl
2
revealed that the most important variables are concentration and ratio of the chemical agent. The maximum surface areas obtained from the activation with ZnCl
2
was 2,024 m
2
/g. It was found that the yield of all experiments was above 35 % regardless of preparation conditions, and in optimum conditions, it reached 47.4 %. The yield was decreased by increasing temperature and dwell time, but increasing heating rate, ZnCl
2
concentration, and chemical ratio, increased the yield. |
| Author | Eksiri, Zahra Najjarzadeh, Hadi Hashemipour Rafsanjani, Hassan Kamandari, Hossein |
| Author_xml | – sequence: 1 givenname: Hossein surname: Kamandari fullname: Kamandari, Hossein email: hkamandari@yahoo.com organization: Department of Chemical Engineering, College of Engineering, Shahid Bahonar University of Kerman – sequence: 2 givenname: Hassan surname: Hashemipour Rafsanjani fullname: Hashemipour Rafsanjani, Hassan organization: Department of Chemical Engineering, College of Engineering, Shahid Bahonar University of Kerman – sequence: 3 givenname: Hadi surname: Najjarzadeh fullname: Najjarzadeh, Hadi organization: Department of Chemical Engineering, College of Engineering, Shahid Bahonar University of Kerman – sequence: 4 givenname: Zahra surname: Eksiri fullname: Eksiri, Zahra organization: Department of Chemical Engineering, Amirkabir University of Technology |
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| Keywords | Iodine number Chemical activation Pistachio shell Activated carbon |
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| Snippet | Activated carbons are prepared by chemical activation from pistachio shell with ZnCl
2
and KOH. Activation consisted of impregnation of a precursor followed by... |
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| Title | Influence of process variables on chemically activated carbon from pistachio shell with ZnCl2 and KOH |
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