An electrochemical and magnetic approach for /H2SO4/HNO3/chitosan functionalized multi-wall carbon nanotubes stable solutions

The aim of the research was to evaluate the effects of sulfonitric and CS (CS) treatment in multilayer carbon nanotubes (MWCNT) on their electrochemical and magnetic properties. Thermogravimetric analysis (TG) showed an increase in thermal properties for CS functionalized MWCNT when compared in sulf...

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Published in:	Journal of materials science. Materials in electronics Vol. 33; no. 27; pp. 21409 - 21424
Main Authors:	Holanda, E. B. N., Cabral, R. L. B., Ladchumananandasivam, R., Neto, N. F. A., Santos, J. E. L., Santos, E. V., Galvão, F. M. F., Bohn, F., Nascimento, J. H. O.
Format:	Journal Article
Language:	English
Published:	New York Springer US 01-09-2022 Springer Nature B.V
Subjects:	Aqueous solutions Carbon Characterization and Evaluation of Materials Chemistry and Materials Science Chitosan Diffraction patterns Electrolytic analysis Electrons Functional groups High resolution electron microscopy Interlayers Magnetic properties Materials Science Multi wall carbon nanotubes Multilayers Optical and Electronic Materials Photoelectrons Raman spectroscopy Spectrum analysis Sulfuric acid Thermodynamic properties Thermogravimetric analysis X ray photoelectron spectroscopy
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Abstract	The aim of the research was to evaluate the effects of sulfonitric and CS (CS) treatment in multilayer carbon nanotubes (MWCNT) on their electrochemical and magnetic properties. Thermogravimetric analysis (TG) showed an increase in thermal properties for CS functionalized MWCNT when compared in sulfonitric medium. High resolution transmission electron microscopy (HRTEM) images revealed a reduction in the average diameter of functionalized MWCNT in the presence of CS in addition to decreasing their interlayer spaces. As evidenced by X-ray Diffraction (XRD) patterns. In addition, X-ray photoelectron spectroscopy (XPS) spectra proved the functional groups inclusion of CS and sulfonitric solution on the (carbon nanotubes) CNT matrix. Unlike pristine MWCNT solutions which are unstable in aqueous media, functionalization with acidic solutions and contributed to its potential stabilization. The results obtained by Raman Spectroscopy prove the functionalization through the insertion of functional groups in the walls of the nanotubes. The electroanalysis showed higher capacitance values by mass and by area for samples functionalized with acids and that the addition of CS during functionalization increases the resistance to current flow, causing an insulating effect.
AbstractList	The aim of the research was to evaluate the effects of sulfonitric and CS (CS) treatment in multilayer carbon nanotubes (MWCNT) on their electrochemical and magnetic properties. Thermogravimetric analysis (TG) showed an increase in thermal properties for CS functionalized MWCNT when compared in sulfonitric medium. High resolution transmission electron microscopy (HRTEM) images revealed a reduction in the average diameter of functionalized MWCNT in the presence of CS in addition to decreasing their interlayer spaces. As evidenced by X-ray Diffraction (XRD) patterns. In addition, X-ray photoelectron spectroscopy (XPS) spectra proved the functional groups inclusion of CS and sulfonitric solution on the (carbon nanotubes) CNT matrix. Unlike pristine MWCNT solutions which are unstable in aqueous media, functionalization with acidic solutions and contributed to its potential stabilization. The results obtained by Raman Spectroscopy prove the functionalization through the insertion of functional groups in the walls of the nanotubes. The electroanalysis showed higher capacitance values by mass and by area for samples functionalized with acids and that the addition of CS during functionalization increases the resistance to current flow, causing an insulating effect.
Author	Cabral, R. L. B. Neto, N. F. A. Bohn, F. Santos, J. E. L. Holanda, E. B. N. Santos, E. V. Galvão, F. M. F. Nascimento, J. H. O. Ladchumananandasivam, R.
Author_xml	– sequence: 1 givenname: E. B. N. surname: Holanda fullname: Holanda, E. B. N. email: elisanbh@gmail.com organization: Postgraduate Program in Mechanical Engineering, Center of Technology, Federal University of Rio Grande do Norte – sequence: 2 givenname: R. L. B. orcidid: 0000-0002-9775-5818 surname: Cabral fullname: Cabral, R. L. B. email: systemriva38@gmail.com organization: Postgraduate Program in Textile Engineering, Center of Technology, Federal University of Rio Grande do Norte – sequence: 3 givenname: R. surname: Ladchumananandasivam fullname: Ladchumananandasivam, R. organization: Postgraduate Program in Mechanical Engineering, Center of Technology, Federal University of Rio Grande do Norte – sequence: 4 givenname: N. F. A. surname: Neto fullname: Neto, N. F. A. organization: LSQM – Laboratory of Chemical Synthesis of Materials – Department of Materials Engineering, Federal University of Rio Grande do Norte – UFRN – sequence: 5 givenname: J. E. L. surname: Santos fullname: Santos, J. E. L. organization: Environmental and Applied Electrochemical Laboratory, School of Science and Technology, Federal University of Rio Grande do Norte – sequence: 6 givenname: E. V. surname: Santos fullname: Santos, E. V. organization: Environmental and Applied Electrochemical Laboratory, School of Science and Technology, Federal University of Rio Grande do Norte – sequence: 7 givenname: F. M. F. surname: Galvão fullname: Galvão, F. M. F. organization: Postgraduate Program in Textile Engineering, Center of Technology, Federal University of Rio Grande do Norte – sequence: 8 givenname: F. surname: Bohn fullname: Bohn, F. organization: Department of Phisics, Federal University of Rio Grande do Norte – sequence: 9 givenname: J. H. O. surname: Nascimento fullname: Nascimento, J. H. O. email: joseheriberto@ct.ufrn.br organization: Postgraduate Program in Mechanical Engineering, Center of Technology, Federal University of Rio Grande do Norte, Postgraduate Program in Textile Engineering, Center of Technology, Federal University of Rio Grande do Norte
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Snippet	The aim of the research was to evaluate the effects of sulfonitric and CS (CS) treatment in multilayer carbon nanotubes (MWCNT) on their electrochemical and...
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SubjectTerms	Aqueous solutions Carbon Characterization and Evaluation of Materials Chemistry and Materials Science Chitosan Diffraction patterns Electrolytic analysis Electrons Functional groups High resolution electron microscopy Interlayers Magnetic properties Materials Science Multi wall carbon nanotubes Multilayers Optical and Electronic Materials Photoelectrons Raman spectroscopy Spectrum analysis Sulfuric acid Thermodynamic properties Thermogravimetric analysis X ray photoelectron spectroscopy
Title	An electrochemical and magnetic approach for /H2SO4/HNO3/chitosan functionalized multi-wall carbon nanotubes stable solutions
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