Pulsed potential co-electrodeposition of Cu2CoSnS4 absorber layer on fluorinated tin oxide (FTO)-coated glass

Thin films of Cu 2 CoSnS 4 (CCTS) are electrodeposited onto fluorine tin oxide substrate using pulsed electrodeposition mode for various time periods followed by sulfurization treatment at 500 °C. The pulse potential (V1) is held constant at 0 V vs. Ag/AgCl, while (V2) is set at − 1.1 V vs. Ag/AgCl....

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Published in:	Journal of applied electrochemistry Vol. 54; no. 12; pp. 2745 - 2756
Main Authors:	Ait Layachi, Omar, Boudouma, Abderrazzak, Lasri, Mohammed, Hrir, Hala, Nini, Meryem, Azmi, Sara, Bousseta, Mohammed, Moujib, Asmaa, Khoumri, El mati
Format:	Journal Article
Language:	English
Published:	Dordrecht Springer Netherlands 2024 Springer Nature B.V
Subjects:	Chemistry Chemistry and Materials Science Diffraction patterns Electrical properties Electrochemical impedance spectroscopy Electrochemistry Electrodeposition Energy gap Fluorine Industrial Chemistry/Chemical Engineering Pattern analysis Physical Chemistry Pulse duration Raman spectra Raman spectroscopy Research Article Silver Spectrum analysis Substrates Sulfurization Thin films Tin Tin oxides X-ray diffraction Solar cells Cu Stannite Pulsed electrodeposition Time effect CoSnS Thin film
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Abstract	Thin films of Cu 2 CoSnS 4 (CCTS) are electrodeposited onto fluorine tin oxide substrate using pulsed electrodeposition mode for various time periods followed by sulfurization treatment at 500 °C. The pulse potential (V1) is held constant at 0 V vs. Ag/AgCl, while (V2) is set at − 1.1 V vs. Ag/AgCl. The effect of pulse duration on the CCTS proprietress is being investigated. Cyclic voltammetry was used to study the electrochemical behaviors of Cu–Co–Sn–S precursors, while in situ electrochemical impedance spectroscopy investigated the electrical properties of the system during electrodeposition of CCTS at − 1.10 V. The impedance spectra revealed a capacitive loop pattern along with Warburg diffusion. The samples were analyzed by X-ray diffraction (XRD), Raman spectroscopy, and UV–visible spectroscopy. Both XRD data and Raman spectra indicated that the CCTS thin films have a stannite structure. The films deposited for 20 min and 30 min exhibit a predominantly pure CCTS phase. Moreover, deposition for 20 min exhibits a homogeneous morphology with a nearly stoichiometric composition along with an optical band gap energy of 1.54 eV. Apart from the CCTS phase, noticeable secondary phases are present in films deposited at both low and high pulse durations, and they have been observed to slightly affect the gap energy. Graphical abstract
AbstractList	Thin films of Cu 2 CoSnS 4 (CCTS) are electrodeposited onto fluorine tin oxide substrate using pulsed electrodeposition mode for various time periods followed by sulfurization treatment at 500 °C. The pulse potential (V1) is held constant at 0 V vs. Ag/AgCl, while (V2) is set at − 1.1 V vs. Ag/AgCl. The effect of pulse duration on the CCTS proprietress is being investigated. Cyclic voltammetry was used to study the electrochemical behaviors of Cu–Co–Sn–S precursors, while in situ electrochemical impedance spectroscopy investigated the electrical properties of the system during electrodeposition of CCTS at − 1.10 V. The impedance spectra revealed a capacitive loop pattern along with Warburg diffusion. The samples were analyzed by X-ray diffraction (XRD), Raman spectroscopy, and UV–visible spectroscopy. Both XRD data and Raman spectra indicated that the CCTS thin films have a stannite structure. The films deposited for 20 min and 30 min exhibit a predominantly pure CCTS phase. Moreover, deposition for 20 min exhibits a homogeneous morphology with a nearly stoichiometric composition along with an optical band gap energy of 1.54 eV. Apart from the CCTS phase, noticeable secondary phases are present in films deposited at both low and high pulse durations, and they have been observed to slightly affect the gap energy. Graphical abstract Thin films of Cu2CoSnS4 (CCTS) are electrodeposited onto fluorine tin oxide substrate using pulsed electrodeposition mode for various time periods followed by sulfurization treatment at 500 °C. The pulse potential (V1) is held constant at 0 V vs. Ag/AgCl, while (V2) is set at − 1.1 V vs. Ag/AgCl. The effect of pulse duration on the CCTS proprietress is being investigated. Cyclic voltammetry was used to study the electrochemical behaviors of Cu–Co–Sn–S precursors, while in situ electrochemical impedance spectroscopy investigated the electrical properties of the system during electrodeposition of CCTS at − 1.10 V. The impedance spectra revealed a capacitive loop pattern along with Warburg diffusion. The samples were analyzed by X-ray diffraction (XRD), Raman spectroscopy, and UV–visible spectroscopy. Both XRD data and Raman spectra indicated that the CCTS thin films have a stannite structure. The films deposited for 20 min and 30 min exhibit a predominantly pure CCTS phase. Moreover, deposition for 20 min exhibits a homogeneous morphology with a nearly stoichiometric composition along with an optical band gap energy of 1.54 eV. Apart from the CCTS phase, noticeable secondary phases are present in films deposited at both low and high pulse durations, and they have been observed to slightly affect the gap energy.
Author	Khoumri, El mati Nini, Meryem Azmi, Sara Boudouma, Abderrazzak Hrir, Hala Lasri, Mohammed Moujib, Asmaa Bousseta, Mohammed Ait Layachi, Omar
Author_xml	– sequence: 1 givenname: Omar surname: Ait Layachi fullname: Ait Layachi, Omar email: aitlayachiomar@gmail.com, omar.aitlayachi-etu@etu.univh2c.ma organization: Laboratory of Physical Chemistry and Biotechnology of Biomolecules and Materials, Faculty of Sciences and Technology, Hassan II University of Casablanca – sequence: 2 givenname: Abderrazzak surname: Boudouma fullname: Boudouma, Abderrazzak organization: Laboratory of Physical Chemistry and Biotechnology of Biomolecules and Materials, Faculty of Sciences and Technology, Hassan II University of Casablanca – sequence: 3 givenname: Mohammed surname: Lasri fullname: Lasri, Mohammed organization: Laboratory of Applied Chemistry and Biomass, Department of Chemistry, Faculty of Sciences, University Cadi Ayyad – sequence: 4 givenname: Hala surname: Hrir fullname: Hrir, Hala organization: Laboratory of Physical Chemistry and Biotechnology of Biomolecules and Materials, Faculty of Sciences and Technology, Hassan II University of Casablanca – sequence: 5 givenname: Meryem surname: Nini fullname: Nini, Meryem organization: Laboratory of Physical Chemistry and Biotechnology of Biomolecules and Materials, Faculty of Sciences and Technology, Hassan II University of Casablanca – sequence: 6 givenname: Sara surname: Azmi fullname: Azmi, Sara organization: Laboratory of Mechanics and Civil Engineering (LMGC), CNRS, University of Montpellier – sequence: 7 givenname: Mohammed surname: Bousseta fullname: Bousseta, Mohammed organization: Laboratory of Materials, Energy, and the Environment (LaMEE), Faculty of Science Semlalia, Cadi Ayyad University – sequence: 8 givenname: Asmaa surname: Moujib fullname: Moujib, Asmaa organization: Laboratory of Physical Chemistry and Biotechnology of Biomolecules and Materials, Faculty of Sciences and Technology, Hassan II University of Casablanca – sequence: 9 givenname: El mati surname: Khoumri fullname: Khoumri, El mati organization: Laboratory of Physical Chemistry and Biotechnology of Biomolecules and Materials, Faculty of Sciences and Technology, Hassan II University of Casablanca
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Snippet	Thin films of Cu 2 CoSnS 4 (CCTS) are electrodeposited onto fluorine tin oxide substrate using pulsed electrodeposition mode for various time periods followed... Thin films of Cu2CoSnS4 (CCTS) are electrodeposited onto fluorine tin oxide substrate using pulsed electrodeposition mode for various time periods followed by...
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SubjectTerms	Chemistry Chemistry and Materials Science Diffraction patterns Electrical properties Electrochemical impedance spectroscopy Electrochemistry Electrodeposition Energy gap Fluorine Industrial Chemistry/Chemical Engineering Pattern analysis Physical Chemistry Pulse duration Raman spectra Raman spectroscopy Research Article Silver Spectrum analysis Substrates Sulfurization Thin films Tin Tin oxides X-ray diffraction
Title	Pulsed potential co-electrodeposition of Cu2CoSnS4 absorber layer on fluorinated tin oxide (FTO)-coated glass
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